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HomeMy WebLinkAbout38316 ALD009840653 089 20020925 CSSI PJL SITE INVESTIGATION CERCLA SITE INVESTIGATION ON JOHN BLUE COMPANY MADISON COUNTY HUNTSVILLE,ALABAMA Pti� PVp PBA T Prepared by: Kenneth L. Prestridge Site Assessment Unit,Environmental Assessment Section Hazardous Waste Branch, Land Division Alabama Department of Environmental Management September 25,2002 Date: September 19,2002 Prepared by: Kenneth L.Prestridge Land Division,Environmental Assessment Section, Site Assessment Unit Alabama Department of Environmental Management Site: John Blue Company 2800 Bob Wallace Avenue Southwest Huntsville,Alabama Madison County EPA ID No.: ALD 009840653 Ref#: 7 3 3 g 1. INTRODUCTION Under authority of the Comprehensive Environmental Response, Compensation,and Liability Act of 1980(CERCLA)and the Superfund Amendments and Reauthorization Act of 1986 (SARA)and a cooperative agreement between the U.S. Environmental Protection Agency and the Alabama Department of Environmental Management(ADEM),a Site Investigation(Sir was conducted at the former John Blue Company Company Site in Huntsville,Alabama. The purpose of this investigation was to collect information to assess/reassess the site and update the information based on the current CERCLA ranking model. The investigation also determined if there were additional considerations to address under CERCLA. The SI included reviewing previous information,site screening by using GeoProbe®borings, surface water drainage sampling, and laboratory analysis,developing a worst case scenario model,developing a study model and carrying out the study plan when the benchmark/cutoff scores were met or exceeded. 2.0 SITE DESCRIPTION The site is a former foundry located at 2800 Bob Wallace Avenue Southwest in Huntsville,AL 5" Street and I"Street. The site comprises approximately 12 acres within an urban/commercial and residential area. The site is located at Latitude 34°4248.5"North,Longitude 86036'28" West;Township 4 South,Range 1 West; SE 1/4, SE 1/4,SE %4 of Section 3 of the Huntsville, Alabama 7.5 Minute topographical map(Attachment 1;Reference 1). 3.0 WASTE/SOURCE SAMPLING During the Site Investigation,borings at three locations were performed utilizing the direct push GeoProbe®unit to ascertain if groundwater was being impacted by prior practices at this C John Blue Company Company- SI Report September 19,2002 Page 2 site(see attached map for each locations). In addition, surficial water and sediment samples were taken along the surface water drainage pathway to ascertain if runoff from the site was impacting the surface water pathway. The contaminants of concern on this site are arsenic, lead, and other heavy metals as well as possible VOCs due to past historical practices of foundries in the state. Groundwater sampling performed included groundwater samples GW-JBC-01,GW-JBC-02, GW-JBC-03,and GW-JBC-D(see attached map for sample location). In addition,public water supplies were sampled at the Lowe Mill Well and at Braham Springs(PWS-WHC/JBC-LMW, and PWS-WHC/JBC-BS respectively).And,finally,the surface water pathway was sampled utilizing 6 sample locations along the stormwater ditch,through Braham Springs,to the confluence of Merrimac Branch and Huntsville Spring Branch, and finally downstream on Huntsville Spring Branch(Reference 1 and 10). The surface water pathway was sampled utilizing both sediment and surface water samples(Reference 1 and 10). Sediment samples were taken at sample locations: SD-LJNT-10, SD-ANT-09, SD-BS-02, SD-MMB-03, SD-HSB-01,and SD-HSB-D(dupficate). Surface water samples were taken at sample locations: SW-BS-02,SW- MMB-03, SW-HSB-01,SW-HSB-D(duplicate),and SW-HSB-05 (sediment sample locations and surface water locations with similar numbers correspond)(Reference 1 and 10). All of these samples were analyzed for various metals(ie. arsenic,cadmium,chromium, lead and mercury)and volatiles. All three boring locations exhibited elevated levels of metals. Borings GW-JBC-01, GW-JBC-03,and GW-JBC-D also exhibited some elevated levels of various volatile constituents(to be further discussed in the groundwater pathway section)(Reference 1 and 10). Along the surface water pathway,one of the six sample locations exhibited detectable levels of lead--no volatiles were found to be above the method detection limit in any of these six sample locations(Reference 1 and 10). 4.0 GROUNDWATER PATHWAY There is historical analysis of contamination in the municipal drinking water wells(ie. Braham Springs and Lowe Mill Well),which indicates that hazardous substances have possibly migrated into groundwater and impacted the public drinking water supplies in this area. In 1988 and 2000, tetrachloroethylene was detected in Lowe Mill Well at 0.006 mg/L and 0.00176 mg/L respectively. In 1997,Braham Springs exhibited elevated levels of TCE(Trichloroethylene)and Tetrachloroethylene at 0.0009 and 0.0006 mg/L respectively(Reference 5 and 7). Sampling of these public water supplies during this last sampling event showed no elevated levels of any volatile organic compounds or metals analyzed for(Reference 5 and 7). In addition,the Dallas Well and Lincoln Well exhibited detectable levels of tetrachloroethylene(10.6 and 4.lppb respectively)and trichloroethylene in the Lincoln Well at 6.8 ppb on August 31,2000(Reference 5 and 7). On the John Blue site,boring GW-JBC-01 (of which GW-JBC-D is a duplicate) exhibited elevated levels of mercury(0.354 ug/L),trichloroethene(409.0 ug/L and 343.25 ug/L), and cis-1,2-Dichloroethene(35.8 ug/L). Boring GW-JBC-02 exhibited elevated levels of lead (9.40 ug/L) and mercury(0.516 ug(L). And,boring GW-JBC-03 exhibited elevated levels of C John Blue Co any Company—SI Report September 19,2002 Page 3 chromium(0.016 ug/L)and lead(2.39 ug/L)and Acetone(230.0 ug/L)(Reference 10). The Huntsville Utilities provides drinking water for the City of Huntsville(Reference 6 and 11). This is a blended system that uses 40 percent groundwater and 60 percent surface water. The system serves a population of 208,000 and obtains water from two surface water intakes on the Tennessee River and five wells and one spring. The estimated portion of the population supplied by the 5 wells and one spring is 79,394 individuals.Based on total production of the wells and spring in the system, apportioned figures for each well is estimated as follows: Braham Spring 8,927; Williams Well, 18,082;Dallas Well,20,830; Lincoln Well,23,806; Lowe Mill Well, 6,716;Hampton Cove Well, 1,033 individuals. There are 3 active public water supply wells (Lowe Mill,Dallas, and Lincoln)and 1 inactive public water supply spring(Braham Spring) which is maintained as a standby water supply within the 4-mile target distance limit from the site(Reference 6 and 11). The closest active public water supply well is the Lowe Mill Well located approximately 0.4 miles to the northeast of the site(Reference 6 and 11). 5.0 SURFACE WATER PATHWAY Surface water drainage from the site appears to be to the east/southeast into an untamed tributary of the Merrimac Branch. The unnamed tributary flows approximately 1.23 miles to the south and flows into Merrimac Branch. From this point,Merrimac Branch flows approximately 0.07 miles to the southeast and joins Huntsville Spring Branch. Huntsville Spring Branch flows approximately 11.2 miles to the southwest into Indian Creek—which comprises the remainder of the 15-mile target distance limit of the surface water pathway(Reference 1 and 10). The unnamed tributary of Merrimac Branch and Merrimac Branch have no use classification listed in the ADEM Admin. Code R. 335-6-11-.02 which defaults to a use classification of fish and wildlife. Huntsville Spring Branch and Indian Creek are listed with use classifications of fish and wildlife(Reference 3). The unnamed tributary of Merrimac Branch,Merrimac Branch and Huntsville Spring Branch have a low flow rates estimated to be less than 10 fl'. Indian Creek has a seven day,ten year low flow rate of 2.9 R3 and a seven day,two year low flow rate of 4.0 fl' (Reference2 and 11). There are no known surface water intakes within 15-Miles downgradient of the site along the surface water pathway. There are approximately 4.5 miles of wetlands located along the surface water pathway and approximately 8.9 miles of the surface water pathway flows through and is located within the boundary of Wheeler National Wildlife Refuge (Reference 1, 10 and 11). Water and sediment samples were taken along the 15-mile target distance limit of the surface water pathway from the John Blue Site(Reference 1 and 10). Sediment samples were taken at sample locations: SD-UNT-10, SD-UNT-09, SD-BS-02, SD-MMB-03, SD-HSB-01, and SD- HSB-D(duplicate). Surface water samples were taken at sample locations: SW-BS-02, SW- MMB-03, SW-HSB-01,SW-HSB-D (duplicate),and SW-HSB-05 (sediment sample locations and surface water locations correspond) (Reference 1 and 10). Sample analysis for the sediment Isamples had no constituents(ie.metals and volatiles), show up above method detection limits (MDL). The water sample, SW-BS-02,had one result above the method detection limit. In this 0 0 John Blue Company Company-SI Report September 19,2002 Page 4 sample lead results indicated 2.13 ug/L,slightly above the 2.00 ug/L MOL. No other constituents were present in the analysis of any other sediment or water sample take from this surface water pathway during this round of testing; however,historical testing of the public water supplies performed in August 1997 exhibited results for trichloroethylene in the Braham Spring at 2.6 ppb(ug/L)(Reference 5 and 10). Braham Spring is utilized for recreation, a standby public water supply,and for fishing(direct observation of investigators)(Reference 5 and 10). Since this is a spring fed pond/small lake,the drinking water threat will be addressed under the groundwater portion of the investigation,while the possibility of being impacted as a fishery and sensitive environment will be addressed under the surface water portion of the investigation. 6.0 SOIL EXPOSURE AND AIR PATHWAY The nearest residence is approximately 30 yards from the site(Reference 1,7 and 10). There are approximately 100 workers at various businesses as well as 225 students attending classes at the Virginia College situated on the former John Blue Site(Reference 7,9 and 10). The nearest school is located approximately 0.2 miles to the northwest. There are 43 schools located within the 4-mile distance radius from the site(Reference 1,7,9 and 10). The estimated population within the four miles target distance radius of the site is as follows: RADIUS RESIDENCES I COUNTY AVG DISTANCE RING POPULATION (in Miles) (per household) (avg per house) 0- 1/4 265 2.78 3.75 993 1/4- 1/2 797 2.78 2.39 1,901 1/2- 1.0 3,342 2.78 2.44 8,154 1.0-2.0 10,552 2.78 2.49 26,241 2.0-3.0 11,798 2.78 2.45 28,895 3.0-4.0 10,520 2.78 2.76 29,038 Total population within the 4-mile radius is 95,312 when workers and students on site are factored in to the total population(Reference 1 and 8). The site has minimal fencing along the north and west edges of the property,with the east and south open to the streets (Reference 1 and 111. No soil samples were taken at this site during this investigation. 7.0 CONCLUSIONS AND RECOMMENDATIONS Based on the current available data,ADEM recommends this site for further action and consideration with regards to CERCLA or SARA. Heavy metal and volatile organic compounds in the groundwater should be addressed. Further testing should be performed to ascertain how extensive soil contamination is on site. Possible cleanup actions by property owners with oversight by the State or EPA could be investigated as an alternative to NPL listing. R 12 s CONFIDENTIAL Q t1 REFERENCES i `J John Blue Company Company—SI Report September 19,2002 Page 5 REFERENCES 1. U.S.G.S. 7.5 Minute Series Topographic Quadrangle Maps of Alabama: Capshaw, 1958 (Photorevised, 1982);Farley, 1964(Photorevised 1982);Greenbrier, 1975 (Photorevised 1988);Huntsville, 1975;Jeff, 1967(Photorevised, 1982);Madison, 1975 (Photorevised, 1991);Mason Ridge, 1949(Photorevised, 1973);Maysville, 1948(Photorevised, 1982); Meridianville, 1964;Moontown, 1948 (Photorevised, 1974);New Hope, 1947 (Photorevised, 1973);Triana, 1964(Photorevised, 1982). Scale 1:24,000. 2. United States Geological Survey in cooperation with the Geological Survey of Alabama. 7- Day Low Flow and Flow Duration of Alabama Streams Through 1973. University of Alabama, 1978. 3. Alabama Department of Environmental Management, Water Division,Water Quality Program, "Water Use Classification', 1986. 4. U.S. Department of Commerce, 1985,Local Climatological Data,annual summary:National Oceanic and Atmospheric Administration,published annually. 5. Alabama Department of Environmental Management,Federal Reporting Data System(FRDS II),Public Water Supply Summary. Huntsville area municipal water supply system. 6. Geohydrology and Susceptibility of Major Aquifers to Surface contamination in Alabama; Area 1,C.R.Bossong and Wiley F.Hams,U.S.Geological Survey, Water Investigations Report 86-4360, 1987. 7. Preliminary Assessment,Alabama Department of Environmental Management,John Blue Company,Huntsville,Alabama,Madison County,ALD 009840653. 8. Alabama State Data Center, Center for Business and Economic Research,College of Com- merce and Business Administration,. The University of Alabama. 1990 CENSUS Alabama Counties and Cities By Race. 9. State of Alabama-Department of Education,Alabama School Populations for 1992 10.Kenneth L. Prestridge,Matt Thomas,Amold Mayberry,Anne Cross and Joe Gibson,ADEM, Land Dividion, Site Assessment Unit, Site Reconnaissance and sampling event,July 10 and 11,2002. 11. Joe Gibson,ADEM,ADEM,Water Division,Groundwater Branch, Hydrogeology Report, February 13,2001. V V ATTACHMENTS John Blue Company Company—SI Report September 19,2002 Page 6 ATTACHMENTS Attachment 1 ........................ 7.5 Minute Topographic Map Attachment 2......................... County Map Attachment 3......................... CERCLA Preliminary Assessment, John Blue Co. Attachment 4......................... Site Sketch Attachment 5......................... Historical Sandbom Maps Attachment 6......................... Site Borings Sampling Locations Maps Attachment 7......................... Site Borings/Public water supply Laboratory Analysis Attachment 8......................... Surface Water Sample Location Map Attachment 9......................... Surface Water/Sediment Laboratory Analysis Attachment 10......................... Hydrogeology Report,February 2001 Attachment 11......................... Excerpt from FRDS II Attachment 12................... Photos c � ATTACHMENT 1 i I II ' , /�' ,� y ,.J ", i %. \ ...,,_,:. '\ v-. 4. :`_ . . -.,- / '• V ' ^,� i'l'/� \ I , } :. 1 r, '� �_ /��,. � 1. 1c� :,i!1, \- r - v ta` .I\ �r r 11 ,� k; 3- 10560-0000 \i. PN , •'1 I # ,yam _y, er(43L C. ::l wt I ' ,I: `5 'N I,, ,�• /f_ 'i v '� e1 ,�I�rr, al•T,i„ �. i n I I � ..:" . I 'r �� , \ \ t1 i� : _ 1 w : / k'L "T fl� I1" 7 L/ I '\-` ,/ S 'I .\ i ,i 4v.9�1- :•4.< bN i- ,s- _ `.-� -`' i .�!:• : _ I O ..:\_ ' p¢ " i _ +m ` 1 �\ ks-. r- i-,,r _ "�' s,.. 'a�a ' `�!, - � � yy v 't\ C•"' d _ .l �"� `4 S ,x�I: \ % l i•1 5 : _ Ir -_ I , - - L � .1. 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F a �w.a er 6.,..Ys':r �� �f yE 1� EoocA Io x coRnFci I9 J ,,(( IT .,.,M _ i ....,. x.e. x,::: ,.. 1 3 �L� i�3333 1 H G nPo s e e .Ymrxo _ .._ i e •mn,e... . :,° m. • - uuxvna®o I-W FIT8 o � -� ALASAT4A t)F.PAR.TItiLENT OF 'TRANSPORTATION 'zF111TITT Y ILA BUREAU OF TNSPfORTATION PLANNLN Y Eee Y:° UI a SUR Rif; 0.N.p MAPPING ➢lYLS10N ; . 6lR'BS ' IrRM1'r RiN wrm iN¢ III e .c•uc.nx.b .. O .. ? g e••t - a . DEPARTMENT OF TRANSPORTATION of ! - — .._ FEDERAL tLI[,t 3lvA.•_ Y :, moeanl _ F ® v Y AD, f1NITUT?ATION x __ _- FFF [ - fR5 8 m _ VIS[ELuv.LLE f au[ In I Y4 1 6F II 1 7 i * FITA E - 1•w •,I 1996 .a ttw • - . • . c,n.p ne otll kun m r t Ir naPaxaund n _. o _ v ve• ? e _ •#• rmnn Yr�tlwPgtl IT.9tl binfine - n fv'M _ : _ • r ,wasw -0M1M Ah[an 4lil - Iry4:n0r1•z,Nm ,. ...en .e,e a •,• ...... mw pd•W+Mr,uu . mm -rl n -I. IPa.I IM. R - Ip • - PrinN etl MlM nlh nrf:h ATTACHMENT PRELIMINARY ASSESSMENT JOHN BLUE COMPANY HUNTSVILLE, MADISON COUNTY, ALABAMA CERCLIS SITE REF. No.: �tip,BA� ti Prepared By Lawrence A.Norris Alabama Department of Environmental Management EnvironmentalAsseasment Section 1 TABLE OF CONTENTS 1. INTRODUCTION 1 2. SITE DESCRIPTION.OPERATIONAL HISTORY,AND WASTE CHARACTERISTICS 2.1 Location 1-2 2.2 Site Description 2-3 2.3 Operational History and Waste Characteristics 3 3. GROUND WATER PATHWAY 3 3.1 Hydrogeologic Setting 3 3.2 Ground Water Targets 4 3.3 Ground Water Conclusion 5 4.SURFACE WATER PATHWAY 5 4.1 Geomorphologic Setting 5-6 4.2 Surface Water Targets 6 4.3 Surface Water Conclusion 6 5. SOIL EXPOSURE AND AIR PATHWAY 7 5.1 Physical Conditions 7 5.2 Soil and Air Targets 7-10 5.3 Soil and Air Pathway Conclusion 10 6. SUMMARY AND CONCLUSIONS 10 REFERENCES (29) PLATES (19) FIGURES (13) ATTACHMENTS (29) Date: August 31, 2001 Prepared by: Lawrence A. Norris(Site Investigator) Northern Compliance Section ADEM—Hazardous Waste Branch Site: John Blue Company 2800 Bob Wallace Avenue Huntsville, Madison County,Alabama CERCLIS Na: 1. INTRODUCTION Under authority of the Comprehensive Environmental Response, Compensation, and Liability Act of 1980 (CERCLA) and the Superfund Amendments and Reauthorization Act of 1986 (SARA) and a cooperative agreement between the U. S. Environmental Protection Agency and the Alabama Department of Environmental Management (ADEM), a Preliminary Assessment (PA) was conducted at the former John Blue Company site. The purpose of this investigation was to collect information concerning conditions at the site sufficient to assess the threat posed to human health and the environment and to determine the need for additional investigation under CERCLA/SARA or other action (Ref. 16). The scope of the investigation included a review of available file information, a comprehensive target survey, and site reconnaissances conducted on December 20, 2000 and May 3, 2001 (Ref. 25 & Atts. 2 & 4). 2. SITE DESCRIPTION,SITE HISTORY,AND WASTE CHARACTERISTICS 2.1 Location The former John Blue Company is located at 2800 Bob Wallace Avenue Southwest in Huntsville, Alabama (Refs. 1, 20 & 27, Figs. 1, 2, 7, & 10 & Atts. 1 & 29). The City of Huntsville has a population of approximately 159,800 and outlying areas add almost 40,000 more to the population (Ref. 10, Att.13). Huntsville is centrally located in Madison County, Alabama. More specifically, the site is an approximately twelve acre parcel of land located in the southeast '/. of the southeast''/.of the southeast ''/C of Section 3, Township 4 South, Range 1 West (Ref. 3 & Art. 1). The geographical coordinates of the site, determined by the Topozone.com database, are 34° 42' 48.5"North Latitude and 860 36'28"West Longitude(Ref. 27&Att. 29). Madison County has a mild, temperate climate with an average annual temperature of 62°F. The average temperature during the summer is 80°F, and the average temperature during the winter is • ,ohn Blue Company 46°F (Malmberg and Downing, 1957). The average annual rainfall is 52 inches, and approximately 22 of the 52 inches of rain per year runs off into the streams (Bossong and Harris, 1987)(Ref. 3 & Att. 1). The John Blue Company site is located in an area determined to be inside of the 500-year flood plain(Ref 11 &Fig. 8). 2.2 Site Description Is The John Blue Company site is located in the city of Huntsville, Alabama at 2800 Bob Wallace Avenue Southwest. The facility is no longer in business at this site, however numerous other businesses (primarily retail) now occupy buildings that were once part of the former John Blue Company. The former John Blue Company site is flat and the site is partially paved or otherwise covered with buildings. The businesses now operating on the site are diverse and unrelated to the former John Blue Company. These businesses include, the Center for Site, Robbins Music Center, Haley's Carpet & Rugs, the Huntsville Madison County Home Builders Association, a new under-construction Center for Site (Plate 18), the InLine Electrical Supply Company, the Alabama Cut Flowers Exchange, Knology, the Three States Supply Company, the Baker Service Center (Plates 6, 7, 8 & 9), VIP Courier, Specialized Medical Devices, the Virginia College at Huntsville(rear building) (Plate 5), MNT Machine (Plates 10, 11 & 12), the Virginia College at Huntsville (front building) (Plate 4), and the McLain Commercial Real Estate Office Building (Plates 1 & 3). The McLain Commercial Real Estate Office Building houses a number of diverse business offices as well (Plate 2). There is also a single microwave tower located on site (Plate 16). The area immediately north and also to the east of the site is occupied by residences. The West Huntsville Elementary School is located less than two blocks from the site to the northwest. Various businesses are located to the west of the site. A field, various businesses and an apartment complex are located south of the site across Bob Wallace Avenue. There were no well-defined erosion channels. The site covers approximately 12 acres about half of which is open field (Plate 17). The concrete foundation of the original foundry is still intact (Plate 15) and an old railroad spur is also visible(Plate 13). There is a fenced scrap metal area on the north side of the site (Platel4). Although the site is relatively flat, there are drainage ditches on the north, east and south borders of the site. The major drainage path is to the southeast(Plate 19). The John Blue Company site is situated in central Madison County,in the Tennessee Valley District of the Highland Rim Section of the Interior Low Plateaus Physiographic Province. The Tennessee Valley District consists of plateaus of moderate relief with chert belts in the north and limestone plains along the rivers. Elevations in this district range from 600 to 800 feet MSL (Sapp&Emplaincourt, 1975). A review of the RCRA Handlers list indicates that there are 76 conditionally exempt small quantity generators, 109 small quantity generators, and 30 large quantity generators in the Huntsville area (Att. 5). There are presently 224 active NPDES Construction Stormwater Permits in Madison County (Att. 6). There are presently 8 active NPDES Mining Permits in Madison County(Att. 7). A search of the ADEM SARA Title III Database and an EPA TRI web search indicated 175 sites (Ref. 19, &Atts. 8 & 22). A review of the ADEM Wasteland Database 2 •• iohn Blue Company found 50 sites in the Huntsville area (Ref. 18, & Att. 9). A review of the City of Huntsville Underground Storage Tanks (USTs) and Leaking Underground Storage Tanks (LUSTs) listing found 467 registered USTs and 129 LUSTs (Art. 20). 2.3 Operational History and Waste Characteristics A historical search including Sanborn Map information (Atts. 11 & 28, Fig. 11), and an interview with personnel(Ref 25, & All. 4) at the most recent John Blue site indicated that the property on which the site is located had been closed and sold in 1986. There are no personnel working at the present site who were employed at the time that the Bob Wallace Avenue site was in operation. Sanborn records seem to indicate that a foundry existed at the site prior to operation by the John Blue Company, maybe as far back as the late 1920's. The John Blue Company started production of various types of farming implements at the site in January of 1946. The site was located on a twelve acre parcel of land and had approximately 43,000 square feet of floor area at start up. By 1954, the facility had expanded to 140,000 square feet. The site contained a die shop, pattern shop, both aluminum and gray iron foundries, forge shop, steel storage area, machine shop, press shop, welding shop, assembly department, paint department, woodworking shop, warehouse, office space, and engineering and experimental divisions. Although the company now primarily produces pumps at its present location, the old Bob Wallace site produced fertilizer distributors, row-crop sprayers and dusters, cotton and corn planters, disc harrows, stalk cutters, and corn shellers and mills. During this time frame, the John Blue Company became the largest independent farm implement manufacturer in the South. No other historical information could be located (Atts. 11 & 28, Fig. 11). As listed in the latest county tax records, the current owners of record are; Eugene M. McLain, Realsight, Inc., Huntsville Madison County Builders, InLine Properties, Inc., Carpet Associates, Inc., Berlin and Carey Robbins and John and Ruth Parker (Ref. 2, Att. 16, Fig. 9). 3. GROUND WATER PATHWAY 3.1 Hydrogeologic Setting The geologic unit that outcrops in the vicinity of the West Huntsville site is the Tuscumbia Limestone (Fig. 5). This unit consists of massive and thin beds of coarsely crystalline dark to light-gray compact limestone. The Tuscumbia Limestone contains interbedded layers of gray chert and the thickness of this unit in the Huntsville area is approximately 200 feet (LaMoreaux, et al., 1950). The site is located in an area that is underlain by limestone and is susceptible to karst development(Refs. 3 & 13, Fig. 5, &Att.1). Geologic units exposed in Madison County range in age from Silurian to Pennsylvanian and consist main) of Mississippian limestones overlain b outliers of Pennsylvanian sandstone shale Y PP Y Y , and coal. The units are essentially flat-lying with a gentle dip to the south and the east (LaMoreaux, et al., 1950). 3 - rr„ • . • rohn Blue Company 3.2 Ground Water Targets The aquifers that have recharge areas in the vicinity of the city of Huntsville are the Fort Payne — Tuscumbia aquifer, Monteagle aquifer, and the Bangor aquifer. The site is located in the recharge area of the Fort Payne—Tuscumbia aquifer (Moore, 1992). The Fort Payne—Tuscumbia aquifer is composed of the Monteagle Limestone, the Tuscumbia Limestone, and the Fort Payne Chert. The most significant sources of water in this aquifer are the Tuscumbia Limestone and the Fort Payne Chert. The aquifer is recharged throughout its outcrop area by water that infiltrates through the regolith, and is partially confined due to the lower hydraulic conductivity of the overlying regolith. The majority of water available in this aquifer is present in joints and bedding planes that have been enlarged by dissolution(Bossong and Harris, 1987). There are 3 active public water supply wells and 1 inactive public water supply spring located within 4 miles of the site(Figure 6). The closest active public water supply well (Lowe Mill Well) is operated by Huntsville Utilities, and is located approximately 0.75 miles to the northeast of the site. See the table at the top of the next page: Brabant Spring Huntsville Utilities Mtf Spring Inactive 0.68 Lowe Mill Well Huntsville Utilities Mtf 78 Public Water Supply 0.75 Dallas Well Huntsville Utilities Mtf 104 Public Water Supply 2.76 Lincoln Well Huntsville Utilities Mtf 106 Public Water Supply 2.8 Mtf -Tuscumbia Limestone and Fort Payne Chert undifferentiated(Bossong and Harris, 1987) Samples collected from Brabant Spring on August 26, 1997 detected tetrachloroethylene at 0.6 ppb and trichloroethylene at 0.9 ppb, and groundwater samples collected from the Lowe Well on August 31, 2000 detected tetrachloroethylene at 1.7 ppb and trichloroethylene at 2.6 ppb. Groundwater samples collected from the Dallas Well on August 31, 2000 detected tetrachloroethylene at 10.6 ppb, and groundwater samples collected from the Lincoln Well on August 31, 2000 detected tetrachloroethylene at 4.1 ppb and trichloroethylene at 6.8 ppb (FRDS, 2000)(Refs. 12, 14, 28, & 29). A treatment system has been constructed to treat contaminated water pumped from the Lincoln and Dallas wells prior to delivery to the water system. The Huntsville Utilities water system is a blended system that uses 40 percent groundwater and 60 percent surface water. The system serves a population of 198,000 and obtains water from two surface water intakes on the Tennessee River and five wells (FADS, 2000)(Refs. 3 & 12, & Atts. I & 3). The site is located in the wellhead protection areas for Brabant Spring and the Lowe well, and the general groundwater flow direction in the area of the site is to the southeast (Baker and Mann, 1996). Private water supply wells are not expected in the immediate vicinity of the site due to the urban nature of the site. 4 0 iohn Blue Company 3.3 Ground Water Conclusions There are 3 active public water supply wells and 1 inactive public water supply spring located within 4 miles of the site (Figure 6). The closest active public water supply well (Lowe Mill Well) is operated by Huntsville Utilities, and is located approximately 0.75 miles to the northeast of the site. New domestic and industrial wells could possibly be located within a four-mile radius of the site, and the wells that have been identified within a four-mile radius of the site could have been abandoned or may no longer be in use (Ref. 3 & Att. 1). Subterranean caves with identified populations of federally listed endangered species i.e. Gray bats (Myotis griecens) and Alabama cave shrimp(Palaemonias alabamae) are have been physically identified in the vicinity of this site (Refs. 8, 9, 13, 15 & 21, Fig. 12, & Atts. 23, 24, 25, 26 & 27). Groundwater contamination with constituents commonly used in dry cleaning operations has been discovered in the public water supply wells serving the Huntsville area (Ref. 3 & Att. 1). Even under the assumption that there has been no release to the groundwater pathway, the John Blue Company warrants further investigation due to its relative proximity to the Huntsville public water supply, proximity of physically identified, listed endangered species, the karst geology of the region, and the potential proximity to the shallowest aquifer. The Huntsville Utilities water system receives approximately forty percent of its water from the aforementioned public water supply wells. A total of 198,000 customers receive their public water from the Huntsville Utilities water system and could be subject to potential contamination from the John Blue Company site via the groundwater pathway(Ref. 3, Fig. 13, & Aft. 1). 4. SURFACE WATER PATHWAY 4.1 Geomorphologic Setting The surface elevation at the site is approximately 600 feet MSL. (Att. 1). Surface water drainage from the site (Fig. 3) appears to be to the east and then south into Merrimac Branch. The approximate overland distance through a drainage ditch to Merrimac Branch is approximately 600 hundred yards. Merrimac Branch flows approximately 1.58 miles to the southeast into Huntsville Spring Branch. Huntsville Spring Branch flows approximately 11.2 miles to the southwest into Indian Creek, and Indian Creek comprises the remainder of the 15-mile surface water pathway from the site. The last 4.25 miles of Huntsville Spring Branch and the 2.2 miles of Indian creek along the surface water pathway are considered to be within Wheeler Lake. Merrimac Branch is not listed in the ADEM Admin. Code R. 335-6-11-.02 with a use classification; however, it is noted in the regulations that segments not listed should be designated as fish and wildlife. Huntsville Spring Branch and Indian Creek are listed with use classifications of fish and wildlife (Refs. 6 & 7, Att. 10). Low flow data was not available for Merrimac Branch and Huntsville Spring Branch; however, Merrimac Branch and Huntsville Spring Branch are small to minimal streams and the low flow rates are estimated to be less than 10 cfs. Indian Creek has a seven day ten year low flow rate of 2.9 cfs and a seven day two year low flow rate of 4.0 cfs (Hayes, 1978)(Refs. 5, 23, &24, Att. 26). Wetlands are present along approximately 4.5 miles of the 5 O • iohn Blue Company surface water pathway, and no known surface water intakes for public drinking water supplies are located along the 15-mile surface water pathway from the site (Ref. 1, Figs. 3 & 10). Approximately 8.6 miles of the surface water pathway are located within the boundary of the Wheeler National Wildlife Refuge(Ref. 1 & Fig. 10). 4.2 Surface Water Targets Within 4 miles of the targeted overland drainage and surface water pathways, there are identifiable wetlands that could come in contact with water from the site (Ref. 1, Fig. 10). The John Blue Company site, and the land along the banks of Merrimac Branch of Spring Branch of Indian Creek and its intermittent tributaries might be critical to the support of many threatened and endangered terrestrial species. The following table lists the aquatic wildlife that is thought to have a high probability of being exposed to contaminants from the John Blue Company site if a substantial amount of hazardous constituents were to enter into the surface water pathway: Common Distribution in Name Listing Alabama Gray bat Endangered Tennessee Valley, Shelby & Conecuh Counties Bald Elude Threatened Statewide Slackwater Darter Threatened, Critical Tennessee River habitat Alabama cave shrimp Endan ered Madison Count Pink mucket pearly mussel Endangered Tennessee&Paint Rock Rivers Rough pigtoe mussel Endangered Tennessee River Price's potato bean Threatened Autauga, Madison, & Marshall Counties Morefield's leather flower Threatened Madison County Slabside pearly mussel Threatened Madison County (Refs. 8& 9) 4.3 Surface Water Conclusion Although there is a conduit(i.e. drainage ditches on the east and southeast side of the property), a release to the surface water pathway should not be assumed. The site is a relatively flat parcel of land and the majority of the activity where operations occurred is still either paved or under roof. There was no physical evidence (i.e. stressed vegetation or soil discoloration) of a past surface discharge during reconnaissance. It should be noted, however, that the field adjacent to where production activities occurred does have evidence of the disposal of foundry waste (primarily sand)which historically have contained heavy metal concentrations. 6 • • John Blue Company 5. SOH.EXPOSURE AND AIR PATHWAY 5.1 Physical Conditions The Soil Conservation Service (SCS) classifies soils at the John Blue Company site as Ooltewah silt loam. Soils in this classification are brownish, poorly drained to moderately well drained soils that consists of local alluvium washed from soils developed over high-grade limestone. Generally the surface layer consists of a brown to reddish-brown friable silt loam, and the subsoil consists of a brown friable silty clay loam mottled with reddish yellow and yellowish gray(Refs. 3 &4, Fig.4, & MIA). Limestone bedrock occurs at depths greater than 6 feet in this soil unit. The permeability of these soils is moderate, and they have a slope of 0 to 2 percent (Swenson, et al., 1958). 5.2 Soil and Air Targets There are approximately 100 people working at businesses as well as 225 students attending class at the Virginia College all now located on the former John Blue Company site. Residences are located as close as 30 yards from the site. The nearest school, West Huntsville Elementary School, is approximately .2 miles northwest of the site and has 330 students enrolled. The Life of God School, located approximately .45 miles north northwest of the John Blue Company site, presently has 24 students enrolled. The Roy L. Stone Middle School is located .5 miles to the north and has 439 students. Westlawn Middle School is located approximately .9 miles to the west of the site. There are 39 other public and private schools that are known to exist between 1 and 4 miles from the site. The schools are fisted on the following table: SCHOOLNAME STUDENT STAFF DISTANCE POP'N POP'N FROM SITE West Huntsville Elementary School (K-5) 330 42 0-.25 Life of God School (K-6) PRIVATE 24 10 .25-.5 Roy L. Stone Middle School (6-8) 439 83 .5-1 Westlawn Middle School (6-8) 423 66 .5-1 Academy for Academics&Arts(K-8) formerly Calvary Hill Jr. High 396 60 1-2 Catholic High School (9-12) PRIVATE 157 23 1-2 Center for Developmental Learning (K-12) 71 33 1-2 Grace Lutheran School (K-8) PRIVATE 186 18 1-2 Holy Family School(K-8) Private 192 23 1-2 Huntsville Achievement School(K-8) PRIVATE 31 6 1-2 Huntsville Christian Academy(K-12)PRIVATE 150 13 1-2 Huntsville High School (9-12) 1011 144 1-2 Louis J. Moms Elementary School (K-5)formerly Madison Pike 362 55 1-2 McDonnell Elementary School(K-5) 414 54 1-2 Oakwood Academy(K42) PRIVATE 327 26 1-2 Randolph School (K-12)PRIVATE 750 110 1-2 Ridgecrest Elementary School (K-5) 485 55 1-2 7 • Sohn Blue Company SCHOOLNAME STUDENT STAFF DISTANCE POP'N POP'N FROM SITE S.R. Butler High School (9-12) 1152 134 1-2 Terry Heights Elementary School (K-5) 212 35 1-2 The Selden Center(K-12) 330 23 1-2 Valley Fellowship Christian Academy(K-12) PRIVATE 225 35 1-2 Blossomwood Elementary School (K-5) 363 41 2-3 East Clinton Elementary School (K-5) 200 34 2-3 Holy Spirit Catholic School (K-8)PRIVATE 420 40 2-3 Huntsville Middle School (6-8) 699 178 2-3 Lincoln Elementary School (K-5) 232 41 2-3 Montview Elementary School (K-5) 321 39 2-3 Schola Maxima Primary Day School (1-4) PRIVATE NA NA 2-3 The Reading Center PRIVATE NA NA 2-3 University Place Elementary School (K-5) 496 58 2-3 Westminster Christian Academy(K-12) PRIVATE 385 60 2-3 Academy for Science& Foreign Language (K-8) 375 61 3-4 Care To Learn School (K-1) PRIVATE NA NA 3.4 Chapman Elementary School (K-5) 348 43 3-4 Chapman Middle School (6-8) 434 78 3-4 Davis Hills Middle School 501 86 3-4 Edward H. White Middle School (6-8) 632 73 3-4 Highlands Elementary School (K-5) 553 60 3-4 Huntsville Islamic Academy(K-6) PRIVATE 27 6 3-4 Jones Valley Elementary School (K-5) 523 61 3-4 Lee High School (9-12) 919 134 3-4 Whitesburg Elementary School (K-6) 375 51 3-4 Whitesburg Middle School (6-8) 568 74 3-4 NA-Not Available Total number of students: 31,676 (Refs. 17, 22, & 26, Atts. 12, 14, 17, 18, 19, & 21) There are no known daycare facilities within one mile of the site. The following table contains a fist of daycare operations known to exist between 1 and 4 miles from the facility. DAYCARE NAME CHILDREN STAFF DISTANCE POP'N POWN FROM SITE Child's World Child Learning Centers 100 17 1-2 Covenant Classical School 83 12 1-2 Covenant Preschool and Kindergarten 60 10 1.2 Deborah's Day Care 40 7 1.2 First Baptist Church 160 34 1-2 First Presbyterian Church NA NA 1-2 Happy Times Preschool NA NA 1-2 Kiddie Kollege Day Care&Kindergarten 70 14 1-2 8 o • '� John Blue Company DAYCARE NAME CHILDREN STAFF DISTANCE POP'N POP'N FROM SITE Madison United Methodist Church 80 17 1-2 Montessori Childrens House NA NA 1-2 Montessori Learning Center 50 7 1-2 Mrs. Ronda's Montessori Academy 55 6 1-2 University Baptist Church Child Development Center 52 10 1-2 Ascension Lutheran Child Development Center 43 12 2-3 First Christian Church 160 18 2-3 Mayfair Child Development Center NA NA 2-3 Trinity Child Development Center NA NA 2-3 Ann's Nursery 58 9 3-4 Barn Christian Academy 68 7 3-4 Cogic Child Development Center 45 5 3-4 Hampton Cove Christian Academy West 130 30 3-4 NA-Not Available (Ref. 25, Atts.12& 15) Total Number of Children: 1204 According to the Alabama 1990 census records, the average number of people living in homes located in Huntsville, Alabama is 2.78 residents per household (Att. 13). In the following table, the total population within the target area has been broken down into sub-populations that live within each specified distance radius from the site: (Ref. 1, &Fig. 10) DISTANCE FROMSITE POPULATION '/4 Mile 743 '/a Mile 2150 I Mile 8197 2 Miles 23390 3 Mlles 25215 4 Miles 27288 TOTALPOPULATION None of the John Blue Company site is considered to be a wetland environment. Within the 4- mile target area and the 15-mile surface water pathway there are identifiable wetlands. It is not known if the John Blue Company site is a critical habitat for federally designated endangered or threatened species, but the table below list the terrestrial species that may utilize the land and surface waters located within the specified target areas: Common Distribution in Name LMng Alabama Florida Panther Endan ered Statewide Bald Ea le Threatened Statewide 9 • (p John Blue Company Common Distribution in Name Listing Alabama Red Wolf Endangered Statewide Backman's Warbler Endangered Statewide Wood Stork Endangered Statewide Red-cockaded woodpecker Endangered Statewide Gray Bat Endangered Madison Count Indiana Bat Endangered Madison Count American Per rine Falcon Endangered Statewide Eskimo Curlew Endangered Statewide Bachman's Warbler Endangered Statewide (Refs. 8, 9, 15, &21, Fig. 12, & Atts. 23 & 24) 5.3 Soil Exposure and Air Pathway Conclusion No obvious air targets or potential air migration pathways are evident at the former John Blue Company site. 6. SUMMARY AND CONCLUSIONS Wetlands are present along approximately 4.5 miles of the surface water pathway. There are no known surface water intakes for public drinking water supplies which are located along the 15- mile surface water pathway from the site. Approximately 8.6 miles of the surface water pathway is located within the boundary of the Wheeler National Wildlife Refuge. Extant records identifying the exact types and volumes of wastes disposed, or otherwise released at the John Blue Company site are not available. However, historically foundries have produced substantial amounts of heavy metal contaminated sand and baghouse dust and that painting operations have produce substantial amounts of volatile contaminated wastes. Current site conditions indicate that the contamination resulting from previous waste handling practices at the John Blue Company have the potential to have impacted groundwater at the site. Due to the site's elevation in relation to the pathways to groundwater and surface water, the potential for migration along these pathways clearly exists. Because of this potential for contamination, and the size of the population such contamination could theoretically effect, a recommendation is made by the ADEM that the John Blue Company site be further evaluated under the authority of CERCLAiSARA. 10 REFERENCES 1. U.S.G.S. 7.5 Minute Series Topographic Quadrangle Maps of Alabama: Capshaw,Alabama 1958 (Photorevised 1982), Farley, Alabama 1964(Photorevised 1982), Greenbrier,Alabama 1975 (Photoinspected 1988), Huntsville, Alabama 1975, Jeff,Alabama 1967 (Photorevised 1982), Madison, Alabama 1975 (Revised 1991), Mason Ridge, Alabama 1949 (Photorevised 1973), Maysville,Alabama 1948 (Photorevised 1982), Meridianville,Alabama 1964, Moonlown,Alabama 1948 (Photorevised 1974), New Hope,Alabama 1947(Photorevised 1973),Triana, Alabama 1964 (Photorevised 1982). Scale 1:24,000. 2. State of Alabama Department of Revenue Ad Valorem Tax Division, County of Madison. 3. Alabama Department of Environmental Management. Memorandum. Gibson, Joe, Groundwater Branch, December 28, 2000. Preliminary Assessment—Groundwater. West Huntsville Cleaners. 4. Stephens, Robert W., United States Department of Agriculture Soil Conservation Service and Forest Service in cooperation with Alabama Department of Agriculture and Industries and Alabama Agricultural Experiment Station, 1984, Soil Survey of Madison County,Alabama. S. Hayes, Eugene C., Geological Survey of Alabama, 1978, 7-Day Low Flows and Flow Duration of Alabama Streams Through 1973. Geological Survey of Alabama Bulletin 113. 6. Alabama Department of Environmental Management; Water Division-Water Quality Program, 1997, Water Quality Criteria, Chapter 335-6-10. 7. Alabama Department of Environmental Management; Water Division-Water Quality Program, 1997, Water Use Classification for Interstate and Intrastate Waters, Chapter 335-6-11. 8. Alabama Department of Conservation and Natural Resources. Alabama Game and Fish Division. Federally Listed Endangered/Threatened Species of Alabama, August 8, 1997. 9. U.S. Fish and Wildlife Service. Daphne Field Office.Alabama's Federally Listed Species(By County). September, 1997. 10. Alabama Municipal Data Book 1993,Alabama Department of Economic and Community Affairs Planning and Economic Development Division, 1992. 11. Federal Emergency Management Agency. National Flood Insurance Program. Flood Insurance Rate Map #01089C0328 D(Panel 328 of 575). Madison County,Alabama and Incorporated Areas. Revised April 20, 1998. 12. Alabama Department of Environmental Management, Federal Reporting Data System (FRDS-ll), Public Water Supply Summary for Selected Areas of Madison and Talladega Counties. 13. U.S. Geological Survey Data Report,AL-97.1, 1998. 14. Handbook of Environmental Contaminants:A Guide for Environmental Assessments, Chris L. Schineldecker, Lewis Publishers, 121 South Main Street, Chelsea, MI 48118, 1992. 0 REFERENCES 15. Geologic, Hydrologic, and Biologic Investigations in Arrowwood, Bobcat, Matthews, and Shelia Caves and Selected Caves, Madison County, Alabama, Geological Survey of Alabama, K.F. Rheams, P.h> Moser, & S.W. McGregor, Tuscaloosa,Alabama 1992. 16, EPA/540/G-911013 P.bfic w 9345.0-01A, Guidance for Performing Preliminary Assessments Under CERCLA, Hazardous She Evaluation Division, Office of Emergency and Remedial Response, Office of Solid Waste and Emergency Response, U.S. Environmental Protection Agency, Washington, DC 20460, September 1991. 17. Internet search for Huntsville City Schools using Lycos Network search engine, 2001 Lyms, Inc., produced http://w .hsv.kl2.al.us./schools/schools.html. 18. Wasteland Data Base search of City of Huntsville using WANG-L VS. OFFICE-Version 2.05.87(c)COpr.Wang 1991,ADEM Central Office-ADEM 100. 19. SARA Title III search of Madison County using WANG-L VS. OFFICE-Version 2.05.87(c) Copr. Wang 1991, ADEM Central Office-ADEM 100. 20. MicroSoft Expedia Streets and Trips 2000, Copyright 1988-1999. 21. United States Fish &Wildlife Service, Endangered Species Act of 1973. 22. 1999-2000 Alabama Education Directory,Alabama State Department of Education, P.O. Box 302101, Montgomery,Alabama. 23. USGS Water Resources Data Alabama-Water Year 1999, Water Data Report AL-99-1,J.L. Peamian, V.E. Stricklin, and W.L. Psinakis. 24. 1996 Alabama Clean Water Stategy Report,Alabama Department of Environmental Management, Montgomery, Alabama. 25. ADEM Environmental Scientist, Lawrence A. Norris, Field Notes from inspections conducted on December 20,2000 and May 3, 2001. 28. BellSouth,The Real Yellow Pages, Huntsville,Alabama 2000-01, BellSouth Advertising & Publishing Corporation. 27. TopoZone-The Web's Topographic Map, http://www.topozone.com/, Maps a la carte, Inc., 2000. 28. NIOSH Pocket Guide To Chemical Hazards, U.S. Department of Health and Human Services, Centers for Disease Control and Prevention, National Institute for Occupational Safety and Health, Publication No. 94-116, U.S. Government Printing Office, June, 1994. 29. Hawley's Condensed Chemical Dictionary, Richard J. Lewis, 12th Ed.,Van Nostrand, Rheinhold, 1993. ATTACHMENT 4 L?dKLS yt a� Gad s0O'll i Ilrr �!!f A _ m e r\ A . . s Y = z 5 a N b D � h D Mo-,,H3LUa MO'Ld NJL4 x 13gwsul z ATTACHMENTS �ilel.s�.a� Y?i � as i a� t�- - g ��IMF—w—;r• L Le aic Y:a� lllif l�a'vasea faC MOR, �1 ! - _ n � n ■ � C. � �i fri;il� � !I a �MOM ®In S1S3 aw I - MIN ATTACHMENT 6 1 Z "• � 1 • r �B'!7.7r r.n'• { ® . 3r � •_y 7T.. y r 7 17 B-2 JBC Ur ` L � I �LAt FORMER JOHN BLUE COMPANY N C Site Inspection 7 Groundvrdter Sample lomGon On-Site Sampling Locations N E Huntsville, Madison County Alabama 100 0 100 200 Feet S ATTACHMENT 7 ADEM 1!&NTGOMERY LABoArORY oe 1890-A Cong.Win.Dickinson Dr.,Montgomery,AL 36109 Z (33a)-260-2T101phone] (33a}271-6718[Fax]O �Analysis Report Date of This Report... OB/06/2002 Fund Code: 521 Date of tire Orieinal Report.. OB/0612002 Send Report.. Anne F.Cross Lab Sample ID: AA31105 Source... GWJBC-01 Collection Date: 07/10/2002 Location... WEST HUNTSVILLE CLEANERS Collection Time: 2:15:00 PM Sample Matrix: WATER Submittal Date: 07/12/2002 Sample Collector: AFCross-AnneCross Submittal Time: 10:45:00 AM Sample Received by: C.D.AMMONS Date Analvsis Validated... 08/06/2002 by WBB The results on the attached report are from the sample that was received and is referenced above. The sample was analyzed using standard EPA(¢sting procedures and quality analysis protocol Instrument calibration and quality control are within acceptable limits of precision and accuracy. A close review by our Quality Assurance Program certifies that all prescribed test hold times were met and our strict quality assurance standards were observed. Submitted by: Zj(a&2ZC, i Quality Assurance Manager ADEM's Central Laboratory has met all Requirements far Certification by EPA Region Four to Analyze Samples for all of the Parameters Required Under the Safe Drinking Water Act Trace Metals Analysis Performed by.... ADC Parameter Result Units MDL Date of Analysis CAS# Method Reference Arsenic, Total <MDL ug/L 10.0 0712912002 7440-38-2 EP4206.2 Cadmium, Total <MDL mg/L 0.003 0712612002 7440-43-9 EPA200.7 Chromium, Total < MDL mg/L 0.015 071262002 7440.47-3 EPA200.7 Lead, Total <MDL ug/L 2.00 0712912002 7439.92-1 EPA239.2 Mercury, Total 0.354 ug(L 0.3 0810612002 7439-97.6 EPA245.2 Volatiles in Liquids Analysis Performed by.... RLH Parameter Result Units MDL Date of Analysis CAS# Method Reference 1,1,1,2-Tetrachloroethane <MDL uglL 125 071152002 630.20-6 SW8260B 1,1,1-Tichloroethane <MDL ug/L 125 071152002 71-55.6 SW8260B 1,1,2,2-Tetrachloroethane <MDL ug/L 125 071152002 79.34-5 SW8260B 1,1,2-Tiichloroethane < MDL ug/L 125 071152002 79.00-5 SW8260B 1,1-Dichloroethane <MDL ug/L 125 071152002 75-34.3 SW8260B 1,1-Dichloroethene < MDL ug/L 125 071152002 75-35.4 SW8260B 1,1-Dichioropropanone < MDL ug/L 125 071152002 613.88-2 SW8260B 1,1-Dichloropropene < MDL ug/L 125 071152002 563-58-6 SW8260B 1,2,3-Tichlorobenzene < MDL ug/L 125 071152002 87.61-6 SW8260B 1,2,3-Tcchloropropane < MDL ug/L 125 0711512002 96.18-4 SW8260B 1,2,4-Tcchlorobenzene <MDL uglL 125 071152002 120-82-1 SW8260B 1,2,4.Trimethylbenzene < MDL ug/L 125 071152002 95-63-6 SW8260B 1,2-Dibromo-3-Chloropropane < MDL ug/L 126 071152002 96-12-8 SW8260B 1,2-Dibromoethane(EDB) < MDL uglL 125 071152002 106.93-4 SW8260B 1,2-Dichlorobenzene < MDL ug/L 125 071152002 95-5D-1 SW8260B 1,2-Dichloroethane < MDL ug/L 125 071152002 107.06.2 SW8260B 1,2-Dichloropropane <MDL ug/L 125 071152002 78.87-5 SW8260B 1,3,5-Trimethylbenzene <MDL uglL 125 0711512002 108.67-8 SW8260B 1,3-Dichlorobenzene <MDL ug/L 125 071152002 541.73-1 SW8260B 1,3-Dichloropropane <MDL uglL 125 071152002 142-28.9 SW8260B Lab Sample Number AA31105 page 1 of 3 Volatiles in Lid..,, ,ti Analysis Performed bO RLH Parameter Resull Units MDL Date of Analysis CAS# Method Reference 1,4-Dichlorobenzene < MDL ug/L 125 0711512002 106-46-7 SW8260B 1-Chlorobutane < MDL ug/L 125 0711512002 109-69-3 SW8260B 2,2-Dichloropropane < MDL ug/L 125 0711512002 590-20-7 SW8260B 2-Butanone < MDL ug/L 125 0711512002 78-93-3 SW8260B 2-Chlorotoluene < MDL ug/L 125 0711512002 95-49-8 SW8260B 2-Hexanone < MDL ug/L 125 0711512002 591-78-6 SW8260B 2-Nitropropane <MDL ug/L 125 0711512002 79-46-9 SW8260B - 4-Chlorotoluene < MDL ug/L 125 0711512002 106.43-4 SW8260B 4-Isopropyltoluene < MDL ug/L 125 0711512002 99-87-6 SW8260B 4-Methyl-2-pentanone(MIBK) < MDL ug/L 125 0711512002 108-10-1 SW8260B Acetone < MDL ug/L 125 0711512002 67-64-1 SW8260B Acrylonitrile < MDL ug/L 125 0711512002 107.13-1 SW8260B Ally Chloride < MDL ug/L 125 0711512002 107-05.1 SW8260B Benzene < MDL ug/L 125 0711512002 71-43-2 SW8260B Bromobenzene < MDL ug/L 125 0711512002 108-86-1 SW8260B Bromochloromethane < MDL ug/L 125 0711512002 74-97-5 SW8260B Bromodichloromethane <MDL ug/L 125 0711512002 75-27-4 SW8260B Bromoform <MDL ug/L 125 0711512002 75-25-2 SW8260B Bromomethane <MDL ug/L 125 0711512002 74-83-9 SW8260B Carbon Disulfide <MDL ug/L 125 0711512002 75-15-0 SW8260B Carbon Tetrachloride < MDL ug/L 125 0711512002 56-23.5 SW8260B Chloroacetonitrile < MDL ug/L 125 0711512002 107-14-2 SW8260B Chlorobenzene < MDL ug/L 125 0711512002 108-90-7 SW8260B Chloroethane < MDL ug/L 125 0711512002 75-00-3 SW8260B Chloroform < MDL ug/L 125 0711512002 67-66-3 SW8260B Chloromethane < MDL ug/L 125 0711512002 74-87-3 SW8260B cis-1,2-Dichloroethene < MDL ug/L 125 0711512002 156.59.2 SW8260B cis-1,3-Dichloropropene < MDL ug/L 125 0711512002 10061-01-5 SW8260B Dibromochloromethane < MDL ug/L 125 0711512002 124-48-1 SW8260B Dibromomethane < MDL ug/L 125 0711512002 74-95-3 SW8260B Dichlorodifluoromethane < MDL ug/L 125 0711512002 75-71-8 SW8260B Diethyl Ether <MDL ug/L 125 0711512002 60-29-7 SW8260B Ethyl Methacrylate <MDL ug/L 125 0711512002 97-63-2 SW8260B Euylbenzene < MDL ug/L 125 0711512002 100.41-4 SW8260B Hexachlorobutadiene < MDL ug/L 125 0711512002 87-68-3 SW8260B Hexachloroethane < MDL ug/L 125 0711512002 67.72-1 SW8260B lodomethane < MDL ug/L 125 0711512002 74-88-4 SW8260B Isopropylbenzene < MDL ug/L 125 0711512002 98-82.8 SW8260B meta-Xylene < MDL ug/L 125 0711512002 108-38.3 SW8260B Methacrylonitrile < MDL ug/L 125 0711512002 126-98-7 SW8260B Methyl t-Butyl Ether < MDL ug/L 125 0711512002 1634-04-4 SW8260B Methylacrylate < MDL ug/L 125 0711512002 96-33-3 SW8260B Methylene Chloride < MDL ug/L 125 0711512002 75-09-2 SW8260B Methylmethacrylate < MDL ug/L 125 0711512002 80-62-6 SW8260B n-Butylbenzene <MDL ug/L 125 0711512002 104-51-8 SW8260B n-Propylbenzene <MDL ug/L 125 0711512002 103-65-1 SW8260B Naphthalene <MDL ug/L 125 0711512002 91-20-3 SW8260B Nitrobenzene <MDL ug/L 125 0711512002 98-95-3 SW8260B ortho-Xylene < MDL ug/L 125 0711512002 95-47-6 SW8260B para-Xylene < MDL ug/L 125 0711512002 106.42-3 SW8260B Pentachloroethane < MDL ug/L 125 0711512002 76-01-7 SW8260B Propionitrile < MDL ug/L 125 0711512002 107-12-0 SW8260B sec-Butylbenzene < MDL ug/L 125 0711512002 135-98-8 SW8260B Styrene < MDL ug/L 125 0711512002 100-42-5 SW8260B tert-Butylbenzene < MDL ug/L 125 0711512002 98-06-6 SW8260B Lab Sample Number. ....... AA31 105 page 2 of 3 Volatiles in Ligla Analysis Performed by, RLH Parameter Result Units MDL Date of Analysis CAS N Method Reference Tetrachloroethylene <MDL ug/L 125 0711512002 127-18-4 SW8260B Tetrahydrofuran < MDL ug/L 125 0711512002 109-99-9 SW8260B Toluene <MDL ug/L 126 0711512002 108-88-3 SW8260B trans-1,2-Dichloroethene <MDL uglL 126 0711512002 156-60-5 SW8260B trans-1,3-Dichloropropene <MDL ug/L 125 0711512002 10061-02-6 SW8260B trans-1,4-Dichloro-2-butene < MDL ug/L 125 0711512002 110.57-6 SW8260B Trichloroethene 409.0 ug/L 125 0711512002 79-01-6 SW8260B Trichlorofluoromethane <MDL ug/L 126 0711512002 75-69-4 SW8260B Vinyl Chloride <MDL ug/L 125 0711512002 75-014 SW8260B Lab Sample Number AA31105 page 3 of 3 ADEM *.INTGOMERY LABO&ORY 0 0 1890-A Cong.Wm,Dickinson Dr.,Montgomery,AL 36109 (334y2W2770[phom] (334)-D7-6718[Fax] Analysis Report 0 Date oJThis ReDort... OB/O6/2002 Fund Code: 521 Date of the Original Report.. 08/06/2002 Send Report... Anne F.Cross Lab Sample 1D: AA31106 Source... GW-JBC-02 Location... WEST HUNTSVILLE CLEANERS Collection Date: 07/10/2002 Sample Matrix: WATER Collection Time: 4:54:00 PM Submittal Date: 07/1212002 Sample Collector. AFCross-AnneCross 10:45:0 10:45:0 A Submittal Time: 0 AM Sample Received by: C. D.AMMONS - Date Analvsis Validated... 08/06/2002 by WBB The results on the attached report are from the sample that was received and is referenced above. The sample was analyzed using standard EPA testing procedures and quality analysis protocol Instrument calibration and quality control are within acceptable limits of precision and accuracy. A close review by our Quality Assurance Program certifies that all prescribed test hold limes were met and our strict quality assurance standards were observed. Submitted by: i5a4 7✓rl/'.FlI'1, Quality Assurance Manager ADEM4 Central laboratory has met all Requirements for Certification by EPA Region Four to Analyze Samples for all of the Parameters Required Under the Safe Drinking Water Act Trace Metals Analysis Performed by.... ADC Parameter Result Units MDL Date of Analysis CAS# Method Reference Arsenic, Total <MDL ug/L 10.0 0712912002 7440.38-2 EPA206.2 Cadmium, Total <MDL mg/L 0.003 0712612002 7440-43-9 EPA200.7 Chromium, Total <MDL mg/L 0.015 0712612002 7440-47-3 EPA200.7 Lead, Total 9.40 ug/L 2.00 0712912002 7439.92-1 EPA239.2 Mercury, Total 0.616 ug/L 0.3 0810612002 7439-97-6 EP4245.2 Volatiles in Liquids Analysis Performed by.... RLH Parameter Result Units MDL Date of Analysis CAS# Method Reference 1,1,1,2-Tetrachloroethane < MDL ug/L 5.0 0711612002 630.20.6 SW8260B 1,1,1-Trichloroethane < MDL uglL 5.0 0711612002 71-55-6 SW8260B 1,1,2,2-Tetrachloroethane < MDL ug/L 5.0 0711612002 79-34-5 SW8260B 1,1,2-Trichloroethane < MDL ug/L 5.0 0711612002 79-OD-5 SW8260B 1,1-Dichloroethane < MDL uglL 5.0 0711612002 75-34-3 SW8260D 1,1-Dichloroethene < MDL ug/L 5.0 0711612002 75-35-4 SW8260B 1,1-Dichloropropanone < MDL ug/L 5.0 0711612002 513-88-2 SW8260B 1,1-Dichloropropene < MDL ug/L 5.0 0711612002 563-58-6 SW8260B 1,2,3-Tichlorobenzene < MDL ug/L 5.0 0711612002 87-61-6 SW8260B 1,2,3-Tichloropropane < MDL ug/L 5.0 0711612002 96-18-4 SW8260B 1,2,4-Trichlorobenzene < MDL ug/L 5.0 0711612002 120.82-1 SW8260B 1,2,4-Trimethylbenzene < MDL ug/L 5.0 0711612002 95-63-6 SW8260B 1,2-Dibromo-3-Chloropropane < MDL uglL 5.0 0711612002 96.12.8 SW8260B 1,2-Dibromoethane(EDB) < MDL uglL 5.0 0711612002 106-93-4 SW8260B 1,2-Dichlorobenzene < MDL ug/L 5.0 071I612002 95-50.1 SW8260B 1,2-Dichloroethane <MDL ug/L 5.0 0711WO02 107.06-2 SW8260B 1,2-Dichloropropane <MDL ug/L 5.0 0711612002 78-87-5 SW8260B 1,3,5-Trimethylbenzene < MDL ug/L 5.0 0711612002 108-67-8 SW8260B 1,3-Dichlorobenzene < MDL ug/L 5.0 0711612002 541-73-1 SW8260B 1,3-Dichloropropane < MDL ug/L 5.0 0711612002 142-28-9 SW8260B Lab Sample Number.............................. AA31106 page 1 of 3 volutiles in Ligb,; Analysis Perfwnred 1114 RLH Parameter Result Units MDL Date of Analysis CAS# Method Reference 1,4-Dichlorobenzene <MDL ug/L 5.0 0711612002 106-46-7 SW8260B 1-Chlorobutane <MDL ug/L 5.0 0711612002 109-69-3 SW8260B 2,2-Dichloropropane < MDL ug/L 5.0 0711612002 590-20-7 SW8260B 2-Butanone < MDL ug/L 5.0 0711612002 78-93-3 SW8260B 2-Chlorotoluene < MDL ug/L 5.0 0711612002 95-49-8 SW82608 2-Hexanone < MDL ug/L 5.0 0711612002 591-78-6 SW8260B 2-Nitropropane < MDL ug/L 5.0 0711612002 79-46-9 SW8260B 4-Chlorotoluene < MDL ug/L 5.0 0711612002 106-43-4 SW8260B 4-Isopropyltoluene < MDL ug/L 5.0 0711612002 99.87-6 SW8260B 4-Methyl-2-pentanone(MIBK) < MDL ug/L 5.0 0711612002 108-10-1 SW8260B Acetone < MDL ug/L 10.0 0711612002 67-64-1 SW8260B Acrylonitrile < MDL ug/L 5.0 0711612002 107-13-1 SW8260B Ally Chloride < MDL ug/L 5.0 0711612002 107-05-1 SW8260B Benzene < MDL ug/L 6.0 0711612002 71-43-2 STY8260B Bromobenzene < MDL ug/L 5.0 0711612002 108-86-1 SW8260B Bromochloromethane < MDL ug/L 5.0 0711612002 74-97-5 SW8260B Bromodichloromethane < MDL ug/L 5.0 0711612002 75-27-4 SW8260B Bromoform < MDL ug/L 5.0 0711612002 75-25-2 SW8260B Bromomethane <MDL ug/L 5.0 0711612002 74-83-9 SW8260B Carbon Disulfide < MDL ug/L 5.0 0711612002 75-15-0 SW8260B Carbon Tetrachloride < MDL ug/L 5.0 0711612002 56-23-5 SW8260B Chloroacetonitrile <MDL ug/L 5.0 0711612002 107-14-2 SW8260B Chlorobenzene <MDL ug/L 5.0 0711612002 108-90-7 SW8260B Chloroethane < MDL ug/L 5.0 0711612002 75-00-3 SW8260B Chloroform < MDL ug/L 5.0 0711612002 67-66-3 SW8260B Chloromethane <MDL ug/L 5.0 0711612002 74.87-3 SW8260B cis-1,2-Dichloroethene < MDL ug/L 5.0 0711612002 156.59.2 SW8260B cis-1,3-Dichloropropene <MDL ug/L 5.0 0711612002 10061-01-5 SW8260B Dibromochloromethane <MDL ug/L 5.0 0711612002 124-48-1 SW8260B Dibromomethane <MDL ug/L 5.0 0711612002 74-95.3 SW8260B Dichlorodifluoromethane <MDL ug/L 5.0 0711612002 75-71-8 SW8260B Diethyl Ether <MDL ug/L 5.0 0711612002 60-29-7 SW8260B Ethyl Methacrylate <MDL ug/L 5.0 0711612002 97-63-2 SW8260B Etylbenzene <MDL ug/L 5.0 0711612002 100-41-4 SW8260B Hexachlorobutadiene <MDL ug/L 5.0 0711612002 87-68-3 SW8260B Hexachloroethane <MDL ug/L 5.0 0711612002 67-72-1 SW8260B lodomethane <MDL ug/L 5.0 0711612002 74-88-4 SW8260B Isopropylbenzene <MDL ug/L 5.0 0711612002 9"2-8 SW8260B meta-Xylene <MDL ug/L 5.0 0711612002 108-38-3 SW8260B Methacrylonitrile <MDL ug/L 5.0 0711612002 126-98-7 SW8260B Methyl t-Butyl Ether < MDL ug/L 5.0 0711612002 1634-04-4 SW8260B Methylacrylate < MDL ug/L 5.0 0711612002 96-33-3 SW8260B Methylene Chloride < MDL ug/L 5.0 0711612002 75-09-2 SW8260B Methylmethacrylate < MDL ug/L 5.0 0711612002 80-62-6 SW8260B n-Butylbenzene < MDL ug/L 5.0 0711612002 104-51-8 SW8260B n-Propylbenzene < MDL ug/L 5.0 0711612002 103-65-1 SW8260B Naphthalene < MDL ug/L 5.0 0711612002 91.20.3 SW8260B Nitrobenzene < MDL ug/L 5.0 0711612002 98-95-3 SW8260B ortho-Xylene < MDL ug/L 5.0 0711612002 95-47-6 SW8260B para-Xylene < MDL ug/L 5.0 0711612002 106-42-3 SW8260B Pentachloroethane < MDL ug/L 5.0 0711612002 76-01-7 SW8260B Propionitrile < MDL ug/L 5.0 0711612002 107-12-0 SW8260B sec-Butylbenzene < MDL ug/L 5.0 0711612002 135-98-8 SW8260B Styrene < MDL ug/L 5.0 0711612002 100-42-5 SW8260B tert-Butylbenzene < MDL ug/L 5.0 0711612002 98-06-6 SW8260B Lab Sample Number.............................. AA31106 page 2 of 3 VOlatiles in Liq* Analysis Performed by RLN Parameter Result Units MDL Date of Analysis CAS N Method Reference Tetrachloroethylene <MDL uglL 5.0 0711612002 127.18-4 SW8260B Tetrahydrofuran <MDL uglL 5.0 0711612002 109-99-9 SW8260B Toluene <MDL uglL 5.0 0711612002 108.883 SW8260B trans-1,2-Dichloroethene <MDL uglL 5.0 0711612002 156-60.5 SW8260B trans-1,3-Dichloropropene < MDL uglL 5.0 0711612002 10061.02-6 SW8260B trans-1,4-Dichloro-2-butene <MDL ug/L 6.0 0711612002 110.57-6 SW8260B Trichloroethene <MDL uglL 5.0 0711612002 79.01-6 SW8260B Trichlorotluoromethane <MDL uglL 5.0 0711612002 75-69.4 SW8260B Vinyl Chloride <MDL uglL 5.0 0711612002 75.01-4 SW82600 Lab Sample Number.............................. AA31106 page 3 of 3 0 ADEM IWNTGOMERY LABOI&TORY 1890-A Cong.Wm. Dickinson Dr.,Montgomery.AL 36109 t �'7 i3341-2614277010homl (3?4)-277-671AIFaxI • .1 " Analysis Report ** Date of This Report... 08/09/2002 Fund Code: 521 Date of the Original Report... 0 810 9/2 0 0 2 Send Report... Anne F. Cross Lab Sample ID: AA31107 .Source... GWJBC-03 02 Location... WEST HUNTSVILLE CLEANERS CollecCollection Date: 5:45:00 PM Sample Matrix: WATER Submittal Time: 07/100 PM Sample Collector., AFCross-AnneCross Submittal Date: 10:45:00 A Submittal Time: 10:45:00 AM Sample Received by: C. D.AMMONS Date Analysis Validated... 08/08/2002 by WBB The results on the attached report are front the santple that was received and is referenced above. The sample was analyzed using standard EPA testing procedures and quality analysis protocol Instrument calibration and quality control are within acceptable/buts of precision and accuracy. A close review by our Quality Assurance Program certyiiesthat al(prescribed test hokl time..,were met and our strict quality assurance standards were observed. Subminedby: Y?,Y,J Rj=CE,1n, Quality Assurance Manager ADEM's Central laboratory has met all Requirements for Certification by EPA Region Four to Analyze Samples for all of the Parameters Required Under the Safe Drinking Water Act. Trace Metals Analysis Performed by.... ADC Parameter Result Units MDL Date ofAnalvsis CAS# Method Re erence Arsenic, Total < MDL uglL 10.0 07/292002 7440-38-2 EPA206.2 Cadmium, Total < MDL mg/L 0.003 07262002 7440-43-9 EPA200.7 Chromium, Total 0.016 mg/L 0.015 07262002 7440.47.3 EPA200.7 Lead, Total 2.39 ug/L 2.00 07292002 7439-92-1 EPA239.2 Mercury, Total <MDL ug(L 0.3 081082002 7439.97.6 EPA245.2 Volatiles in Liquids Analysis Performed by.... RLH Parameter Result Units MDL Date of Anal sis CAS# Method Re erence 1,1,1,2-Tetrachloroethane <MDL uglL 5.0 071152002 630.20.6 SW8260B 1,1,1-Trichloroethane <MDL ug/L 6.0 071152002 71-56-6 SW8260B 1,1,2,2-Tetrachloroethane < MDL ug/L 5.0 071152002 79-34-5 SW8260B 14,2-Trichloroethane < MDL ug/L 6.0 0711512002 79.00.5 SW8260B 1,1-Dichloroethane < MDL uglL 5.0 071152002 75-34-3 SW8260B 1,1-Dichloroethene < MDL ug/L 5.0 071152002 75-35-4 SW8260B 1,1-Dichloropropanone < MDL ug/L 5.0 071152002 513-88-2 SW8260B 1,1-Dichloropropene < MDL ug/L 5.0 071152002 563.58.6 SW8260B 1,2,3-Trichlorobenzene < MDL ug/L 5.0 071152002 87-61-6 SW8260B 1,2,3-Tichloropropane < MDL ug/L 5.0 071152002 96-18-4 SW8260B 1,2,4-Trichlorobenzene < MDL ug/L 5.0 071152002 120-82-1 SW8260B 1,2,4-Trimethylbenzene < MDL ug/L 5.0 071152002 95-63.6 SW8260B 1,2-Dibromo-3-Chloropropane < MDL uglL 5.0 0711512002 96.12.8 SW8260B '1,2-Dibromoethane(EDB) < MDL uglL 5.0 0711512002 106-93-4 SW8260B 1,2-Dichlorobenzene <MDL uglL 5.0 0711512002 95-50-1 SW8260B 1,2-Dichloroethane <MDL uglL 5.0 0711512002 107-06.2 SW8260B 1,2-Dichloropropane <MDL ug/L 6.0 0711512002 78-87-5 SW8260B 1,3,5-Trimethylbenzene < MDL ug/L 6.0 071I M002 108-67.8 SW8260B 1,3-Dichlorobenzene <MDL ug/L 5.0 0711512002 541.73.1 SW8260B, 1,3-Dichloropropane <MDL ug/L 5.0 0711512002 142-28-9 SW8260B Lab Sample Number.............................. AA31107 Page 1 of Volatiles in Li(, -A Anah'sis Performed l RLH Parameter Result Units MDL Date a rahsis CAS# Method Reference 1,4-Dichlorobenzene < MDL ug/L 5.0 0711512002 106-46-7 SW8260B 1-Chlorobutane < MDL ug/L 5.0 0711512002 109-69-3 ,SIV8260B 2,2-Dichloropropane < MDL ug/L 5.0 0711512002 590-20-7 SIV82608 2-Butanone < MDL ug/L 5.0 0711512002 78-93-3 SLV82608 2-Chlorotoluene < MDL ug/L 5.0 0711512002 95-49-8 SW8260B 2-Hexanone < MDL ug/L 5.0 0711512002 591-7&6 SIV8260B 2-Nitropropane < MDL ug/L 5.0 0711512002 79-46-9 SW8260B 4-Chlorotoluene < MDL ug/L 5.0 0711512002 106.43-4 SIV8260B 4-Isopropyltoluene <MDL ug/L 5.0 0711512002 99-87-6 SIV8260B 4-Methyl-2-pentanone(MIBK) < MDL ug/L 5.0 0711512002 108-10-1 SIV8260B Acetone 230.0 ug/L 10.0 0711512002 67-64-1 SW8260B Acrylonitrile < MDL ug/L 5.0 0711512002 107-13-1 SW8260B Ally Chloride <MDL ug/L 5.0 0711512002 107-05-1 SW8260B Benzene <MDL ug/L 5.0 0711512002 71-43-2 SW8260B Bromobenzene < MDL ug/L 5.0 0711512002 108.86-1 SW8260B Bromochloromethane < MDL ug/L 5.0 0711512002 74-97.5 SIV8260B Bromodichloromethane <MDL ug/L 5.0 0711512002 75-27.4 SVV8260B Bromoform < MDL ug/L 5.0 0711512002 75-25-2 SW8260B Bromomethane < MDL ug/L 5.0 0711512002 74-83-9 SW8260B Carbon Disulfide < MDL ug/L 5.0 0711512002 75.15-0 SW8260B Carbon Tetrachloride <MDL ug/L 5.0 0711512002 56-23-5 SIV8260B Chloroacetonitrile <MDL ug/L 5.0 0711512002 107-14-2 SIV8260B Chlorobenzene < MDL ug/L 5.0 071152002 108-90-7 SIV8260B Chloroethane < MDL ug/L 5.0 0711512002 75-00.3 SW8260B Chloroform < MDL ug/L 5.0 071152002 67-66-3 ,SIV8260B Chloromethane <MDL ug/L 5.0 0711512002 74.87-3 SW8260B cis-1,2-Dichloroethene < MDL ug/L 5.0 0711512002 156-59.2 SW8260B cis-1,3-Dichloropropene < MDL ug/L 6.0 0711512002 10061-01-5 SW8260B Dibromochloromethane < MDL ug/L 5.0 0711512002 124-48-1 SIVS260B Dibromomethane <MDL ug/L 5.0 0711512002 74-95-3 SW8260B Dichlorodifluoromethane <MDL ug/L 5.0 0711512002 75-71.8 SW8260B Diethyl Ether < MDL ug/L 5.0 0711512002 60-29-7 SW8260B Ethyl Methacrylate < MDL ug/L 5.0 0711512002 97-63-2 SW8260B Ethylbenzene < MDL ug/L 5.0 0711512002 100-41-4 SW8260B Hexachlorobutadiene < MDL ug/L 5.0 0711512002 87-68-3 SIV8260B Hexachloroethane <MDL ug/L 5.0 071152002 67-72-1 SW8260B lodomethane <MDL ug/L 5.0 0711512002 74.88.4 SIV8260B Isopropylbenzene <MDL ug/L 5.0 0711512002 98.82.8 SW8260B meta-Xylene < MDL ug/L 5.0 0711512002 108-38-3 SIV8260B Methacrylonitrile < MDL ug/L 5.0 0711512002 126-98-7 SW8260B Methyl t-Butyl Ether < MDL ug/L 5.0 0711512002 1634-04-4 SW8260B Methylacrylate <MDL ug/L 5.0 0711512002 96-33-3 SW8260B Methylene Chloride <MDL ug/L 5.0 0711512002 75.09.2 SW8260B Methylmethacrylate < MDL ug/L 5.0 0711512002 80-62-6 SW8260B n-Butylbenzene < MDL ug/L 5.0 071152002 104-51-8 SW8260B n-Propylbenzene < MDL ug/L 5.0 0711512002 103-65-1 SW8260B Naphthalene < MDL ug/L 5.0 0711512002 91-20.3 SW8260B Nitrobenzene < MDL ug/L 5.0 0711512002 98.95.3 SW8260B ottho-Xylene < MDL ug/L 5.0 0711512002 95-47-6 SW8260B para-Xylene <MDL ug/L 5.0 0711512002 106-42-3 SIV8260B Pentachloroethane <MDL ug/L 5.0 0711512002 76.01-7 SW82608 Propionitrile <MDL ug/L 5.0 071152002 107.12-0 SW8260B sec-Butylbenzene <MDL ug/L 5.0 0711512002 135.98-8 SW8260B Styrene < MDL ug/L 5.0 0711512002 100-42-5 SIV8260B tert-Butylbenzene < MDL ug/L 5.0 0711512002 98-06-6 SW8260B Lab Sample Number.............................. AA31107 page 2 of 3 Volatiles in Liquie Analysis Perfn-med by...0 Rut Parameter Result Units MDL Date oiAnalysfs CAS N Method Reference Tetrachloroethylene < MDL ug/L 5.0 0711512002 127-18-4 SW8260B Tetrahydroluran < MDL uglL 5.0 0711512002 109-99.9 SW8260B Toluene <MDL ug/L 5.0 0711512002 108.88-3 SW8260B trans-1,2-Dichloroethene < MDL ug/L 5.0 0711512002 156.60-5 SW8260B trans-1,3-Dichloropropene < MDL ug/L 5.0 071152002 10061-02.6 SW8260B trans-1,4-Dichloro-2-butene < MDL ug/L 5.0 0711512002 110.57.6 SW8260B Trichloroethene <MDL ug/L 5.0 071152002 79.01-6 SW8260B Trichlorolluoromethane < MDL ug/L 5.0 0711512002 75-69.4 SW8260B Vinyl Chloride < MDL ug/L 5.0 071152002 75-01.4 SW8260B Lab Sample Number.............................. AA31107 Page 3 of 3 ADEM M&TGOMERY LABORAORY 0 1890-A Cong.Wm. Dickinson Dr..Montgomery. AL 36109 (334)-36027701phon<] (334)-277-6718(Fan] A' �,' y Analysis Report !; � Date of T/pis Report... OB/09/2002 Fund Code: 521 Date of the Origin(Report 08/09/2002 Send Report.. Anne F.Cross Lob Sample ID: AA31108 Source... GW-JBC-D Location... WEST HUNTSVILLE CLEANERS Collection Date: 07/10/2002 Sample Matrix: WATER Collection Time: 2:15:00 PM Sample Collector: AFCross-AnneCross Submittal Date: 07/12/2002 Submittal Time: 10:45:00 AM Sample.Received by: C. D.AMMONS Date Analvsis Validated... 08/08/2002 by WBB The results on the attached report are from tine sample that was received and is referenced above. The sample was analyzed using standard EPA tesling procedures and quality analysis protocol. Instrument calibration and quality control are within acceptable limits of precision and accuracy. A close review by our Quality Assurance Program certifies that all prescribed test hold does were met and our strict quality assurance standards were observed. Submitted by: R(;U84zC&ji'u• Quality Assurance Manager ADEM's Central Laboratory has met all Requirements for Certification by EPA Region Four to Analyze Samples for all of the Parameters Required Under the Safe Drinking Water Act. Trace Metals Analvsis Performed by.... ADC _Parameter Result Units MDL Date of Analysis CAS# Method Reference Arsenic, Total <MDL uglL 10.0 071292002 7440-38-2 EPA206.2 Cadmium, Total <MDL mg/L 0.003 0712612002 7440.43-9 EPA200.7 Chromium, Total <MDL mg/L 0.015 07126f2002 7440.47.3 EPA200.7 Lead, Total <MDL ug/L 2.00 072912002 7439-92-1 EPA239.2 Mercury, Total <MDL uglL 0.3 081082002 7439-97-6 EPA245.2 VOlatiles in Liquids Analysis Performed by.... RLH _Parameter Result Units MDL Date of Analysis CAS# Method Reference 1,1,1,2-Tetrachloroethane <MDL ug/L 5.0 071162002 630-20-6 SW8260B 1,1,1-Trichloroethane <MDL ug/L 5.0 0711612002 71.55-6 SW8260B 1,1,2,2-Tetrachloroethane <MDL ug/L 5.0 0711612002 79.34.5 SW8260B 1,1,2-Trichloroethane <MDL uglL 6.0 0711612002 79.00-6 SW8260D 1,1-Dichloroethane <MDL uglL 5.0 0711612002 75-34.3 SW8260B 1,1-Dichloroethene <MDL uglL 5.0 07116f2002 75.354 SW8260D 1,1-Dichloropropanone <MDL ug/L 5.0 071162002 513-88-2 SW8260B 1,1-Dichloropropene <MDL ug/L 5.0 071162002 563.58.6 SW8260B 1,2,3-Trichlorobenzene <MDL ug/L 5.0 0711612002 87-61-6 SW8260B 1,2,3-Trcchloropropane < MDL uglL 5.0 071162002 96-18-4 SW8260B 1,2,4.Trichlorobenzene < MDL uglL 5.0 0711612002 120-82-1 SW8260B 1,2,4-Trimethylbenzene < MDL uglL 5.0 071162002 95.63.6 SW8260D 1,2-Dibromo-3-Chloropropane < MDL uglL 5.0 07116f1002 96-12.8 SW8260B 1,2-Dibromoethane(EDB) < MDL ug/L 5.0 07116/2002 106-93-4 SW8260B 1,2-Dichlorobenzene < MDL ug/L 5.0 0711612002 95.5D-1 SW8260B 1,2.Dichloroethane <MDL ug/L 5.0 0711612002 107.06.2 SW8260B 1,2-Dichloropropane <MDL ug/L 5.0 0711612002 78.87-5 SW8260B 1,3,5-7'rimethylbenzene <MDL ug/L 5.0 071162002 108.67-8 SW8260B 1,3-Dichlorobenzene _ <MDL ug/L 5.0 0711612002 541.73-1 SW8260B _ 1,3-Dichloropropane <MDL ug/L 5.0 071162002 142.28-9 SW8260B Lab Sample Number.............................. AA31108 Page 1 of 3 Volarile.s in Liyuiv AnalY_d.r Performed bv_.- RLH Parameter Result Units ,MDL Date of Analysis CAS# Method Reference 1,4-Dichlorobenzene < MDL ug/L 5.0 0711612002 106-46-7 SW8260B 1-Chlorobutane < MDL ug/L 5.0 0711612002 109-69-3 SIV8260B 2,2-Dichloropropane < MDL ug/L 5.0 0711612002 590.20.7 SW8260B 2-Butanone < MDL ug/L 5.0 0711612002 78-93-3 SW8260B 2-Chlorotoluene < MDL ug/L 5.0 0711612002 95-49-8 SW8260B 2-Hexanone < MDL ug/L 5.0 0711612002 591-78-6 SIV8260B 2-Nitropropane < MDL ug/L 5.0 0711612002 79-46-9 SIV8260B 4-Chlorotoluene < MDL ug/L 5.0 0711612002 106-43-4 SIV8260B 4-lsopropyltoiuene < MDL ug/L 5.0 0711612002 99-87-6 SW8260B 4-Methyl-2-pentanone(MIBK) < MDL ug/L 5.0 0711612002 108.10.1 SIV8260B Acetone < MDL ug/L 10.0 0711612002 67-64-1 SW8260B Acrylonitrile < MDL ug/L 5.0 0711612002 107-13.1 SVV8260B Ally Chloride < MDL ug/L 5.0 0711612002 107-05-1 SW8260B Benzene < MDL ug/L 5.0 0711612002 7143-2 SIV8260B Bromobenzene < MDL ug/L 5.0 0711612002 108-86-1 SIV8260B Bromochloromethane < MDL ug/L 5.0 0711612002 74-97-5 SIV8260B Bromodichloromethane < MDL ug/L 5.0 0711612002 75-27-4 S1V8260B Bromoform < MDL ug/L 5.0 0711612002 75-25-2 SW8260B Bromomethane < MDL ug/L 5.0 0711612002 74-83-9 SW8260B Carbon Disulfide < MDL ug/L 5.0 0711612002 75-15.0 SW8260B Carbon Tetrachloride < MDL ug/L 5.0 0711612002 56-23-5 SIV8260B Chloroacetonitrile < MDL ug/L 5.0 0711612002 107-14-2 SW8260B Chlorobenzene < MDL ug/L 5.0 0711612002 108-90-7 SIV8260B Chloroethane < MDL ug/L 5.0 0711612002 75-00-3 SW8260B Chloroform < MDL ug/L 5.0 0711612002 67-66-3 SIVS260B Chloromethane < MDL ug/L 5.0 0711612002 74-87-3 SW8260B cis-1,2-Dichloroethene 35.8 ug/L 5.0 0711612002 156-59-2 SW8260B cis-1,3-Dichloropropene < MDL ug/L 5.0 0711612002 10061-01.5 SW8260B Dibromochloromethane < MDL ug/L 5.0 0711612002 124-48-1 SW8260B Dibromomethane <MDL ug/L 5.0 0711612002 74-95-3 SW8260B Dichlorodifluoromethane < MDL ug/L 5.0 0711612002 75.71.8 SW8260B Diethyl Ether < MDL ug/L 5.0 0711612002 60-29-7 SW8260B Ethyl Methacrylate < MDL ug/L 5.0 0711612002 97.63.2 SW8260B Ethylbenzene < MDL ug/L 5.0 0711612002 100-41-4 SW8260B Hexachlorobutadiene < MDL ug/L 5.0 0711612002 87-68-3 SW8260B Hexachloroethane < MDL ug/L 5.0 0711612002 67-72-1 SW8260B lodomethane < MDL ug/L 5.0 0711612002 74.88.4 SIVS260B Isopropylbenzene <MDL ug/L 5.0 0711612002 98.82.8 SW8260B meta-Xylene < MDL ug/L 5.0 0711612002 108-38-3 SW8260B Methacrylonitrile < MDL ug/L 5.0 0711612002 126-98-7 SW8260B Methyl t-Butyl Ether < MDL ug/L 5.0 0711612002 1634.04-4 SW8260B Methylacrylate < MDL ug/L 5.0 0711612002 96-33-3 SW8260B Methylene Chloride < MDL ug/L 5.0 0711612002 75-09-2 SW8260B Methylmethacrylate < MDL ug/L 5.0 0711612002 80-62-6 SW8260B n-Butylbenzene < MDL ug/L 5.0 0711612002 104.51-8 SW8260B n-Propylbenzene < MDL ug/L 5.0 0711612002 103-65-1 SW8260B Naphthalene < MDL ug/L 5.0 0711612002 91-20-3 SW8260B Nitrobenzene < MDL ug/L 5.0 0711612002 98-95-3 SW8260B .ortho-Xylene < MDL ug/L 5.0 0711612002 95-47-6 SW8260B para-Xylene < MDL ug/L 5.0 0711612002 106-42.3 SW8260B Pentachloroethane <MDL ug/L 5.0 0711612002 76-01.7 SW8260B Propionitrile <MDL ug/L 5.0 0711612002 107-12-0 SW8260B sec-Butylbenzene <MDL ug/L 5.0 0711612002 135-98.8 SW8260B Styrene < MDL ug/L 5.0 0711612002 100.42-5 SW8260B _ tert-Butylbenzene < MDL ug/L 5.0 0711612002 98-06-6 SW8260B- Lab Sample Number.............................. AA31108 Page 2 of 3 Volatiles in Liqui[• Analysis Performed by... RLH Parameter Result Units MDL Dare o Ana ysis CAS# Method Reference Tetrachloroethylene < MDL ug/L 5.0 0711612002 127-18-4 SW8260B Tetrahydroturan <MDL ug/L 5.0 0711612002 109-99-9 SW8260B Toluene < MDL ug/L 5.0 0711612002 108.88.3 SW82608 trans-1,2-Dichloroethene < MDL ug/L 5.0 0711612002 156-60-5 SW8260B trans-1,3-Dichloropropene < MDL ug/L 5.0 0711612002 10061-02-6 SW8260B trans-1,4-Dichloro-2-butene <MDL ug/L 5.0 0711612002 110.57.6 SW8260B Trichloroethene 343.25 ug/L 5.0 0711612002 79.01.6 SW8260B Trichlorotluoromethane < MDL ug/L 5.0 0711612002 75.69.4 SW8260B Vinyl Chloride <MDL ug/L 5.0 0711612002 75.01.4 SW8260B Lab Sample Number.............................. AA31108 page 3 of 3 ADEM MWTGOMERY LABORAORY 0 1890-A Con,,. Wm. Dickinson Dr.,Montgomery. AL 36109 (3341-260-2770(,] nd 0141.177-671%IFaa1 Analysis Report * Date of This Report... OB/09/2002 Fund Code: 521 Date of the Orieitnal Report 0 810 9/2 0 0 2 Send Report... Anne F.Cross Lab Sample ID: AA31116 Source... PWS-WHC/JBC-UMW Location... WEST HUNTSVILLE CLEANERS Collection Date: 07/10/2002 Sample Matrix: WATER Collection Time: 10:24:00 AM Submittal Date: 07/12/2002 Sample Collector: AFCross-AnneCross Submittal Time: 10:45:00 AM Sample Received by: C. D. AMMONS Date Analvsis Validated... 08/08/2002 by WBB The results on the attached report are from the sample that was received and is referenced above. The sample was analyzed using standard EPA testing procedures and quality analysis protocol Instrument calibration and quality control are within acceptable limits of precision and accuracy. A close review by our Quality Assurance Program certifies that aB prescribed test hold times were met and our strict quality assurance standards were observed. Submitted by: gl( ,Flzm. Quality Assurance Manager ADEM's Central laboratory has met all Requirements for Certification by EPA Region Four to Analyse Samples for all of the Parameters Required Under the Safe Drinking Water Act Trace Metals Anahsis Performed by... ADC Parameter Result Units MDL Date ofAnalysis CAS# Method Re erence Arsenic, Total <MDL ug/L 10.0 071292002 7440.38-2 EPA206.2 Cadmium, Total <MDL mg/L 0.003 07262002 7440.43-9 EPA200.7 Chromium, Total <MDL mg/L 0.015 0712612002 7440-47-3 EPA200.7 Lead, Total <MDL ug/L 2.00 0712912002 7439.92-1 EPA239.2 Mercury, Total <MDL ug/L 0.3 081082002 7439.97.6 EPA245.2 Volatiles in Liquids Analvsis Performed by.... RLH Parameter Result Units MDL Date ofAnal sis CAS# Method Reference 1,1,1,2-Tetrachloroethane < MDL ug/L 5.0 071162002 630-20-6 SW8260B 1,1,1-Trichloroethane < MDL ug/L 5.0 07116)2002 71-55-6 SW8260B 1,1,2,2-Tetrachloroethane < MDL ug/L 5.0 0711612002 79-34.5 SW8260B 1,1,2-Trichloroethane < MDL ug/L 5.0 071162002 79-00.5 SW8260B 1,1-Dichloroethane < MDL ug/L 5.0 071162002 75-34.3 SW8260B 1,1-Dichloroethene < MDL ug/L 5.0 071162002 75.35-4 SW8260B 1,1-Dichloropropanone < MDL ug/L 6.0 071162002 613-88-2 SW8260B 1,1-Dichloropropene < MDL ug/L 5.0 '071162002 563-58-6 SW8260B 1,2,3-Trichlorobenzene < MDL ug/L 5.0 0711612002 87.61.6 SW8260B 1,2,3-Trichloropropane < MDL ug/L 5.0 071162002 96.18.4 SW8260B 1,2,4-Tichlorobenzene < MDL ug/L 5.0 0711612002 120.82.1 SW8260B 1,2,4-Trimethylbenzene < MDL ug/L 5.0 071162002 95-63.6 SW8260B 1,2-Dibromo-3-Chloropropane < MDL uglL 5.0 071162002 96-12-8 SW8260B 1,2-Dibromoethane(EDB) <MDL ug/L 5.0 0711612002 106.93-4 SW8260B 1,2-Dichlorobenzene <MDL ug/L 5.0 071162062 95-50-1 SW8260B 1,2-Dichloroethane < MDL ug/L 5.0 0711612002 107-06.2 SW8260B 1,2-Dichloropropane < MDL ug/L 5.0 0711612002 78.87-5 SW8260B 1,3,5-Trimethylbenzene < MDL ug/L 5.0 071162002 108.67-8 SW8260B 1,3-Dichlorobenzene < MDL ug/L 5.0 0711612002 541.73.1 SW8260B 1,3-Dichloropropane <MDL uglL 5.0 0711612002 142-28.9 SW8260B Lab Sample Number.............................. AA31 1 16 page 1 of 3 Volatiles in Liqui• Anahuis Perinnued br...• RLH Parameter Result Units MDL Date of Analysis CAS# bletb d Be1•r me 1,4-Dichlorobenzene < MDL ug/L 5.0 0711612002 106-46-7 SIV82608 1-Chlorobutane <MDL ug/L 5.0 0711612002 109.69-3 SW8260B 2,2-Dichloropropane <MDL ug/L 5.0 0711612002 590-20.7 SIV8260B 2-Butanone < MDL ug/L 5.0 0711612002 78-93.3 .SW8260B 2-Chlorotoluene < MDL ug/L 5.0 071/62002 95-49-8 SW8260B 2-Hexanone < MDL ug/L 5.0 0711612002 591.78-6 SIV8260B 2-Nitropropane <MDL ug/L 5.0 0711612002 79.46-9 SIV8260B 4-Chlorotoluene <MDL ug/L 5.0 0711612002 106.43-4 SM26011 4-Isopropyltoluene <MDL ug/L 5.0 0711612002 99-87.6 SW8260B 4-Methyl-2-pentanone(MIBK) < MDL ug/L 5.0 0711612002 108.10.1 SIV8260B Acetone < MDL ug/L 10.0 0711612002 67-64.1 SW8260B Acrylonitrile <MDL ug/L 5.0 071162002 107.13-1 SIV8260B Ally Chloride <MDL ug/L 5.0 0711612002 107.05.1 SW8260B Benzene < MDL ug/L 5.0 0711612002 71-43.2 SW8260B Bromobenzene < MDL ug/L 5.0 0711612002 108.86-1 SW8260B Bromochloromethane < MDL ug/L 5.0 0711612002 74-97-5 SW8260B Bromodichloromethane <MDL ug/L 5.0 0711612002 75-27.4 SW8260B Bromoform <MDL ug/L 6.0 0711612002 75.25-2 SW8260B Bromomethane < MDL ug/L 5.0 0711612002 74.83-9 SIV8260B Carbon Disulfide < MDL ug/L 5.0 0711612002 75-15-0 SW8260B Carbon Tetrachloride < MDL ug/L 5.0 0711612002 56.23-5 SW8260B Chloroacetonitrile <MDL ug/L 5.0 071162002 107-14-2 STY8260B Chlorobenzene <MDL ug/L 5.0 0711612002 108-90-7 SW8260B Chloroethane < MDL ug/L 5.0 0711612002 75.00-3 SW8260B Chloroform < MDL ug/L 5.0 0711612002 67.66-3 SIV8260B Chloromethane < MDL ug/L 5.0 071162002 74-87.3 SW8260B cis-1,2-Dichloroethene <MDL ug/L 5.0 071162002 156-59.2 SW8260B cis-1,3-Dichloropropene < MDL ug/L 5.0 0711612002 10061.01-5 SW8260B Dibromochloromethane < MDL ug/L 5.0 0711612002 124-48-1 SW8260B Dibromomethane < MDL ug/L 5.0 071162002 74.95-3 SW8260B Dichlorodifluoromethane <MDL uglL 5.0 0711612002 75-71-8 STY8260B Diethyl Ether <MDL ug/L 5.0 0711612002 60-29.7 SW8260B Ethyl Methacrylate <MDL ug/L 5.0 0711612002 97-63.2 SW8260B Etylbenzene < MDL ug/L 5.0 071162002 100.41-4 SW8260B Hexachlorobutadiene <MDL ug/L 5.0 071162002 87.68-3 SIV8260B Hexachloroethane <MDL ug/L 5.0 071162002 67.72.1 SW8260B lodomethane <MDL ug/L 5.0 0711612002 74-88.4 SW8260B Isopropylbenzene < MDL ug/L 5.0 0711612002 98-82.8 SW8260B meta-Xylene < MDL ug/L 5.0 0711612002 108-38-3 SW8260B Methacrylonitrile < MDL ug/L 5.0 071162002 126-98.7 SW8260B Methyl t-Butyl Ether <MDL ug/L 5.0 0711612002 1634.04.4 SW8260B Methylacrylate <MDL ug/L 5.0 071162002 96-33.3 SW8260B Methylene Chloride < MDL ug/L 5.0 071162002 75-09.2 SW8260B Methylmethacrylate < MDL ug/L 5.0 071162002 80-62-6 SW8260B n-Butylbenzene < MDL ug/L 5.0 0711612002 104.51-8 SW8260B n-Propylbenzene <MDL ug/L 5.0 071162002 103-65.1 SW8260B Naphthalene <MDL ug/L 5.0 071162002 91-20-3 SW8260B Nitrobenzene <MDL ug/L 5.0 071162002 98-9S-3 SW8260B ortho-Xylene < MDL ug/L 5.0 071162002 95.47-6 SW8260B para-Xylene < MDL ug/L 5.0 0711612002 106-42-3 SW8260B Pentachloroethane <MDL ug/L 5.0 071162002 76-01.7 SW8260B Propionitrile <MDL ug/L 6.0 0711612002 107-12-0 SW8260B sec-Butylbenzene <MDL ug/L 5.0 071162002 135.98-8 SW8260B Styrene < MDL ug/L 5.0 0711612002 100-42.5 SW8260B tart-Butylbenzene < MDL ug/L 5.0 0711612002 98-06.6 SW8260B Lab Sample Number.............................. AA31 1 16 Page 2 of 3 Volatiles in Liqui! Analysis Perfi rmer/l;r... RLH Parameter Result Units MDL Dale o Ana sis CAS# 'h/erlrod Refer nce Tetrachloroethylene < MDL ug/L 5.0 0711612002 127.18-4 SW8260B Tetrahydrofuran <MDL ug/L 5.0 0711612002 109.99.9 SVY8260B Toluene <MDL ug/L 5.0 0711612002 108-883 SW8260B trans-1,2-Dichloroethene < MDL ug/L 5.0 0711612002 156-60-5 ,SW8260B trans-1,3-Dichloropropene < MDL ug/L 5.0 0711612002 10061-02.6 SW8260B trans-1,4-Dichloro-2-butene <MDL ug/L 5.0 0711612002 110.57-6 SW8260B Trichloroethene <MDL ug/L 5.0 0711612002 79-01-6 SW8260B Trichlorofluoromethane <MDL ug/L 5.0 0711612002 75.69.4 SIV8260B Vinyl Chloride < MDL ug/L 5.0 0711612002 75-01-4 SW8260B Lab Sample Number.............................. AA31116 page 3 of 3 ADEM M64TGOMERY LABOROORY oa 1890-A Cnng.Wm. Dickinson Dr.. Montgomery.AL 36109 F �9 (3i0-2fi(1-]0]01Phnnd (374)-277.fi11X IPosI � • ' Analysis Report I Date of This Report... 08/09/2002 Fund Code: 521 Date ofthe Orikina[Report 0 810 9/2 0 0 2 Send Report.. Anne F.Cross Lab Sample ID: AA31115 Source... PWS-WHC/JBC-BS Location... WEST HUNTSVILLE CLEANERS Collection Date: 07/10/2002 Sample Matrix: WATER Collection Time: 9:48:00 AM Submittal Date: 07/12/2002 Sample Collector: AFCross-AnneCross Submittal Time: 10:45:00 AM Sample Received by: C. D.AMMONS Date Analvsis Validated... 08/08/2002 by WBB The results on the attached report are from the sample that was received and is referenced above. Tire sample was analyzed using standard EPA testing procedures and quality analysis protocol Instrument calibration and quality control are within acceptable limits of precision and accuracy. A close review by our Quality Assurance Program certifies that all prescribed test hold times were met and our strict quality assurance standards were observed. Submitted by: & ftrnr�.in. Quality Assurance Manager ADEM's Central laboratory has met all Requirements for Certification by EPA Region Four to Analyze Samples for all of the Parameters Required Under the Safe Drinking Water Act. Trace Metals Analysis Performed by.... ADC Parameter Result Units MDL Date ofAnalsis CAS# Method Reference Arsenic, Total. <MDL ug/L 10.0 07/292002 7440-38-2 EPA206.2 Cadmium, Total <MDL mg/L 0.003 071262002 7440.43-9 EPA200.7 Chromium, Total < MDL mg/L 0.015 0712612002 7440.47-3 EPA200.7 Lead, Total <MDL ug/L 2.00 0729)2002 7439-92-1 EPA239.2 Mercury, Total <MDL ug[L 0.3 081082002 7439-97-6 EPA245.2 Volatiles in Liquids Analysis Performed by.... RLH Parameter Result Units MDL Date of Analysis CAS# Method Re erence 1,1,1,2-Tetrachloroethane < MDL ug/L 5.0 071162002 630-20.6 SW8260B 1,1,1-Trichloroethane < MDL ug/L 5.0 071162002 71-55.6 SW8260B 1,1,2,2-Tetrachloroethane <MDL ug[L 5.0. 0711612002 79.34.5 SW8260B 1,1,2-Trichloroethane < MDL ug/L 5.0 071162002 79.00-5 SW8260B 1,1-Dichloroethane < MDL ug/L 5.0 071162002 75-34-3 SW8260B 1,1-Dichlorcethene < MDL ug/L 5.0 071162002 75-35.4 SW8260B 1,1-Dichloropropanone <MDL ug/L 5.0 0711612002 513-88-2 SW8260B 1,1-Dichlompropene <MDL ug/L 5.0 071162002 563-58-6 SW8260B 1,2,3-Trichlorobenzene <MDL ug/L 5.0 0711612002 87-61-6 SW8260B 1,2,3-Tiichloropropane < MDL ug/L 5.0 071162002 96-18-4 SW8260B 1,2,4-Trichlorobenzene < MDL ug/L 5.0 071162002 120.82-1 SW8260B 1,2,4-Trimethylbenzene <MDL ug/L 5.0 071162002 95.63-6 SW8260B 1,2-Dibromo-3-Chloropropane < MDL ug/L 5.0 0711612002 96.12-8 SW8260B 1,2-Dibromoethane(EDB) < MDL ug/L 5.0 071162002 106.93.4 SW8260B 1,2-Dichlorobenzene < MDL ug/L 5.0 0711612002 95.50-1 SW8260B 1,2-Dichloroethane < MDL ug/L 5.0 0711612002 107-06-2 SW8260B 1,2-Dichloropropane <MDL ug[L 5.0 0711612002 78-87.5 SW8260B 1,3,5-Trimethylbenzene <MDL ug[L 5.0 0711612002 108-67-8 SW8260B 1,3-Dichlorobenzene <MDL ug/L 5.0 071162002 541.73-1 SW8260B 1,3-Dichloropropane <MDL ug/L 5.0 071162002 142-28-9 SW8260B Lab Sample Number.............................. AA31115 Page 1 of 3 Volatiles in Liqui• dnulyris Perfrrrnred hr...4 RLH Parameter Result Units hIDL Date .Inat s' CdSN Method Refe 1,4-Dichlorobenzene < MDL ug/L 5.0 0711612002 106-46-7 SVV82608 1-Chlorobutane <MDL ug/L 5.0 0711612002 109-69-3 ,SW82601? 2,2-Dichloropropane <MDL ug/L 5.0 0711612002 590-20-7 SW8260B 2-Butanone < MDL ug/L 5.0 0711612002 78.93-3 SIV8260B 2-Chlorotoluene < MDL ug/L 5.0 0711612002 95-49.8 SW8260B 2-Hexanone < MDL ug/L 5.0 0711612002 591.78-6 SW8260B 2-Nitropropane < MDL ug/L 5.0 0711612002 79-46.9 SW8260B 4-Chlorotoluene <MDL ug/L 5.0 0711612002 106-43.4 SIV8260B 4-Isopropyltoluene < MDL ug/L 5.0 071162002 99.87.6 SW8260B 4-Methyl-2-pentanone(MIBK) < MDL ug/L 5.0 0711612002 108.10-1 SW82608 Acetone < MDL ug/L 10.0 0711612002 67-64.1 SW8260B Acrylonitrile <MDL ug/L 5.0 0711612002 107-13-1 SIV8260B Ally Chloride <MDL ug/L 5.0 0711612002 107-05.1 SW8260H Benzene < MDL ug/L 5.0 0711612002 71.43-2 PV8260B Bromobenzene < MDL ug/L 5.0 0711612002 108.86-1 SIV8260B Bromochloromethane <MDL ug/L 5.0 0711&2002 74.97.5 SIV8260B Bromodichloromethane <MDL ug/L 5.0 0711612002 75-27.4 SW8260B Bromoform < MDL ug/L 5.0 0711612002 75.25-2 SW8260B Bromomethane < MDL ug/L 5.0 0711612002 74.83.9 SW82608 Carbon Disullide <MDL ug/L 5.0 0711612002 75.15-0 SW8260B Carbon Tetrachloride <MDL ug/L 5.0 0711612002 56.23-5 SW8260B Chloroacetonitrile < MDL ug/L 5.0 0711612002 107.14.2 SW8260B Chlorobenzene < MDL ug/L 5.0 07116/2002 108-90-7 SW8260B Chloroethane <MDL ug/L 5.0 071162002 75-00.3 SW8260B Chloroform <MDL ug/L 5.0 0711612002 67-66.3 SW8260B Chloromethane < MDL ug/L 5.0 071162002 74-87.3 SW8260B cis-1,2-Dichloroethene < MDL ug/L 5.0 0711612002 156-59-2 SVV8260B cis-1,3-Dichloropropene <MDL ug/L 5.0 071162002 10061-01.5 SW8260B Dibromochloromethane <MDL ug/L 5.0 0711612002 124-48.1 SW8260B Dibromomethane < MDL ug/L 5.0 071162002 74.95.3 SW8260B Dichlorodifluoromethane < MDL ug/L 5.0 0711612002 75.71-8 SW8260D Diethyl Ether <MDL ug/L 5.0 0711612002 60-29.7 SW8260B Ethyl Methacrylate <MDL ug/L 5.0 0711612002 97-63-2 SW8260B Ethylbenzene < MDL uglL 5.0 071162002 100.41-4 SW8260B Hexachlarobutadiene < MDL ug/L 5.0 0711612002 87.68.3 SW8260B Hexachloroethane < MDL ug/L 5.0 071162002 67.72-1 SW8260B lodomethane <MDL ug/L 5.0 071162002 74.88-4 SW8260B Isopropylbenzene < MDL ug/L 5.0 0711612002 98-82-8 SW8260B meta-Xylene < MDL ug/L 5.0 07116/2002 108-38-3 SW8260B Methacrylonitrile <MDL ug/L 5.0 071162002 126-98.7 SW8260B Methyl t-Butyl Ether <MDL ug/L 5.0 071162002 1634-04.4 SW8260B Methylacrylate <MDL ug/L 5.0 071162002 96.33.3 SW8260B Methylene Chloride < MDL ug/L 5.0 0711612002 75-09-2 SW8260B Methylmethacrylate <MDL ug/L 5.0 0711612002 80.62-6 SW8260B n-Butylbenzene <MDL ug/L 5.0 0711612002 104.51-8 SW8260B n-Propylbenzene <MDL ug/L 5.0 0711612002 103-65-1 SW8260B Naphthalene < MDL ug/L 5.0 0711612002 91.20-3 SW8260B Nitrobenzene < MDL ug/L 5.0 0711612002 98-95-3 SW8260B ortho-Xylene < MDL ug/L 5.0 071162002 95.47-6 SW8260B para-Xylene <MDL uglL 5.0 0711612002 106-42-3 SW8260B Pentachloroethane < MDL ug/L 5.0 0711612002 76-01.7 SW8260B Propionitrile < MDL ug/L 5.0 0711612002 107.12-0 SW8260B sec-Butylbenzene <MDL ug/L 5.0 0711612002 135.98-8 SW8260B Styrene <MDL ug/L 5.0 07116/2002 100-42.5 SIV8260B tert-Butylbenzene < MDL ug/L 5.0 0711612002 98-06.6 SW8260B Lab Sample Number............ .. . .. .. AA31115 page 2 of 3 Volatiles in Liqui� Analysis Performed bp... RLN Parameter Result Units MDL D M n Ana s's CAS# Method od Reference Tetrachlorcethylene <MDL ug/L 5.0 0711612002 127-18-4 • SW8260B Tetrahydrofuran < MDL ug/L 5.0 07/l612002 109-99.9 SIV8260B Toluene < MDL ug/L 5.0 0711612002 108-88.3 SW8260B trans-1,2-Dichloroethene < MDL ug/L 5.0 0711612002 156-60-5 SW8260B trans-1,3-Dichloropropene < MDL ug/L 5.0 0711612002 10061-02-6 STY82608 trans-1,4-Dichloro-2-butene <MDL ug/L 5.0 0711612002 110-57.6 SIV8260B Trichloroethene < MDL ug/L 6.0 0711612002 79.01-6 SIV8260B Trichlorolluoromethane < MDL ug/L 5.0 071162002 75.69-4 SW8260B Vinyl Chloride < MDL ug/L 5.0 071162002 75-01-4 SIV8260B Lab Sample Number.............................. AA31115 page 3 of 3 � ADEM MPNTGOMERY LABOR#ORY o N . 1890-A Cone. Wm. Dickinson Dr.,Monteomery, AL 36109 (334).360-2770Iphonel (334)-2776718 IFu. ♦r �• o ,. t : Analysis Report y FAr Date of This Report.. 7/17/02 Fund Code, 521 Date of the Original Report 7/17/02 Send Report.. Anne F. Cross Lab Sample 1D: AA31114 Source... TB-WHC/JBC-01 Location... WEST HUNTSVILLE CLEANERS Collection Date: 718/02 Sample Matrix. WATER Collection Time: 10:00:00 AM Sample Collector: AFCross-AnneCross Submittal Date: 7/12102 Submittal Time: 10:45:00 AM Sample Received by: C.D.AMMONS Date Analysis Validated... 7117/02 by WBB The results on the attached report ore from the sample that was received and is referenced above. The sample was analyzed using standard EPA testing procedures and quality analysis protocol Instrument calibration and quality control are within acceptable limits of precision and accuracy. A close review by our Quality Assurance Program certifies that all prescribed test hold times were met and our strict quality assurance standards were observed. Submiuedby: Rjjj �.R6tf%A Quality Assurance Manager ADEM's Cenaal laboratory has met all Requirements for Cergkadon by EPA Region Four to Analyze Samples for all of the Parameter,Required Under the Safe Drinking Water Act. Volatiles in Liquids Analysis Performed by.... RLH Parameter Result Units MDL Date ofAnalvsis CAS# Method Reference 1,1,1,2-Tetrachloroethane <MDL ug/L 5.0 7116102 630.20-6 SW8260B 1,1,1-Trichloroethane <MDL ug/L 5.0 7116102 71.55-6 SW8260B 1,1,2,2-Tetrachlorcethane <MDL ug/L 5.0 7116102 7934.5 SW8260B 1,1,2-Trichloroethane <MDL ug/L 5.0 7116102 79.00.5 SW8260B 1,1-Dichloroethane <MDL ug/L 5.0 7116102 7534-3 SW8260B 1,1-Dichloroethene <MDL ug/L 5.0 7116102 75.35-4 SW8260B 1,1-Dichloropropanone <MDL ug/L 5.0 7116102 513.88.2 SW8260B 1,1-Dichloropropene <MDL ug/L 5.0 7116102 563-58.6 SW8260B 1,2,3-Trichlorobenzene <MDL ug/L 5.0 7116102 87.61-6 SW8260B 1,2,3-Trichlaropropane < MDL ug/L 5.0 7116102 96.18-4 SW8260B 1,24-Trichlorobenzene <MDL ug/L 5.0 7116102 120-82.1 SW8260B 1,2,4-Ttimethylbenzene <MDL ug/L 5.0 7116102 95-63.6 SW8260B 1,2-Dibromo3-Chloropropane <MDL ug/L 5.0 7116102 96-12-8 SW8260B 1,2-Dibromoethane(EDB) < MDL ug/L 5.0 7116102 106-93-4 SW8260B 1,2-Dichlorobenzene <MDL ug/L 5.0 7116102 95-50.1 SW8260B 1,2-Drchloroethane <MDL ug/L 5.0 7116102 107-06-2 SW8260B 1,2-Dichloropropane <MDL ug/L 5.0 7116102 78-87.5 SW8260B 1,3,5-Trimethylbenzene <MDL uglL 5.0 7116102 108-67.8 SW8260B 1,3-Dichlorobenzene <MDL ug/L 5.0 7116102 541.73.1 SW8260B 1,3-Dichloropropane <MDL ug/L 5.0 7116102 142-28.9 SW8260B 1,4-Drchlorobenzene <MDL ug/L 5.0 7116102 106-46-7 SW8260B 1-Chlorobutane < MDL ug/L 5.0 7116102 109.69.3 SW8260B 2,2-Dichloropropane < MDL ug/L 5.0 7116102 590-20.7 SW8260B 2-Butanone <MDL ug/L 5.0 7116102 78-933 SW8260B 2-Chlorotoluene < MDL ug/L 5.0 7116102 95-49-8 SW8260B 2-Hexanone <MDL ug/L 5.0 7116102 591-78-6 SW8260B 2-Nitropropane < MDL ug/L 5.0 7116102 79-46-9 SW8260B Lab Sample Number............. ............. AA31 1 14 page 1 of 3 Volatiles in Ligeti Analvsis Pe formed bv. RLH Parameter b Result U tits MDL Date n(A�sis CAS# Method Reference 4-Chlorotoluene <MDL ug/L 5.0 7176102 106-43.4 SIV8260B 4-lsopropyltoluene < MDL ug/L 5.0 7116102 99.87-6 SW8260B 4-Methyl-2-pentanone(MIBK) <MDL ug/L 5.0 7116102 108-10.1 SIV8260B Acetone <MDL ug/L 10.0 7116102 67-64-1 SIV8260B Acrylonitrile < MDL ug/L 5.0 7116102 107.13-1 SIV8260B Ally Chloride <MDL ug/L 5.0 7116102 107-05.1 SIV8260B Benzene < MDL ug/L 5.0 7116102 71.43-2 STY8260B Bromobenzene <MDL ug/L 5.0 7116102 108-86.1 SIV8260B Bromochicromethane <MDL ug/L 5.0 7116102 74-97.5 SW8260B Bromodichloromethane < MDL ug/L 5.0 7116102 75-27-4 STY8260B Bromoform <MDL ug/L 5.0 7116102 75.25-2 SIV8260B Bromomethane < MDL ug/L 5.0 7116102 74-83.9 SW8260B Carbon Disulfide <MDL ug/L 5.0 7116102 75-15-0 SIV8260B Carbon Tetrachloride <MDL ug/L 5.0 7116102 56.23-5 SW8260B Chloroacetonitrile < MDL ug/L 5.0 7116102 107-14-2 SW8260B Chlorobenzene <MDL ug/L 5.0 7116102 108.9D-7 STY8260B Chloroethane < MDL ug/L 5.0 7116102 75.00-3 SW8260B Chloroform <MOL ug/L 5.0 7116102 67.66-3 SIV8260B Chloromethane <MDL ug/L 5.0 7116102 74-87-3 SW8260B cis-1,2-Dichloroethene <MDL ug/L 5.0 7116102 156-59.2 SW8260B cis-1,3-Dichloropropene <MDL ug/L 5.0 7116102 10061.01-5 SIV8260B Dibromochicromethane <MDL ug/L 5.0 7116102 124.48-1 SW8260B Dibromomethane <MDL ug/L 5.0 7116102 74-95-3 SW8260B Dichlorodilluoromethane < MDL ug/L 5.0 7116102 75.71-8 STY8260B Diethyl Ether <MDL ug/L 5.0 7116102 60-29-7 SW8260B Ethyl Methacrylate < MDL ug/L 5.0 7116102 97-63-2 SW8260B Euylbenzene <MDL ug/L 5.0 7116102 100-41.4 SW8260B Hexachlorobutadiene < MDL ug/L 5.0 7176102 87-68-3 SW8260B Hexachloroethane <MDL ug/L 5.0 7116102 67-72-1 SW8260B lodomethane <MDL ug/L 5.0 7116102 74-88-4 SW8260B Isopropylbenzene <MDL ug/L 5.0 7116102 98-82-8 SW8260B meta-Xylene <MDL ug/L 5.0 7116102 108-38-3 SW8260B Methacrylonitrile <MDL ug/L 5.0 7116102 126-98-7 SW8260B Methyl RBufyl Ether - < MDL ug/L 5.0 7116102 1634-04.4 SW8260B Methyiacrylate <MDL ug/L 5.0 7116102 96-33-3 SW8260B Methylene Chloride <MOL ug/L 5.0 7116102 75-09.2 SW8260B Methylmethacrylate <MDL ug/L 5.0 7116102 80-62.6 SW8260B n-Butylbenzene < MDL ug/L 5.0 7116102 104-51.8 SW8260B n-Propylbenzene <MDL ug/L 5.0 7116102 103-65-1 SW8260B Naphthalene <MDL ugtL 5.0 7116102 91-20-3 SW8260B Nitrobenzene <MDL ug/L 5.0 7116102 98.95.3 SW8260B ortho-Xylene <MDL ug/L 5.0 7116102 95-47-6 SW8260B Para-Xylene <MOL ug/L 5.0 7116102 106.42-3 SW8260B Pentachloroethane <MDL ug/L 5.0 7116102 76.01.7 SW8260B Propionitrile <MDL ug/L 5.0 7116102 107-12-0 SW8260B sec-Butylbenzene <MDL ug/L 5.0 7116102 135-98.8 SW8260B Styrene <MDL ug/L 5.0 7116102 100-42.5 SW8260B tert-Butylbenzene < MDL ug/L 5.0 7116102 98-06-6 STY8260B Tetrachloroethyiene < MOL ug/L 5.0 7116102 127.18.4 SW8260B Tetrahydrofumn <MDL ug/L 5.0 7116102 109.99-9 SW8260B Toluene < MDL ug/L 5.0 7116102 108-88-3 SW8260B trans-1,2-Dichloroethene <MDL ug/L 5.0 7116102 156-60.5 SW8260B trans-1,3-Dichloropropene <MDL uglL 5.0 7116102 10061-02-6 SW8260B trans-1,4-Dichloro-2-butene < MDL ug/L 5.0 7116102 110-57-6 SW8260B Trichloroethene <MDL ug/L 5.0 7116102 79-01-6 SW8260B Lab Sample Number................ AA31114 page 2 of 3 Volatiles in Liquids Analvsis Performed bv.... RLH Parameter Result Units MDL Date ofA, Deis CAS# Method Reference Trichlorofluoromethane <MDL - ug/L 5.0 7116102 75-69.4 SW82608 Vinyl Chloride <MDL ug/L 5.0 7116102 75.01-4 SW8260B Lab Sample Number.............................. AA311 14 Page 3 of 3 ATTACHMENT 1 , ,d ggg � ` I e Vi Pa.�r Surface Water Sample Location CERCLA Site Inspection N Surface Water Sample Locations Huntsville, Madison County Alabama µt g 2000 0 2000 4000 Feet s G ATTACHMENT 9 III i i ADEM MWGOMERY LABORAO)RY 0 O 1890-A Cone. Wm. Dickinson Dr., Montgomery. AL 36109 l,Bq Ta9r 1334b260-3]70(phnn<1 (3741-277-6718(Fax I Analysis Report FAT sE* Date of This Report... OB/09/2002 Fund Code: 521 Date of the Original Report... 08/09/2002 Send Report... Anne F. Cross Lab Sarnple ID: AA31110 Source... SW-BS-02 Location... WEST HUNTSVILLE CLEANERS CollecCollection Date: 12: 1:0002 Sample Matrix: WATER Submittal Time: 1 7/1:/0 PM Sample Collector: AFCross-AnneCross Submittal Date: 10:45:00 A Submittal Time: 10:45:00 AM Sample Received by: C. D.AMMONS Date Analvsis Validated... 0 8/0 812 0 02 by WBB The results on tire attached report are from the sample that was received and is referenced above. Tile sample was analyzed using standard EPA testing procedures and quality analysis protocol. htstrttment calibration and quality control are within acceptable limits of precision and accuracy. A close review by our Quality Assurance Program certifies that all prescribed test hold times were met and our strict quality assurance standards were observed. Submitted by: %!7.� R4ZZCEisl1 Quality Assurance Manager ADEM's Cenral laboratory has met all Requirements for Certification by EPA Region Four to Analyze Samples for all of the Parameters Required Under the Safe Drinking Water Act. Trace Metals Analysis Performed by.... ADC Parameter Result Units MDL Date jAnalysis CAS# Method Reference Arsenic, Total <MDL ugtL 10.0 071292002 7440-38.2 EP4206.1 Cadmium, Total <MDL mg/L 0.003 0712612002 7440-43-9 EPA200.7 Chromium, Total < MDL mg/L 0.015 0712612002 7440.47.3 EPA200.7 Lead, Total 2.13 uglL 2.00 0712912002 7439.92-1 EPA239.2 Mercury, Total < MDL ug/L 0.3 081082002 7439-97.6 EP4245.1 Volatilgs in Liquids Analysis Performed by.... RLH Parameter Result Units MDL Date of Analysis CAS# Method Reference 1,1,1,2-Tetrachloroethane <MDL ug/L 5.0 0711612002 630.20-6 SW8260B 1,1,1-Trichloroethane <MDL ug/L 6.0 071162002 71-55-6 SW8260D 1,1,2,2-Tetrachloroethane <MDL ug/L 5.0 0711612002 79-34-5 SW8260B 1,1,2-Trichloroethane <MDL ug/L 5.0 071162002 79.OD-5 SW8260B 14-Dichloroethane <MDL ug/L 5.0 071162002 75.34-3 SW8260B 1,1-Dichloroethene <MDL ug/L 5.0 071162002 75-35-4 SW8260B 1,1-Dichloropropanone <MDL ug/L 5.0 0711612002 513-88.2 SW8260B 1,1-Dichloropropene <MDL ug/L 5.0 071162002 563-58.6 SW8260B 1,2,3-Trichlorobenzene < MDL ug/L 5.0 0711612002 87-61.6 SW8260B 1,2,3-Tichooropropane < MDL ug/L 5.0 071162002 96.18-4 SW8260B 1,2,4-Trichlorobenzene <MDL ug/L 5.0 0711612002 120.82-1 SW8260D 1,2,4-Trimethylbenzene < MDL ug/L 5.0 0711612002 95.63.6 SW8260B 1,2-Dibromo-3-Chloropropane < MDL ug/L 5.0 071162002 96.12-8 SW8260B 1,2-Dibromoethane(EDB) < MDL ug/L 5.0 071162002 106-93-4 SW8260B. 1,2-Dichlorobenzene < MDL ug/L 5.0 071162002 95.50-1 SW8260B 1,2-Dichloroethane <MDL ug/L 5.0 071162002 107-06-2 SW8260B 1,2-Dichloropropane < MDL ug/L 5.0 071162002 78-87-5 SW8260B 1,3,5-Trimethylbenzene < MDL ug/L 5.0 071162002 108-67.8 SW8260B 1,3-Dichlorobenzene _ < MDL ugiL 5.0 071162002 541-73-1 SW8260B .. 1,3-Dichloropropane < MDL ug/L 5.0 071162002 142.28-9 SW8260B Lab Sample Number............................. AA31110 page 1 of Vulariles in Liquids• rinalcsis' Performed b1.... RLH Parameter Result Units VIDL Dare . Andrs s CAS p Method Reference 1,4-Dichlorobenzene <MDL ug/L 5.0 0711612002 106.46.7 ,SIV8260B 1-Chlorobutane < MDL ug/L 5.0 0711612002 109-69.3 SIV8260B 2,2-Dichloropropane < MDL ug/L 5.0 0711612002 590.20.7 SIVS260B 2-Butanone < MDL ug/L 5.0 0711612002 78.93-3 SIV8260B 2-Chlorotoluene <MDL ug/L 5.0 0711612002 95.49-8 SIVS260B 2-Hexanone < MDL ug/L 5.0 0711612002 591-78-6 SIV8260B 2-Nitropropane < MDL ug/L 5.0 0711612002 79-46-9 SIV8260B 4-Chlorotoluene <MDL ug/L 5.0 0711612002 106-43.4 SIV8260B 4-Isopropyltoluene <MDL ug/L 5.0 0711612002 99.87-6 SIV8260B 4-Methyl-2-pentanone(MIBK) < MDL ug/L 5.0 0711612002 108-10-1 SIV8260B Acetone < MDL ug/L 10.0 0711612002 67.64-1 STY8260B Acrylonitrile < MDL ug/L 5.0 0711612002 107-13-1 SIV8260B Ally Chloride <MDL ug/L 5.0 0711612002 107.05-1 SIV8260B Benzene <MDL ug/L 5.0 0711612002 71-43-2 SW8260B Bromobenzene < MDL ug/L 5.0 0711612002 108-86-1 SIV8260B Bromochloromethane <MDL ug/L 5.0 0711612002 74-97-5 SIV8260B Bromodichloromethane <MDL ug/L 5.0 0711612002 75-27.4 SIV8260B Bromoform <MDL ug/L 5.0 0711612002 75-25.2 SW8260B Bromomethane < MDL ug/L 5.0 0711612002 74.83-9 SIV8260B Carbon Disulfide <MDL ug/L 6.0 0711612002 75-15-0 SW8260B Carbon Tetrachloride <MDL ug/L 5.0 0711612002 56-23.5 STY8260B Chloroacetonitrile <MDL ug/L 5.0 0711612002 107.14-2 SW8260B Chlorobenzene <MDL ug/L 5.0 0711612002 108-90-7 SIV8260B Chloroethane < MDL ug/L 5.0 0711612002 75-00-3 SW8260B Chloroform <MDL ug/L 5.0 0711612002 67-66-3 SW8260B Chloromethane <MDL ug/L 5.0 0711612002 74-87.3 SW8260B cis-1,2-Dichloroethene <MDL ug/L 5.0 0711612002 156.59-2 SIV8260B cis-1,3-Dichloropropene <MDL ug/L 5.0 0711612002 10061-01-5 SW8260B Dibromochloromethane < MDL ug/L 5.0 0711612002 124-48.1 SW8260B Dibromomethane <MDL uglL 5.0 0711612002 74-95.3 SW8260B Dichlorodifluoromethane <MDL ug/L 5.0 0711612002 75.71.8 SW8260B Diethyl Ether <MDL ug/L 5.0 0711612002 60-29-7 SW8260B Ethyl Methacrylate <MDL ug/L 5.0 0711612002 97-63-2 SW8260B Ethylbenzene <MDL ug/L 5.0 0711612002 100-41-4 SW8260B Hexachlorobutadiene <MDL ug/L 5.0 0711612002 87.68-3 SW8260B Hexachloroethane <MDL ug/L 5.0 0711612002 . 67.72-1 SW8260B lodomethane <MDL uglL 5.0 0711612002 74-88-4 SW8260B Isopropylbenzene <MDL uglL 5.0 0711612002 98-82-8 SW8260B meta-Xylene <MDL ug/L 5.0 0711612002 108-38-3 SIV8260B Methacrylonitrile < MDL ug/L 5.0 0711612002 126-98.7 SW8260B Methyl t-Butyl Ether < MDL ug/L 5.0 0711612002 1634-04-4 SW8260B Methylacrylate <MDL ug/L 6.0 0711612002 96.33-3 SW8260B Methylene Chloride <MDL ug/L 5.0 0711612002 75-09.2 SW8260B Methylmethacrylate <MDL ug/L 5.0 071162002 80.62-6 SW8260B n-Butylbenzene <MDL ug/L 5.0 0711612002 104-51-8 SW8260B n-Propylbenzene <MDL uglL 5.0 071162002 103.65-1 SW8260B Naphthalene <MDL ug/L 5.0 0711612002 91-20-3 SW8260B Nitrobenzene <MDL ug/L 5.0 0711612002 98-95.3 SW8260B ortho-Xylene < MDL ug/L 5.0 0711612002 95-47.6 SW8260B para-Xylene < MDL uglL 5.0 0711612002 106-42-3 SW8260B Pentachloroethane < MDL ug/L 5.0 0711612002 76-01.7 SW8260B Propionitrile <MDL ug/L 5.0 0711612002 107-12-0 SIV8260B sec-Butylbenzene <MDL ug/L 5.0 0711612002 135-98-8 SW8260B Styrene _ <MDL ug/L 5.0 0711612002 100-42-5 SW8260B tort-Butylbenzene <MDL uglL 5.0 0711612002 98-06.6 SW8260B-" Lab Sample Number.............................. AA31110 Page 2 of 3 Volatiles in Liquids• Anah'.vi.e Performed Ig.... #RLH Parameter R 1t Units MIDI Dale of Anah CAS# bletl d Re erence Tetrachloroethylene <MDL ug/L 5.0 0711612002 127-18.4 S;V8260B Tetmhydroluran <MDL ug/L 5.0 0711612002 109-99.9 SW8260B Toluene < MDL ug/L 5.0 0711612002 108-88-3 SW8260B trans-1,2-Dichloroethene <MDL ug/L 5.0 0711612002 156-60-5 SW8260B trans-1,3-Dichloropropene <MDL ug/L 5.0 0711612002 10061-02.6 SW8260B trans-1,4-Diehloro-2-hutene < MDL ug/L 5.0 0711612002 110.57-6 SIV8260B Trichloroethene <MDL ug/L 5.0 0711612002 79-01.6 SIV8260B Trichlorolluoromethane < MDL ug/L 5.0 0711612002 75.69-4 SIV8260B Vinyl Chloride <MDL ug/L 5.0 0711612002 75-01-4 SW82608 i i Lab Sample Number.............................. AA31110 Page 3 of D ADEM MWGOMERY LABORAO)RY 1890-A Cong. Wm. Dickinson Dr..Montgomcry.AL 36109 1,.Bp, T �9 0;4i 260-?7701,honel (1;4,.±77-6"',IFa.I � " Analysis Report �4T Date of This Report... 08/09/2002 Fund Code: 521 Date of the Original Report.. 08/09/2002 Send Report... Anne F.Cross Lab Sample 1D: AA31111 Source... SW-MMB-03 Location... WEST HUNTSVILLE CLEANERS Collection Date: 07/112002 Sample Matrix: WATER Collection Time: 10:58:00 AM Submittal Date: 07/12/2002 Sample Collector: AFCross-AnneCross Submittal Time: 10:45:00 AM Sample Received by: C. D.AMMONS Date Analvsis Validated... 08/082002 by WBB The results on the attached report are from the sample that was received and is referenced above. The sample was analyzed using standard EPA testing procedures and quality analysis protocol. Instrument calibration and quality control are within acceptable limits of precision and accuracy. A close review by our Quality Assurance Program certifies that all prescribed test hold tines were met and our strict quality assurance standards were observed. Submiltedby: j?jZj?,X& 'L(42, Quality Assurance Manager ADEM's Central laboratory has net all Requirements for Certification by EPA Region Four to Analyze Samples for all of the Parameters Required Under the Safe Drinking Water Act. Trace Metals Analysis Performed by.... ADC _Parameter Result Units MDL Date of Analysis CAS# Method Reference Arsenic, Total <MDL uglL 10.0 0712912002 7440.38.2 EPA206.2 Cadmium, Total <MDL mg/L 0.003 072612002 7440-43-9 EPA200.7 Chromium, Total <MDL mg/L 0.015 071262002 7440-47-3 EPA200.7 Lead, Total <MDL ug/L 2.00 0712912002- 7439.92-1 EPA239.2 Mercury, Total <MDL ug/L 0.3 081082002 7439-97.6 EPA245.2 VOlatiles in Liquids Analysis Performed by.... RLH Parameter - Result Units MDL Date of Analysis CAS# Method Re erence 1,1,1,2-Tetrachloroethane <MDL uglL 5.0 07/15)2002 630.20-6 SW8260D 1,1,1-Trichloroethane -<MDL ug/L 6.0 071152002 71-55-6 SW8260B 1,1,2,2-Tetrachloroethane <MDL ug/L 5.0 0711512002 79-34.5 SW8260B 1,1,2-Trichloroethane <MDL uglL 5.0 071152002 79.00.5 SW8260B 1,1-Dichloroethane <MDL ug/L 5.0 071152002 75.34-3 SW8260B 14-Dichloroethene <MDL uglL 5.0 071152002 75-35-4 SW8260B 1,1-Dichloropropanone <MDL uglL 6.0 0711512002 513-88.2 SW8260B 1,1-Dichloropropene < MDL ug/L 5.0 071152002 563-58-6 SW82608 1,2,3-Trichlorobenzene <MDL ug/L 5.0 0711512002 87-61.6 SW8260B 1,2,3-Trichloropropane <MDL ug/L 5.0 071152002 96-18.4 SW8260B 1,2,4-Trichlorobenzene <MDL ug/L 5.0 071152002 12D-82-1 SW8260B 1,2,4-Trimethylbenzene <MDL ug/L 5.0 071152002 95-63-6 SW8260B 1,2-Dibromo-3-Chloropropane <MDL ugh- 5.0 0711512002 96.12-8 SW8260B 1,2-Dibromoethane(EDB) <MDL uglL 5.0 071152002 106-93.4 SW8260B 1,2-Dichlorobenzene < MDL uglL 5.0 071152002 95.50-1 SW8260B 1,2-Dichloroethane < MDL ug/L 5.0 071152002 107.06-2 SW82608 1,2-Dichloropropane < MDL ug/L 5.0 071152002 78-87.5 SW8260B 1,3,5-Trimethylbenzene < MDL uglL 5.0 071152002 108.67-8 SW8266B 1,3-Dichlorobenzene <MDL ug/L 5.0 071152002 541.73-1 SW8260B 1,3-Dlchloropropane <MDL ug/L 5.0 071152602 142-28.9 SW8260B-1. Lab Sample Number............................. AA31111 Page 1 of 3 - Volatiles in Liquids• Analysis PnJornred b,.... •RLH Parameter Result Units VIDE Date o -Analysts CAS N Method R le once 1,4-Dichlorobenzene <MDL ug/L 5.0 0711512002 106-46-7 SW82608 1-Chlorobutane < MDL ug/L 5.0 0711512002 109-69.3 SVV8260B 2,2-Dichloropropane <MDL ug/L 5.0 0711512002 590.20-7 SIVS260B 2-Butanone < MDL ug/L 5.0 0711512002 78.93-3 SSV82608 2-ChlorotDluene < MDL ug/L 5.0 0711512002 95-49.8 SW8260B 2-Hexanone <MDL ug/L 5.0 0711512002 591.78-6 SIV8260B 2-Nitropropane <MDL ug/L 5.0 071152002 79.46.9 SW8260B 4-Chlorotoluene <MDL ug/L 5.0 0711512002 106.43-4 SW8260B 4-Isopropyltoluene < MDL ug/L 5.0 0711512002 99-87.6 SIV8260B 4-Methyl-2-pentanone(MIBK) <MDL ug/L 5.0 0711512002 108-10-1 SIV8260B Acetone <MDL ug/L 10.0 0711512002 67-64-1 SW8260B Acrylonitrile < MDL ug/L 5.0 0711512002 107-13-1 SIV82608 Ally Chloride < MDL ug/L 5.0 0711512002 107-05.1 SW8260B Benzene <MDL ug/L 5.0 0711512002 71.43-2 SIV82608 Bromobenzene <MDL ug/L 5.0 0711512002 108.86-1 SW8260B Bromochloromethane < MDL ug/L 5.0 0711512002 74.97-5 SIV8260B Bromodichloromethane < MDL ug/L 5.0 0711512002 75.27-4 SW8260B Bromoform <MDL ug/L 5.0 0711512002 75-25.2 SW8260B Bromomethane < MDL ug/L 5.0 0711512002 74-83-9 SW8260B Carbon Disulfide < MDL ug/L 5.0 0711512002 75.15-0 SM260B Carbon Tetrachloride <MDL ugtL 5.0 071152002 56-23.5 SW8260B Chloroacetonitrile <MDL ug/L 5.0 071152002 107.14-2 SW8260B Chlorobenzene < MDL ug/L 5.0 0711512002 108-90.7 SW8260B Chloroethane <MDL ug/L 5.0 071152002 75-00.3 SW8260B Chloroform <MDL ug/L 5.0 071152002 67.66-3 SIV8260B Chloromethane <MDL ug/L 5.0 0711512002 74.87-3 SW8260B cis-1,2-Dichloroethene < MDL ug/L 5.0 0711512002 156-59-2 SW8260B cis-1,3-Dichloropropene <MDL ug/L 5.0 071152002 10061-01-5 SW8260B Dibromochloromethane <MDL ug/L 5.0 0711512002 124.48-1 SW8260D Dibromomethane <MDL ug/L 5.0 071152002 74.95-3 SW8260B Dichlorodifluoromethane < MDL ug/L 5.0 071152002 75-71-8 SW8260B Diethyl Ether <MDL ug/L 5.0 071152002 60.29-7 SW8260B Ethyl Methacrylate, <MDL ug/L 5.0 0711512002 97-63-2 SW8260B Euylbenzene <MDL ug/L 5.0 071152002 100-41-4 SW8260B Hexachlorobutadiene <MDL ug/L 5.0 0711512002 87-68.3 SW8260B Hexachloroethane <MDL ug/L 5.0 071152002 67-72-1 SW8260B lodamethane <MDL ug/L 5.0 0711512002 74.88-4 SW8260B Isopropylbenzene <MDL ug/L 5.0 071152002 98-82-8 SW8260B meta-Xylene <MDL uglL 5.0 0711512002 108.38-3 STY8260B Methacrylonitrile <MDL ug/L 5.0 071152002 126.98-7 SW8260B Methyl t-Butyl Ether <MDL ug/L 5.0 071152002 1634-04-4 SW8260B Methylacrylate <MDL ug/L 5.0 071152002 96-33-3 SW8260B Methylene Chloride <MDL ug/L 5.0 0711512002 75-09.2 SW8260B Methylmethacrylate <MDL ug/L 5.0 0711512002 80-62.6 SW8260B n-Butylbenzene <MDL ug/L 5.0 071152002 104-51-8 SW8260B n-Propylbenzene <MDL ug/L 5.0 071152002 103-65-1 SW8260B Naphthalene < MDL ug/L 5.0 071152002 91-20.3 SW8260B Nitrobenzene <MDL ug/L 5.0 0711512002 98-95.3 SW8260B ortho-Xylene <MDL ug/L 5.0 0711512002 95.47-6 SW8260B para-Xylene <MDL ug/L 5.0 0711512002 106.42-3 SW8260B Pentachloroethane <MDL uglL 5.0 071152002 76-01-7 SW8260B Propionitrile <MDL ugtL 5.0 071152002 107-12.0 SW8260B sec-Butylbenzene <MDL ug/L 5.0 0711512002 135-98.8 SW8260B Styrene <MDL ug/L 5.0 0711512002 100.42-5 SW8260B tert-Butylbenzene <MDL ug/L 5.0 0711512002 98-06-6' SW8260B` Lab Sample Nsntber.............................. AA31111 Page 2 of 3 Volatiles in Liquids Anah'sis Performed 15v .. RLH Parameter esult Units MDL Date of Anal CAS N Method Reference Tetrachloroethylene <MDL ug/L 5.0 0711512002 127-18.4 SIV8260B Tetrahydrofuran < MDL ug/L 5.0 0711512002 109-99-9 SW82608 Toluene < MDL ug/L 5.0 071152002 108.88-3 SW82608 trans-1,2-Dichloroethene < MDL ug/L 5.0 0711512002 lSS-60.5 SW8260B trans-1,3-Dichloropropene < MDL ug/L 6.0 071152002 10061-02.6 SW8260B trans-1,4-Dichloro-2-butene < MDL ug/L 5.0 0711512002 11D-67-6 SW8260B Trichloroethene <MDL ug/L 5.0 0711512002 79-01-6 SW8260B Trichlorofluoromethane < MDL ug/L 5.0 0711512002 75-69.4 SIV8260B Vinyl Chloride <MDL ug/L 5.0 0711512002 75.01-4 SW8260B Lab Sample Number AA31111 page 3 of 3 ADEM MOWGOMERY LABORAORY 0 1890-A Con_•. Wm. Dickinson Dr.. Montgomery.AL 36109 I1:11-I60-2770IPhanel 03,41d77 6718 IFaxt O Analysis Report +T Date of This Report... 08/09/2002 Fund Code: 521 Date of the Orieinal Report.. 0810912002 Send Report... Anne F. Cross Lab Sample ID: AA31109 Source... SW-HSB-01 Location... WEST HUNTSVILLE CLEANERS CollecCollection Date: 10:30:00 A Sample Matrix: WATER Submiliort Time: 1 7/12J 0 AM Sample Collector: AFCross-AnneCross Submittal Date: 07/1220 Submittal Time: 10:45:00 AM Sample Received by: C. D.AMMONS Date Analvsis Validated... 08/082002 by WBB The results on the attached report are from the sample that was received and is referenced above. The sample was analyzed using standard EPA testing procedures and quality analysis protocol. Instrument calibration and quality control are within acceptable limits of precision and accuracy. A close review by our Quality Assurance Program certifies that all prescribed test hold time..,were met and one strict quality assurance standards were observed. Submittedby: $tj7.�vaCk rrs, Quality Assurance Manager ADEM's Central laboratory has met all Requirements far Certification by EPA Region Four to Analyze Samples for all of the Parameters Required Under the Safe Drinking Water Act. Trace Metals Analysis Performed by.... ADC Parameter Result Units MDL Date of Analysis CAS# Method Reference Arsenic, Total <MDL ug/L 10.0 0712912002 7440-38.2 EPA206.2 Cadmium, Total <MDL mg/L 0.003 072612002 7440-43-9 EPA200.7 Chromium, Total <MDL mg/L 0.015 071262002 7440-47-3 EPA200.7 Lead, Total <MDL ug/L 2.00 071292002 7439.92.1 EPA239.2 Mercury, Total <MDL ug/L 0.3 081082002 7439-97-6 EPA245.2 Volatiles in Liquids Analysis Performed by.... RLH Parameter Result Units MDL Date of Analysis CAS# Method Reference 1,1,1,2-Tetrachloroethane <MDL ug/L 5.0 0711612002 630.20-6 SW8260B 1,1,1-Trichloroethane <MDL ug/L 5.0 0711612002 71.55-6 SW8260B 1,1,2,2-Tetrachloroethane <MDL uglL 5.0 071162002 79-34.5 SW8260B 1,1,2-Trichloroethane <MDL ug/L 5.0 0711612002 79-00.5 SW8260B 1,1-Dichloroethane <MDL ug/L 5.0 0711611002 75-34-3 SW8260B 1,1-Dichloroethene <MDL ug/L 5.0 0711612002 75-354 SW8260B 1,1-Dichloropropanone <MDL ug/L 5.0 0711612002 513-88.2 SW8260B 14-Dichloropropene <MDL ug/L 5.0 0711612002 563-58-6 SW8260B 1,2,3-Trlchlorobenzene <MDL ug/L 5.0 0711612002 87-61-6 SW8260B 1,2,3-Tcchloropropane <MDL ug/L 5.0 0711612002 96-18.4 SW8260B 1,2,4-Trichlorobenzene <MDL ug/L 5.0 071162002 120-82-1 SW8260B 1,2,4-Trimethylbenzene <MDL ug/L 5.0 0711612002 95.63-6 SW8260B 1,2-Dibromo-3-Chloropropane <MDL ug/L 5.0 0711612002 96-12.8 SW8260B 1,2-Dibromoethane(EDB) <MDL ug/L 5.0 0711612002 106.93-4 SW8260B 1,2-Dichtorobenzene <MDL ug/L 5.0 0711612002 95-50-1 SW8260B 1,2-Dichloroethane <MDL ug/L 5.0 0711612002 107.06.2 SW8260B 1,2-Dichloropropane <MDL ug/L 6.0 071162002 78-87-5 SW8260B 1,3,5-Trimethylbenzene <MDL ug/L 5.0 0711612002 108.67-8 SW8266B 1,3-Dichlorobenzene <MDL ug/L 5.0 0711612002 541.73-1 SW8260B ,, 1,3-Dichloropropane <MDL uglL 5.0 0711612002 142,28.9 SW8260B Lab Sample Number.............................. AA31109 page 1 of 3 Volariles in Liquids• Anul,Avs Perfbr ..ed be.... •RLH Parameter Result Units ,Y1D/_ Date o(.4nalvsrs CAS# Method Reference 1,4-Dichlorobenzene < MDL ug/L 5.0 0711612002 106-46-7 SIV82608 1-Chlorobutane < MDL ug/L 5.0 0711612002 109-69-3 SIV8260B 2,2-Dichloropropane < MDL ug/L 5.0 0711612002 590.20-7 SIV3260B 2-Butanone < MOL ug/L 5.0 0711612002 78-93.3 SIV826011 2-Chlorotoluene < MDL ug/L 5.0 0711612002 95.49-8 SIV8260B 2-Hexanone < MDL ug/L 5.0 0711612002 591-78-6 SIV82608 2-Nitropropane <MDL ug/L 5.0 0711612002 79-46.9 SIV8260B 4-Chlorotoluene < MDL ug/L 5.0 0711612002 106-43.4 SIV8260B 4-1sopropyltoluene < MDL ug/L 5.0 0711612002 99-87-6 SIV8260B 4-Methyl-2-pentanone(MIBK) < MDL ug/L 5.0 0711612002 108.10.1 SIVS260B Acetone < MDL ug/L 10.0 0711612002 67-64.1 SW8260B Acrylonitrile < MDL ug/L 5.0 0711612002 107.13-1 SIV8260B Ally Chloride < MDL ug/L 5.0 0711612002 107-05.1 SIV82608 Benzene <MOL ug/L 5.0 071162002 71-43.2 SIVS260B Bromobenzene <MDL ug/L 5.0 0711612002 108-86-1 SIV82608 Bromochloromethane < MDL ug/L 5.0 0711612002 74.97-5 SW8260B Bromodichloromethane < MDL ug/L 5.0 071162002 75.27-4 SW8260B Bromoform <MDL ug/L 5.0 0711612002 75-25.2 SIV8260B Bromomethane <MDL ug/L 5.0 0711612002 74.83.9 SIV8260B Carbon Disulfide < MDL ug/L 5.0 0711612002 75-15.0 SIV8260B Carbon Tetrachloride < MDL ug/L 5.0 0711612002 56.23-5 SW8260B Chloroacetonitrile <MDL ug/L 5.0 0711612002 107.14.2 SW8260B Chlorobenzene <MDL ug/L 5.0 0711612002 108.90-7 SIV8260B Chloroethane < MDL ug/L 5.0 0711612002 75-00-3 SYV8260B Chloroform < MDL ug/L 5.0 0711612002 67-66-3 SIV8260B Chloromethane <MDL ug/L 5.0 071162002 74-873 SW8260B cis-1,2-Dichloroethene <MDL ug/L 5.0 071162002 156-59-2 SIV8260B cis-1,3-Dichloropropene < MDL ug/L 5.0 0711612002 10061-01-5 SW8260B Dibromochloromethane < MDL ug/L 5.0 0711612002 124.48.1 STV8260B Dibromomethane <MDL ug/L 5.0 071162002 74.95.3 SW8260B Dichlorodifluoromethane <MDL ug/L 5.0 0711612002 75-71-8 SW8260B Diethyl Ether <MDL ug/L 5.0 0711612002 60-29-7 SW8260B Ethyl Methacrylate < MDL ug/L 5.0 071162002 97.63-2 SIV8260B Etylbenzene - < MDL ug/L 5.0 071162002 100-41-4 SW8260B Hexachlorobutadiene <MDL ug/L 5.0 071162002 87.68-3 SIV8260B Hexachloroethane <MDL ug/L 5.0 0711612002 67-72-1 SW8260B lodomethane < MDL ug/L 5.0 071162002 74.88.4 SW8260B Isopropylbenzene < MDL ug/L 5.0 0711612002 98.82-8 - SW8260B meta-Xylene <MDL ug/L 5.0 071162002 108-38.3 SW8260B Methacrylonitrile <MDL ug/L 5.0 0711612002 . 126.98.7 SW8260D Methylt-Butyl Ether <MDL ug/L 5.0 0711612002 1634.04-4 SW8260B Methylacrylate < MDL ug/L 5.0 0711612002 96.33-3 SW8260B Methylene Chloride < MDL ug/L 5.0 0711612002 75.09-2 SW8260B Methylmethacrylate < MDL ug/L 5.0 0711612002 80.62.6 SW8260B n-Butylbenzene <MDL ug/L 5.0 0711612002 104-51-8 SW8260B n-Propylbenzene <MDL ug/L 5.0 0711612002 103-65-1 SW8260B Naphthalene < MDL ug/L 5.0 071162002 91-20-3 SW8260B Nitrobenzene <MDL ug/L 5.0 0711612002 98.95-3 SW8260B ortho-Xylene < MDL ug/L 5.0 071162002 95.47.6 SW8260B para-Xylene < MDL ug/L 5.0 0711612002 106-42.3 SW8260B Pentachloroethane < MDL ug/L 5.0 071162002 76-01-7 SW8260B- Propionitrile <MDL ug/L 5.0 0711612002 107-12-0 SW8260B sec-Butylbenzene <MDL ug/L 5.0 071162002 135-98-8 SW82608 Styrene <MDL ug/L 5.0 0711612002 100-42-5 SW8260B _ Wrt-Butylbenzene <MDL ug/L 5.0 071162002 98-06-6 SW8260B Lab Saatple Number............................. AA31109 Page 2 of 3 VOlatiles in Liquid Ana/vsis Perfinmed bc.... RCH Parameter OResalt Units 4VIDL Date ojAaa CAS N Method Reference Tetrachloroethylene < MDL ug/L 5.0 0711612002 127-18-4 .SIV8260B Tetrahydroturan < MDL ug/L 5.0 0711612002 109-99-9 SW82608 Toluene < MDL ug/L 5.0 0711612002 108-88-3 SW8260B trans-1,2-Dichloroethene < MDL ug/L 5.0 0711612002 156-60-5 SIV8260B trans-1,3-Dichloropropene < MDL ug/L 5.0 0711612002 10061.02-6 SIV8260B trans-1,4-Dichlorc-2-butene < MDL ug/L 5.0 0711612002 110.57-6 SIV8260B Trichloroethene < MDL ug/L 5.0 0711612002 79-01-6 SIV8260B Trichlorotluoromethane < MDL ug/L 5.0 0711612002 75.69.4 SW826011 Vinyl Chloride <MDL ug/L 5.0 0711612002 75-01-4 SW8260B Lab Sample Number.............................. AA31 109 Page 3 of 3 ADEM MOOOGOMERY LABORAARY OQ 1890-A Cong.Wm. Dickinson Dr.,Montgomery. AL 36109 /% (:u+)-260 27701r1u,n=I (131)-277 6718 fr.,] Analysis Report + Date of This Report.,. 08/09/2002 Fund Code: 521 Date of the Original Report... 0 810 9/2 0 0 2 Send Report... Anne F.Cross Lab Sample lD: AA31113 Source... SW-HSB-D Location... WEST HUNTSVILLE CLEANERS Collection Date: 07/1120 Sample Matrix: WATER Collection Time: 1 / : 0 A AM Subntitta(Date: 07/12/2002 Sample Collector: AFCross-AnneCross ,Submittal Time: 10:45:00 AM Sample Received by: C. D.AMMONS Date Analvsis Validated... 08/08/2002 by WBB The results on the attached report are from the sample that was received and is referenced above. The sample was analy¢ed using standard EPA testing procedures and quality analysis protocol. Instrument calibration and quality control are within acceptable limits of precision and accuracy. A close review by our Quality Assurance Program certifies that all prescribed test hold times were met and our strict quality assurance standards were observed. Submitted by: S ZRmCk:.a, Quality Assurance Manager ADEM's Central Laboratory has met all Requirements for Certification by EPA Region Four to Analyze Samples fir all of the Parameters Required Under the Safe Drinking Water Act. Trace Metals Analysis Performed by.... ADC Parameter Result Units MDL Date of Analysis CAS# Method Reference Arsenic, Total <MDL ug/L 10.0 0712912002 7440.38-2 EPA2061 Cadmium, Total <MDL mg/L 0.003 0712612002 7440.43.9 EPA200J Chromium, Total <MDL mg/L 0.015 0712612002 7440.47.3 EPA200.7 Lead, Total <MDL ug/L - 2.00 071292002 7439.92-1 EPA239.2 Mercury, Total <MDL ug/L 0.3 0810812002 7439.97-6 EPA245.2 Volatiles in Liquids Analysis Performed by.... RLII Parameter Result Units MDL Date of Analysis CAS# Method Reference 1,1,1,2-Tetrachloroethane <MDL ug/L 5.0 071152002 630.20.6 SW8260B 1,1,1-Trichloroethane <MDL ug/L 5.0 071152002 71-55-6 SW8260B 1,1,2,2-Tetrachloroethane <MDL ug/L 5.0 07/15/2002 79-34-5 SW8260B 1,1,2-Trichloroethane <MDL ug/L 6.0 0711512002 79-00-5 SW8260B 1,1-Dichloroethane <MDL ug/L 5.0 07/152002 75.34-3 SW8260B 1,1-Dichloroethene <MDL ug/L 5.0 07/152002 75.35-4 SW8260B 1,1-Dichloropropanone <MDL ug/L 5.0 0711512002 513-88.2 SW8260B 1,1-Dichloropropene <MDL ug/L 5.0 07/152002 563-58-6 SW8260B 1,2,3-Trlchierobenzene <MDL ug/L 5.0 0711512002 87-61.6 SW8260B 1,2,3-Ticchloropropane <MDL ug/L 5.0 071152002 96-18.4 SW8260B 1,2,4-Tichoorobenzene <MDL ug/L 6.0 071152002 120-82-1 SW8260B 1,2,4-Trimethylbenzene <MDL ug/L 5.0 071152002 95-63.6 SW8260B 1,2-Dibromo-3-Chloropropane <MDL ug/L 5.0 071152002 96-12.8 SIV8260B 1,2-Dibromoethane(EDB) < MDL ug/L 6.0 071152002 106-93-4 SW8260B 1,2-Dichlorobenzene <MDL ug/L 5.0 071152002 95-50-1 SW8260B 1,2-Dichloroethane <MDL ug/L 5.0 071152002 107.06-2 SW8260B 1,2-Dichloropropane <MDL ug/L 5.0 071152002 78-87-5 SW8260B 1,3,5-7'rimethylbenzene <MDL ug/L 5.0 071152002 108.67-8 SW8260B 1,3-Dichlorobenzene <MDL ug/L 5.0 071152002 541.73-1 SW8260B 1,3-Dichloropropane <MDL ug/L 5.0 071152002 142-28-9 SW8260B Lab Sample Number............................. AA31113 page 1 of 3 Volariles in Liquids• A....h. is Pe,Jbnued I>c.... •RLH Parameter Result Units ,VIOL Date of Analysis CAS# Aletbnd Reference 1,4-Dichlorobenzene < MDL ug/L 5.0 0711512002 106-46-7 SIV'82608 1-Chlorobutane < MDL ug/L 5.0 0711512002 109-69-3 ,SIV826011 2,2-Dichloropropane < MDL ug/L 5.0 0711512002 590-20-7 SII'8260B 2-Butanone <MDL ug/L 5.0 0711512002 78-93.3 SIV8260B 2-Chlorotoluene <MDL ug/L 5.0 0711512002 95-49-8 ,SIV8260B 2-Hexanone <MDL ug/L 5.0 0711512002 591-78.6 SIV826011 2-Nitropropane < MDL ug/L 5.0 0711512002 79.46-9 SIV826OR 4-Chlorotoluene <MDL ug/L 5.0 0711512002 106-43.4 SIV8260B 4dsopropyltoluene < MDL ug/L 6.0 0711512002 99.87-6 SIV8260B 4-Methyl-2-pentanone(MIBK) < MDL ug/L 5.0 0711512002 108.10-1 SIV8260B Acetone <MDL ug/L 10.0 0711512002 67-64-1 SIV8260B Acrylonitrile < MDL ug/L 5.0 071IS12002 107.13.1 SIV8260B Ally Chloride <MDL ug/L 5.0 0711512002 107-06-1 SIV8260B Benzene < MDL ug/L 5.0 0711512002 71-43.2 SW8260B Bromobenzene < MDL ug/L 5.0 0711512002 108.86.1 SIV8260B Bromochloromethane < MDL ug/L 5.0 071152002 74.97.5 SIV8260B Bromodichloromethane < MDL ug/L 5.0 07/15/2002 75-27-4 SIV82608 Bromoform < MDL ug/L 5.0 0711512002 75.25.2 SIV8260B Bromomethane < MDL ug/L 5.0 0711512002 74-83-9 SW8260B Carbon Disulfide < MDL ug/L 5.0 0711512002 75-15-0 SIV8260B Carbon Tetrachloride < MDL ug/L 5.0 0711512002 56.23.5 SVV8260B Chloroacetonitrile <MDL- ug/L 5.0 0711512002 107.14.2 STY8260B Chlorobenzene <MDL ug/L 5.0 0711512002 108.90-7 STV8260B Chloroethane <MDL ug/L 5.0 071152002 75.00-3 SW8260B Chloroform <MDL ug/L 6.0 0711512002 67.66.3 SIV8260B Chloromethane <MDL ug/L 5.0 0711512002 74-87.3 SW8260B cis-1,2-Dichloroethene <MDL ug/L 6.0 0711512002 156-59.2 SIV8260B cis-1,3-Dichloropropene <MDL ug/L 5.0 0711512002 10061-01-5 SW8260B Dibromochloromethane < MDL ug/L 5.0 0711512002 124-48-1 SW8260B Dibromomethane < MDL ug/L 5.0 071152002 74-95-3 SW8260B Dichlorodifluoromethane < MDL ug/L 5.0 0711512002 75-71-8 SW8260B Diethyl Ether < MDL ug/L 5.0 0711512002 60-29-7 SIV8260B Ethyl Methacrylate < MDL ug/L 5.0 0711512002 97-63.2 SW8260B Euylbenzene < MDL ug/L 5.0 0711512002 100.41-4 SIV8260B Hexachlorobutadiene < MDL ug/L 6.0 0711512002 87-68.3 SW8260B Hexachloroethane <MDL ug/L 5.0- 0711512002 67-72.1 SW82608 lodomethane <MDL ug/L 5.0 0711512002 74-88-4 SIV8260B Isopropylbenzene <MDL ug/L 6.0 071152002 98-82-8 SW8260B meta-Xylene <MDL ug/L 5.0 0711512002 108-38-3 SW8260B Methacrylonitrile <MDL ug/L 5.0 0711512002 126-98-7 SW8260B Methyl t-Butyl Ether <MDL ug/L 5.0 0711512002 1634-04-4 SW8260B Methylacrylate <MDL ug/L 5.0 071152002 96.33-3 SW8260B Methylene Chloride <MDL ug/L 5.0 071152002 75-09.2 SW8260B Methylmethacrylate < MDL ug/L 5.0 071152002 80.62-6 SW8260B n-Butylbenzene < MDL ug/L 5.0 071152002 104-51-8 SW8260B n-Propylbenzene < MDL ug/L 5.0 0711512002 103.65-1 SW8260B Naphthalene < MDL ug/L 5.0 0711512002 91-20-3 SW8260B Nitrobenzene < MDL ug/L 5.0 6711512002 98-95.3 SW8260B ortho-Xylene < MDL ug/L 5.0 0711512002 95-47-6 SW8260B para-Xylene < MDL ug/L 5.0 0711512002 106-42-3 SW8260B Pentachloroethane <MDL ug/L 5.0 07/152002 76-01.7 SW8260B Propionitrile <MDL ug/L 5.0 0711512002 107-12-0 SW8260B sec-Butylbenzene <MDL ug/L 5.0 0711512002 13S-98.8 SW8260B Styrene <MDL ug/L 5.0 0711512002 100-42-5 _ SW8260B tert-Butylbenzene <MDL ug/L 5.0 071152002 98.06-6 SW8260B iLab Sample Number........ ........... AA31 1 13 Page 2 of 3 Volatiles in Liquids,. Anah.sis PerJbrmed by.... •RLH Parameter Result Units MDL Date of Analysis CAS N Method Reference Tetrachloroethylene < MDL ug/L 5.0 0711512002 127-18.4 .SIV8260B Tetrahydrofuran < MDL ug/L 5.0 071152002 109-99-9 S1V826011 Toluene <MDL ug/L 5.0 071152002 108-88-3 SIVS2608 trans-1,2-Dichloroethene <MDL ug/L 5.0 0711512002 156-60.5 SIV8260B trans-1,3-Dichloropropene <MDL ug/L 5.0 0711512002 10061-02-6 SW826011 trans-1,4-Dichloro-2.6utene <MDL ug/L 5.0 0711512002 110-57-6 SIV8260B Trichloroethene <MDL ug/L 5.0 0711512002 79-01-6 SIV8260B Trichlorofluoromethane <MDL ug/L 5.0 0711512002 75-69.4 SIV8260B Vinyl Chloride < MDL ug/L 5.0 071152002 75.01-4 SW8260B Lab Sample Number.............................. AA31113 page 3 of 3 ADEM M(WGOMERY LABORAORY 0 O 1890.A Con,. Win. Dickinson Dr.. Montgomery. AL 36109 L,,4T 1!i+,2fin4]i0lPhnnd p!bp x 7]]�t]IX IfAnalysis Report Date of This Report... 09/04/2002 Fund Code• 521 Date ofthe Original Report.. 0 910 4/2 0 0 2 Send Report... Anne F. Cross Lob Sample ID: AA31186 Source... SW-HSB-05 02 Location... WEST HUNTSVILLE CLEANERS Collection Date: 3:10:00 PM Sample MCurix: SWATER Submittal Time: 07/19/ 00 Submittal Date: 07/19/2002 Sample Collector: AFCross-AnneCross Submittal Time: 10:15:00 AM Sample Received by: C. D.AMMONS Date Analysis Validated... 09/03/2002 by WBB The results on lire attached report are from lire sample that was received and is referenced above. The sample was analyzed using standard EPA testing procedures and quality analysis protocol. Instrument calibration and quality control are within acceptable limits of precision and accuracy. A close review by our Quality Assurance Program certifies that all prescribed test hold times were met and our strict quality assurance standards were observed. Submittedby: Quality Assurance Manager ADEM's Central Laboratory has met all Requirements far Certification by EPA Region Four to Analyze Samples for all of the Parameters Required Under the Safe Drinking Water Act Trace Metals Analysis Performed by.... ADC Parameter Result Units MDL Date of Analysis CAS# Method Reference Arsenic, Total < MDL ug/L 10.0 . 0910312002 7440-38-2 EPA206.2 Cadmium, Total <MDL mg/L 0.087 091032002 7440-43-9 EPA200.7 Chromium, Total <MDL mglL 0.079 0910312002 7440-47-3 EPA200.7 Lead, Total <MDL uglL 2.00 091032002 7439-92-1 EPA239.2 Mercury, Total <MDL uglL 0.3 08/0911002 7439-97-6 EPA245.2 Volatiles in Liquids Anal-vsis Performed by.... RL.H Parameter Result Units MDL Date of Analysis CAS# Method Reference 1,1,1,2-Tetrachloroethane <MDL ug/L 5.0 0712212002 630.20.6 SW8260B 1,1,1-Trichloroethane <MDL ug/L 5.0 0712212002 71-55-6 SW8260B 1,1,2,2-Tetrachloroethane <MDL ug/L 5.0 0712212002 79-34-5 SW8260B 1,1,2-Trichloroethane <MDL ug/L 6.0 07)2212002 79-00-5 SW8260B 1,1-Dichloroethane <MDL ug/L 5.0 0712212002 75.34.3 SW8260B 1,1-Dichloroethene <MDL ug/L 6.0 0712212002 75.35-4 . SW8260B 1,1-Dichloropropanone <MDL ug/L 5.0 071222002 613.88-2 SW8260B 1,1-Dichloropropene <MDL ug/L 5.0 07222002 $63-58-6 SW8260B 1,2,3-Trlchlorobenzene <MDL ug/L 5.0. 07222002 87-61-6 SW8260B 1,2,3-Tichloropropane <MDL uglL 5.0 07222002 96-18-4 SW8260B 1,2,4-Trichlorobenzene <MDL _ ug/L 5.0 07222002 120.82-1 SW8260B 1A4-Trimethylbenzene <MDL uglL 5.0 07222002 95-63-6 SW8260B 1,2-Dibroma-3-Chloropropane <MDL ug/L 5.0 07222002 96-12.8 SW8260B 1,2-Dibromoethane(EDB) <MDL uglL 5.0 07222002 106-93-4 SW8260B 1,2-Dichlorobenzene <MDL uglL 5.0 07222002 95-50-1 SW8260B 1,2-Dichloroethane <MDL ug/L 5.0 07222002 107-06-2 SW8260B 1,2-Dichloropropane <MDL uglL 5.0 0712212002 78-87-5 SW8260B 1,3,5-Trimethylbenzene <MDL ug/L 5.0 071222002 108.67-8 SW8260B _ 1,3-Dichlorobenzene <MDL ug/L 5.0 07222002 541-73-1 SW8266B 1,3-Dichloropropane <MDL uglL 5.0 071222002 142-28-9 SW8260B Lab Sample Number............. ..... AA31186 page 1 of 3 ➢}ladles in Liquie Anah'si., Per/firmed Irv... HLH Parameter io Result Lnitc VIDL Date af.1n is CAS# Alethod Rererence 1,4-Dichlorobenzene < MDL ug/L 5.0 0712212002 106-46-7 .SIV82608 1-Chlorobutane < MDL ug/L 5.0 0712212002 109-69.3 SW826011 2,2-Dichloropropane < MDL ug/L 5.0 0712212002 590-20.7 SIV82608 2-Butanone < MDL ug/L 5.0 0712212002 78-93.3 ,S1V8260B 2-Chlorotoluene < MDL ug/L 5.0 0712212002 95-49-8 SIV8260B 2-Hexanone < MDL ug/L 5.0 0712212002 591-78-6 SIV8260B 2-Nitropropane < MDL ug/L 5.0 071222002 79-46.9 SIVS260B 4-Chlorotoluene < MDL ug/L 5.0 0712212002 106-43.4 SIV8260B 4-Isopropyltoluene < MDL ug/L 5.0 0712212002 99.87.6 SIV8260B 4-Methyl-2-pentanone(MIBK) < MDL ug/L 5.0 0712212002 108-10-1 SIV8260B Acetone < MDL ug/L 10.0 071222002 67-64-1 SW8260B Acrylonitrile < MDL ug/L 5.0 071222002 107-13-1 SVV8260B Ally Chloride < MDL ug/L 5.0 0712212002 107-05-1 SIV8260B Benzene . < MDL ug/L 5.0 071222002 71.43-2 SIV8260B Bromobenzene < MDL ug/L 5.0 0712212002 108.86-1 STY8260B Bromochloromethane < MDL ug/L 5.0 0712212002 74-97-5 SIV8260B Bromodichloromethane < MDL ug/L 5.0 071222002 75-27.4 SIV82608 Bromotorm < MDL ug/L 5.0 071222002 75-25-2 SVV8260B Bromomethane < MDL ug/L 5.0 071222002 74-83.9 SIV8260B Carbon Disulfide < MDL ug/L 5.0 0712212002 75-15-0 SIV8260B Carbon Tetrachloride < MDL ug/L 5.0 0712212002 56-23-5 SIV8260B Chloroacetonitrile < MDL ug/L 5.0 07222002 107-14-2 SIV8260B Chlorobenzene < MDL ug/L 5.0 0712212002 108-90-7 SW8260B Chloroethane < MDL ug/L 5.0 072212002 75-00.3 SW8260B Chloroform < MDL ug/L 5.0 0712212002 67.66-3 SW8260B Chloromethane < MDL ug/L 5.0 072212002 74.87-3 SW8260B cis-1,2-Dichloroethene < MDL ug/L 5.0 072212002 156-59.2 SIV8260B cis-1,3-Dichloropropene <MDL ug/L 5.0 07222002 10061-01.5 SW8260B Dibromochloromethane < MDL ug/L 5.0 071222002 124.48.1 SW8260B Dibromomethane < MDL ug/L 5.0 07222002 74-95-3 SW8260B Dichlorodifluoromethane < MDL ug/L 5.0 072212002 75-71-8 SW82608 Diethyl Ether <MDL ug/L 5.0 07222002 60.29-7 SW8260B Ethyl Methacrylate <MDL ug/L 5.0 07222002 97-63-2 SW8260B Ethylbenzene <MDL ug/L 5.0 07222002 100-41.4 SW8260B Hexachlorobutadiene <MDL ug/L 5.0 07222002 87-68-3 SIV8260B Hexachloroethane < MDL ug/L 5.0 07222002 67-72.1 SW8260B lodomethane < MDL ug/L 5.0 07222002 74-88.4 SIY8260B Isopropylbenzene < MDL uglL 5.0 07222002 - 98-82-8 SW8260B meta-Xylene <MDL uglL 5.0 07222002 108-38.3 SW8260B Methacrylonitrile <MDL ug/L 5.0 071222002 126-98-7 SW8260B Methyl t-Butyl Ether <MDL ug/L 5.0 07222002 1634-04-4 SW8260B Methylacrylate <MDL ug/L 5.0 07222002 96-33-3 SW8260B Methylene Chloride < MDL ug/L 5.0 07222002 75-09-2 SW8260B Methylmethacrylate < MDL uglL 5.0 07222002 80-62-6 SW8260B n-Butylbenzene <MDL ug/L 5.0 07222002 104-51.8 SW8260B n-Propylbenzene <MDL ug/L 5.0 07222002 - 103-65-1 SW8260B Naphthalene <MDL uglL S.C. 071222002 91-20-3 SW8260B Nitrobenzene <MDL uglL 5.0 071222002 98-95-3 SW8260B ortho-Xylene <MDL ug/L 5.0 07222002 95-47.6 SW82608 para-Xylene <MDL uglL . 5.0 072212002 106.42-3 SW8260B Pentachloroethane < MDL ug/L 5.0 07222002 76.01-7 SW8260B Propionitrile < MDL ug/L 5.0 07222002 107-12-0 SW8260B sec-Butylbenzene < MDL ug/L 5.0 07222002 135-98-8 SW8260H Styrene <MDL ug/L 5.0 07222002 100-42-5 SW8260B tert-Butylbenzene <MDL uglL 5.0 07222002 98-06-6 SW8260B Lab Sample Number.............................. AA31186 page 2 of 3 Volutiles in Liql Analysis Perjhrn,ed 1>y RLH Parameter I* Result Unit.+ MDL Data of'. ysis CAS# Method Reference Tetrachloroethylene <MDL ug/L 5.0 0712212002 127.18.4 SIV82608 Tetrahydroturan <MDL ug/L 5.0 0712212002 109-99-9 SIVS2608 Toluene < MDL ug/L 5.0 07122/2002 108.88.3 SW826011 trans-1,2-Dichloroethene < MDL ug/L 5.0 0712212002 156-60-5 SW8260B trans-1,3-Dichloropropene < MDL ug/L 5.0 0712212002 10061.02-6 SIV82608 trans-1,4-Dichloro-2-butene < MDL ug/L 5.0 0712212002 110.57.6 SVV'82608 Trichlorcethene < MDL ug/L 5.0 0712212002 79-01-6 SIV3260B Trichlorotluoromethane < MDL ug/L 5.0 072212002 75-69-4 SIV8260B Vinyl Chloride < MDL ug/L 5.0 0712212002 75-01-4 SW82608 Lab Sample Number AA31186 page 3 of 3 ADEM MOTGOMERY LABORAORY 00 1890-A Cang. Wm. Dickinson Dr.. Montgomery. AL 36109 LSA (33J)-'-h0-277010hum1 03s1-'-77.87181Fasl • � t't Analysis Report e.T Date of This Report.. 09/04/2002 Fund Code- 521 Date of the Original Report.. 09/04/2002 Send Resort.. Anne F.Cross Lab Sample ID: AA31185 Source... SD-UNT-10 Location... WEST HUNTSVILLE CLEANERS Collection Date: 07/17/2002 Sarnsle Matrix: SEDIMENT Collection Time: 5:10:00 PM Submittal Date: 07/19/2002 Sample Collector., AFCross-AnneCross Submittal Time: 10:15:00 AM Sample Received by: C. D.AMMONS Date Analvsis Validated... 09/04/2002 by W BB The results on the attached report are from the sample that was received and is referenced above. The sample was analyzed using standard EPA testing procedures and quality analysis protocol Instrument calibration and quality control are within acceptable limits of precision and accuracy. A close review by our Quality Assurance Program certifies that all prescribed test hold time.,were met and our spice quality assurance standards were observed. Submitted by: 2?(&Seazk A1, Quality Assurance Manager ADEM's Central Laboratory has met all Requirements far Certification by EPA Region Four to Analyze Samples fur all of the Parameters Required Under the Safe Drinking Water Act Trace Metals Analvsis Performed by.... ADC Parameter Result Units MDL Date of Analysis CAS# Method Reference Arsenic, Total <MDL ug/g 10.0 0910312002 7440-38-2 EPA200.7 Cadmium, Total <MDL ug/g 1.0 0910312002 7440.43-9 EPA200.7 Chromium, Total < MDL ug/g 1.5 0910312002 7440.47-3 EPA200.7 Lead, Total <MDL ug/g 10.0 0910312002 7439.92.1 EPA200.7 Mercury, Total <MDL ug/g 0.10 0910*2002 7439-97-6 EPA245.5 Volatiles in Solids Analvsis Performed by.... RLH _Parameter Result Units MDL Date of Analysis CAS# Method Reference 1,1,1,2-Tetrachloroethane <MDL ugfg 0.05 07222002 630-20-6 SW8260B 1,1,1-Trlchloroethane <MDL ug/g 0.06 07222002 71-55.6 SW8260B 1,1,2,2-Tetrachloroethane <MDL ugfg 0.05 07)222002 79-34-5 SW8260B 1,1,2-Trichloroethane <MDL ug/g 0.05 07222002 79.00.5 SW8260B 1,1-Dichloroethane <MDL ug/g 0.06 071222002 75.34-3 SW8260B 1,1-Dichloroethene <MDL ug/g 0.06 07222002 75.354 SW8260B 1,1-Dichloropropanone <MDL ug/g 0.05 072212002 513-88-2 SW8260B 1,1-Dichloropropene <MDL ug/g 0.05 07222002 563-58-6 SW8260B 1,2,3-Trichlorobenzene <MDL ug/g 0.05 07222002 87-61-6 SW8260B 1,2,3-Trlchloropropane <MDL ug/g 0.05 07222002 96-18.4 SW8260B 1,24-Trichlorobenzene <MDL ug/g 0.05 07222002 120-82.1 SW8260B 1,2,4-Trimethylbenzene <MDL ug/g 0.05 07222002 95-63-6 SW8260B 1,2-Dibromo-3-Chloropropane <MDL uglg 0.05 072212002 96-12.8 SW8260B 1,2-Dibromoethane(EDB) <MDL ug/g 0.05 07222002 106.93.4 SW8260B 1,2-Dichlorobenzene < MDL ug/g 0.06 07222002 95-50.1 SW8260B 1,2-Dichloroethane < MDL ug/g 0.05 07222002 107-06-2 SW8260B 1,2-Dichloropropane < MDL uglg 0.06 07222002 78.87.5 SW8260B 1,3,5-Trimethylbenzene <MDL ug/g 0.05 07222002 108.67-8 SW8260B 1,3-Dichlorobenzene <MDL ugfg 0.05 07222002 641-73-1 SW8260B 1,3-Dichloropropane <MDL ug/g 0.05 07222002 142-28-9 SW8260D Lab Sample Number..........0................... AA31185 page 1 of 3 Volariles in Solids* Anal)'sis Performed bi....• RLH Parameter Result Units VIDL Date ofAnalvsi, CAS N Method Reference 1,4-Dichlorobenzene < MDL ug/g 0.05 0712212002 106-46.7 SIY8260B 1-Chlorobutane <MDL ug/g 0.05 0712212002 109.69-3 SW82608 2,2-Dichloropropane <MDL ug/g 0.05 0712212002 590.20.7 SW8260B 2-Butanone < MDL ug/g 0.05 0712212002 78-93.3 SIV8260B 2-Chlorotoluene < MDL ug/g 0.05 071222002 95.49-8 SW8260B 2-Hexanone <MDL ug/g 0.05 072212002 591-78-6 SIV8260B 2-Nitropropane < MDL ug/g 0.05 071222002 79.46-9 SW8260B 4-Chlorotoluene < MOL ug/g 0.05 072212002 106-43.4 SIV8260B 4-lsopropyltoluene < MDL ug/g 0.05 072212002 99-87.6 SW8260B 4-Methyl-2-pentanone(MIBK) <MDL ug/g 0.05 0712212002 108.10-1 SIV8260B Acetone < MDL ug/g 0.05 0712212002 67.64-1 SIV8260B Acrylonitrile < MDL ug/g 0.05 072212002 107-13-1 SW8260B Ally Chloride < MDL ug/g 0.05 071222002 107.05-1 SW8260B Benzene <MDL ug/g 0.05 07/222002 71.43-2 SIV8260B Bromobenzene <MDL ug/g 0.05 072212002 108-86-1 SW8260B Bromachloromethane < MDL ug/g 0.05 07222002 74-97-5 SIV8260B Bromodichloromethane < MDL ug/g 0.05 0712212002 75-27-4 STV8260B Bromoform <MDL ug/g 0.05 07222002 75.25-2 SW8260B Bromomethane <MDL ug/g 0.05 072212002 74-83.9 SW8260B Carbon Disulfide <MDL ug/g 0.05 07222002 75-15-0 SW8260B Carbon Tetrachloride < MDL ug/g 0.05 071222002 56.23-5 SW8260B Chloroacetonitrile <MDL ug/g 0.05 072212002 107-14.2 SW8260B Chlorobenzene <MDL ug/g 0.05 072212002 108-90-7 SIV8260B Chloroethane <MDL ug/g 0.05 071222002 75.00-3 SW8260B Chloroform <MDL ug/g 0.05 07222002 67-66-3 SW8260B Chloromethane <MDL ug/g 0.05 072212002 74-87.3 SW8260B cis-1,2-Dichloroethene <MDL ug/g 0.05 072212002 156-59-2 SW8260B cis-1,3-Dichloropropene <MDL ug/g 0.05 071222002 10061-01-5 SW82608 Dibromochloromethane <MDL ug/g 0.05 07222002 124.48-1 SW8260B Dibromomethane <MDL ug/g 0.05 07222002 74-95-3 SW8260B Dichlorodifluoromethane < MDL ug/g 0.05 072212002 75-71-8 SW8260B Diethyl Ether <MDL ug/g 0.05 07222002 60-29-7 SW8260B Ethyl Methacrylate <MDL ug/g 0.05 07222002 97-63-2 SW8260B Ethylbenzene <MDL ug/g 0.05 07222002 100.41-4 SW8260B Hexachlorobutadiene <MDL ug/g 0.05 07222002 87-68-3 SW8260B Hexachloroethane <MDL ug/g 0.05 07222002 67-72.1 SW8260B lodomethane <MDL ug/g 0,05 07222002 74.88-4 SW8260B Isopropylbenzene <MDL ug/g 0.05 07222002 98-82-8 SW8260B meta-Xylene <MDL ug/g 0.05 07222002 108-38-3 SW82608 Methecrylonitrile <MDL ug/g 0.05 07222002 126-98-7 SW8260B Methyl t-Butyl Ether <MDL ug/g 0.05 07222002 1634-04-4 SW8260B Methylacrylate <MDL ug/g 0.05 071222002 96-33-3 SW8260B Methylene Chloride <MDL ug/g 0.05 07222002 75-09-2 SW8260B Methylmethacrylate <MDL ug/g 0.05 072212002 80-62-6 SW8260B n-Butylbenzene <MDL ug/g 0.05 07222002 104-51-8 SW8260B n-Propylbenzene <MDL ug/g 0.05 07222002 103-65-1 SW8260B Naphthalene <MDL ug/g 0.05 07222002 91-20-3 SW82608 Nitrobenzene <MDL ug/g 0.05 07222002 98-95-3 SW8260B prtho-Xylene <MDL ug/g 0.05 07222002 95-47-6 SW8260B para-Xylene <MDL ug/g 0.05 072212002 106.42-3 SW8260B Pentachloroethane <MDL ug/g 0.05 07222002 76-01-7 SW8260B Propionitrile <MDL ug/g 0.05 072212002 107-12-0 SW8260B sec-Butylbenzene <MDL ug/g 0.05 07222002 135-98-8 SW82608 Styrene <MDL ug/g 0.05 07222002 100-42.5 SW8260B tert-Butylbenzene <MDL ug/g 0.05 07222002 98-06.6 SW8260B Lab Sample Number.............................. AA31 185 Page 2.ot 3 Volatiles in Solid* Analysis Performed by.... RLH Parameter Result Units MDL Date o, At+aas CAS k Method Reference Tetrachloroethylene < MDL ug/g 0.05 0712212002 127-18.4 SW82608 Tetrahydrofuran < MDL ug/g 0.05 0712212002 109-99-9 SW8260B Toluene <MDL ug/g 0.05 0712212002 108.88-3 SW82608 trans-1,2-Dichloroethene <MDL ug/g 0.05 0712212002 156-60-5 SW8260B trans-1,3-Dichloropropene <MDL ug/g 0.05 0712212002 10061.02-6 SW8260B trans-1,4-Dichloro-2-butene <MDL ug/g 0.05 0712212002 110.57-6 SW8260B Trichloroethene < MDL ug/g 0.05 0712212002 79-01-6 SW8260H Trichlorofluoromethane < MDL ugig 0.05 0712212002 75-69.4 SW8260B Vinyl Chloride < MDL ug/g 0.05 0712212002 75.01-4 SW8260B i i Lab Sample Number.............................. AA31 185 page 3 of 3 a ADEM M(OTGOMERY LABORAODRY 1890-A Cong. W m.Dickinson Dr..Montgomery.AL 36109 T �9 1334�2hM127701phonc 1 013)-277-e]Ie[Fa,I 1 t- O Analysis Report4T Date oJThis Report... 09/04/2002 Fend Code, 521 Date of the Original Report.. 09/04/2002 Send Report... Anne F. Cross Lab Sample ID: AA31184 Source... SD-UNT-09 Location... WEST HUNTSVILLE CLEANERS Collection Date: 07/17/2002 Collection Tinge: 4:15:00 PM Sample Matrix: SEDIMENT Submittal Date: 07/19/2002 Sample Collector: AFCross-AnneCross Submittal Time: 10:15:00 AM Sample Received by: C. D.AMMONS Date Analvsis Validated... 09/04/2002 by WBB The results on the punched report are from the sample that was received and is referenced above. The sample was analyzed using standard EPA testing procedures and quality analysis protocol. Instrument calibration and quality control are within acceptable limits of precision and accuracy. A close review by our Quality Assurance Program certifies that all prescribed lest hold time,were met and our strict quality assurance standards were observed. Submitted by: Rill %?etCk, , Quality Assurance Manager ADEM's Central Laboratory has met all Requirements for Certifutadon by EPA Region Four to Analyze Samples for all of the Parameters Required Under the Safe Drinking Water Act. Trace Metals Analvsis Performed by.... ADC Parameter Result Units MDL Date of Analysis CAS# Method Reference Arsenic, Total <MDL ug/g 10.0 0910312002 7440-38-2 EP4200.7 Cadmium, Total <MDL ug/g 1.0 0910312002 7440.43.9 EPA200.7 Chromium, Total <MDL ug/g 1.5 09/03/2002 7440.47-3 EPA200.7 Lead, Total <MDL ug/g 10.0 0910312002 7439.92-1 EPA200.7 Mercury, Total <MDL ug/g 0.10 0910412002 7439.97-6 EPA245.5 Volatiles in Solids Analvsis Performed by.... RLH Parameter Result Units MDL Date of Analysis CAS# Method Reference 1,1,1,2-Tetrach/oroethane <MDL ug/g 0.05 071220002 630-20-6 SW8260B 1,1,1-Trich/oroethane <MDL ug/g 0.05 07)2212002 71-55-6 SW8260B 1,1,2,2-Tetrachlorcethane <MDL ug/g 0.05 07122,2002 79.34-5 SW8260B 1,1,2-Trichlaroethane <MDL ug/g 0.05 07222002 79.00-5 SW8260B 1,1-Dichloroethane <MDL ug/g 0.05 071222002 75.34-3 SW8260B 1,1-Dichloroethene <MDL ug/g 0.05 07222002 75-35.4 SW8260B 1,1-Dichloropropanone <MDL ug/g 0.05 07222002 513.88.2 SW8260B 1,1-Dichloropropene <MDL ug/g 0.05 072212002 563-58-6 SW8260B 1,2,3-Trichlorobenzene <MDL ug/g 0.05 07222002 87-61-6 SW8260B 1,2,3-Tichloropropane _<MDL ug/g 0.05 07222002 96-18.4 SW8260B 1,2,4-Trichlorobenzene <MDL ug/g 0.05 07222002 120.82-1 SW8260B 1,2,4-Trimethylbenzene <MDL ug/g 0.05 07222002 95-63-6 SW8260B 1,2-Dibromo-3-Chloropropane <MDL ug/g 0.05 07222002 96-12.8 SW8260B 1,2-Dibromoethane(EDB) < MDL ug/g 0.05 07222002 106-93-4 SW8260B 1,2-Dichlorobenzene < MDL ug/g 0.05 0712212002 95-50-1 SW8260B 1,2-Dichloroethane < MDL ug/g 0.05 07222002 107.06-2 SW8260B 1,2-Dichloropropane <MDL ug/g 0.05 071222002 78-87-5 SW8260B 1,3,5-Trimethylbenzene <MDL ug/g 0.05 071222002 108-67-8 SW8260D 1,3-Dichlorobenzene <MDL ug/g 0.05 07222002 541-73-1 SW82608 1,3-Dichloropropane <MDL ug/g 0.05 07222002 142.28-9 SW8260B Lab Sample Number.............................. AA31 184 page 1 of 3 Parameter Vo lutiles in Solid 0 Ann/e.ris Performed by... RLH Result U its MDL Date o(An�'. CAS# Method od Reference 1,4-Dichlorobenzene < MDL ug/g 0.05 0712212002 106-46-7 SW82608 1-Chlorobutane <MDL ug/g 0.05 071222002 109-693 SW8260B 2,2-Dichloropropane < MDL ug/g 0.05 0712212002 590-20-7 SW8260H 2-Butanone < MDL ug/g 0.05 071222002 78-93-3 SIV8260B 2-Chlorotoluene <MOL ug/g 0.05 0712212002 95.49-8 SW8260B 2-Hexanone < MDL ug/g 0.05 072212002 591-78.6 SW8260B 2-Nitmpropane < MDL ug/g 0.05 072212002 79.46-9 SW82608 4-Chlorotoluene < MDL ug/g 0.05 071222002 106-43-4 SW8260B 4-Isopropyltoluene < MDL ug/g 0.05 072212002 99.87-6 SW8260B 4-Methyl-2-pentanone(MIBK) < MDL ug/g 0.05 0722/2002 108-10.1 SW8260B Acetone <MDL ug/g 0.05 0712212002 67-64.1 SW8260B Acrylonitrile < MDL ug/g 0.05 072212002 107-13-1 SW8260B Ally Chloride < MDL ug/g 0.05 072212002 107-05.1 SW8260B Benzene < MDL ug/g 0.05 071222002 71-43.2 SW8260B Bromobenzene <MDL ug/g 0.05 072212002 108-86-1 SW8260B Bromochloromethane < MDL ug/g 0.05 071222002 74-97.5 SW8260B Bromodichloromethane < MDL ug/g 0.05 072212002 75.27-4 SW8260B Bromoform <MDL ug/g 0.05 07222002 75-25.2 SW82608 Bromomethane < MDL ug/g 0.05 071222002 74.83.9 SW8260B Carbon Disulfide < MDL ug/g 0.05 072212002 75-15-0 SW8260B Carbon Tetrachloride <MDL ug/g 0.05 07222002 56-23-5 SW82608 Chloroacetonitrile <MDL ug/g 0.05 07222002 107.14-2 SW8260B Chlorobenzene < MDL ug/g 0.05 072212002 108.90-7 SW8260B Chloroethane < MDL ug/g 0.05 072212002 75.00-3 SW8260B Chloroform <MDL ug/g 0.05 07222002 67-66.3 SW8260B Chloromethane <MDL ug/g 0.05 072212002 74.87-3 SW8260B cis-1,2-Dichloroethene < MDL ug/g 0.05 072212002 156-59.2 SW8260B cis-1,3-Dichloropropene <MDL ug/g 0.05 07222002 10061-01-5 SW82608 Dibromochloromethane <MDL ug/g 0.05 07222002 124-48-1 SW8260B Dibromomethane < MDL ug/g 0.05 07222002 74-95-3 SW8260B Dichlorodifluoromethane <MDL ug/g 0.05 07222002 75-71.8 SW8260B Diethyl Ether <MDL ug/g 0.05 07222002 60.29.7 SW8260B Ethyl Methacrylate <MDL ug/g 0.05 07222002 97-63-2 SW8260B Ethylbenzene <MDL ug/g 0.05 07222002 100-41-4 SW8260B Hexachlorobutadiene <MDL ug/g 0.05 07222002 87-68.3 SW8260B Hexachloroethane <MDL ug/g 0.05 0722/2002 67.72.1 SW8260B lodomethane <MDL ug/g 0.05 07222002 74-88.4 SIV8260B Isopropylbenzene <MDL ug/g 0.05 07222002 98-82.8 SW8260B meta-Xylene < MDL ug/g 0.05 07222002 108-38-3 SW8260B Methacrylonitrile <MDL ug/g 0.05 07222002 126-98-7 SW8260B Methyl t-Butyl Ether <MDL ug/g 0.05 07222002 1634.04-4 SW8260B Methylacrylate <MDL ug/g 0.05 07222002 96-33-3 SW8260B Methylene Chloride < MDL ug/g 0.05 07222002 75.09-2 SW8260B Methylmethacrylate < MDL ug/g 0.05 07/222002 80.62-6 SW8260B n-Butylbenzene < MDL ug/g 0.05 07222002 104-51-8 SW8260B n-Propylbenzene -<MDL ug/g 0.05 07222002 103-65-1 SW8260B Naphthalene <MDL ug/g 0.05 07222002 91-20.3 SW8260B Nitrobenzene <MDL ug/g 0.05 072212002 98-95.3 SW8260B .ortho-Xylene <MDL ug/g 0.05 07222002 95.47-6 SW8260B Para-Xylene < MDL ugfg 0.05 07222002 106-42.3 SW8260B Pentachloroethane <MDL ug/g 0.05 07222002 76-01-7 SW8260B Propionitrile <MDL ug/g 0.05 07222002 107-12.0 SW8260B sec-Butylbenzene <MDL ug/g 0.05 072212002 135-98.8 SW8260B Styrene <MDL ug/g 0.05 07222002 100.42-5 SW8260B tert-Butylbenzene <MDL ug/g 0.05 07222002 98.06.6 SW8260B Lab Sample Number........................ AA31 184 page 2 of 3 Volutiles in Solid.* Analysis Performed bs....• RLH Parameter Result Units' MDL Date ofAnalysls CAS# Method Reference Tetrachloroethylene < MDL ug/g 0.05 0712212002 127-18-4 SW8260B Tetrahydrofuran <MDL ug/g 0.05 0712212002 109-99-9 SW8260B Toluene <MDL ug/g 0.05 0712212002 108-88-3 SW8260B trans-1,2-Dichloroethene < MDL ug/g 0.05 0712212002 156.60-5 SW8260B trans-1,3-Dichloropropene < MDL ug/g 0.05 0712212002 10061-02-6 SW8260B trans-1,4-Dichloro-2-butene < MDL ug/g 0.05 0712212002 110-57-6 SW8260B Trichloroethene < MDL ug/g 0.05 0712212002 79-01.6 SW8260B Trichlorofluoromethane < MDL ug/g 0.05 0712212002 75-69-4 SW8260B Vinyl Chloride < MDL ug/g 0.05 0712212002 75-01.4 SW8260B Lab Sample Number AA31 184 page 3 of 3 ADEM M4KTGOMERY LABOR*ORY oa 1890-A Cong.Wm. Dickinson Dr., Montgomery.AL 36109 f.8 (334)-260,2770IPhnnd (334)-277b718[Fuel • �:. 01 Analysis Report Date of This Report.. 09/03/2002 Fund Code: 521 Date of the Original Report.. 09/03/2002 Send Report... Anne F.Cross Lab Sample ID: AA31123 Source... SD-BS-02 Location... WEST HUNTSVILLE CLEANERS Collection Dale: 12: 1:0002 Sample Matrix: SEDIMENT Collection Time: 12 12/0 PM Submittal Date: 10:45:00 A Sample Collector: AFCross-AnneCross Submittal Time: 10:45:00 AM Sample Received by: C,D.AMMONS Date Analysis Validated... 09/03/2002 fic CDA The results on the attached report are from the sample that was received and is referenced above. The sample was analyzed using standard EPA testing procedures and quality analysis protocol Instrument calibration and quality control are within acceptable limits of precision and accuracy. A Nose review by our Quality Assurance Program certifies that all prescribed test hold tines were met and our strict quality assurance standards were observed. Submitted by: &Z geZ CE4U, Quality Assurance Manager ADEM's Central laboratory has met all Requirements for Certification by EPA Region Four to Analyze Samples for all of the Parameters Required Under the Safe Drinking Water Act. Trace Metals Analysis Performed by.... ADC Parameter Result Units MDL Date of Analysis CAS# Method Reference Arsenic, Total <MDL ug/g 10.0 09/032002 7440.38-2 EPA200.7 Cadmium, Total <MDL ug/g 1.0 091032002 7440.43.9 EPA200.7 Chromium, Total <MDL ug/g 1.5 091032002 7440-473 EPA200.7 Lead, Total <MDL ug/g 10.0 091032002 7439-92-1 EPA200.7 Mercury, Total <MDL ug/g 0.10 071162002 7439-97-6 EPA245.5 Volatiles in Solids Analysis Performed by.... RLH Parameter Result Units MDL Date of Analysis CAS# Method Reference 1,1,1,2-Tetrachloroethane < MDL ug/g 5.0 071172002 630.20.6 SW8260B 1,1,1-Trichloroethane < MDL ug/g 5.0 07/172002 71-55.6 SW8260B 1,1,2,2-Tetrachloroethane < MDL ug/g 5.0 07/172002 79-34.5 SW8260B 1,1,2-Trichloroethane < MDL ug/g 5.0 071172002 79-00.5 SW8260B I,1-Dichloroethane < MDL ug/g 5.0 071172002 75-34.3 SW8260B 1,1-Dichloroethene < MDL ug/g 5.0 071172002 76-35-4 SW8260B 1,1-Dichloropropanone < MDL ug/g 5.0 071172002 613.88.2 SW8260B 1,1-Dichloropropene < MDL ug/g 5.0 071172002 563-58-6 SW8260B 1,2,3-Trichlorobenzene < MDL ug/g 5.0 071172002 87.61-6 SW8260B 1,2,3-Trichloropropane <MDL ug/g 5.0 071172002 96-18-4 SW8260B 1,2,4-Trichlorobenzene <MDL uglg 5.0 071172002 120-82-1 SW8260B 1,2,4-Trimethylbenzene <MDL ug/g 5.0 071172002 95-63-6 SW8260B 1,2-Dibromo-3-Chloropropane <MDL ug/g 5.0 071172002 96.12-8 SW8260B 1,2-Dibromoethane(EDS) <MDL ug/g 6.0 071172002 106-93-4 SW8260B 1,2-Dichlorobenzene <MDL ug/g 5.0 071172002 95-50-1 SW8260B 1,2-Dichloroethane <MDL ug/g 5.0 0711712002 107-06-2 SW8260B 1,2-Dichloropropane <MDL ug/g 5.0 071172002 78.87-5 SW8260B 1,3,5-Trimethylbenzene <MDL ug/g 5.0 071172002 108-67-8 SW8260B 1,3-Dichlorobenzene <MDL ug/g 5.0 071172002 541-73-1 SW8260B 1,3-Dichloropropane <MDL ug/g 5.0 071172002 142-28-9 SW8260B Lab Sample Number.............................. AA31 123 Page 1 of 3 Volettiles in Solids• Analysis Performed Gv....• RLH Parameter Result Units AIDL Date of Analysis CAS N I'lethod Reference 1,4-Dichlorobenzene < MDL ug/g 5.0 0711712002 106-46.7 SW8260B 1-Chlorobutane < MDL ug/g 5.0 0711712002 109-69-3 SIV8260B 2,2-Dichloropropane < MDL ug/g 5.0 0711712002 590.20-7 SW82608 2-Butanone < MDL ug/g 5.0 0711712002 78-93-3 SIV8260B 2-Chlorotoluene < MDL ug/g 5.0 0711712002 95-49-8 SW8260B 2-Hexanone < MDL ug/g 5.0 0711712002 591-78.6 SIV8260B 2-Nitropropane < MDL ug/g 5.0 0711712002 79-46.9 SW8260B 4-Chlorotoluene < MDL ug/g 5.0 0711712002 106.43-4 SW8260B 4-Isopropyltoluene < MDL ug/g 5.0 0711712002 99-87-6 SIV8260B 4-Methyl-2-pentanone(MIBK) < MDL ug/g 5.0 0711712002 108-10-1 SIV8260B Acetone < MDL ug/g 5.0 0711712002 67.64-1 SW8260B Acrylonitrile < MDL ug/g 5.0 0711712002 107-13-1 SW8260B Ally Chloride < MDL ug/g 5.0 0711712002 107-05-1 SW8260B Benzene < MDL ug/g 5.0 0711712002 71-43-2 SW8260B Bromobenzene < MDL ug/g 5.0 0711712002 108.86-1 SW8260B Bromochloromethane <MDL ug/g 5.0 0711712002 74-97-5 SW8260B Bromodichloromethane < MDL ug/g 5.0 0711712002 75.27-4 SW8260B Bromoform < MDL ug/g 5.0 0711712002 75-25.2 SW8260B Bromomethane < MDL ug/g 5.0 0711712002 74-83.9 SW8260B Carbon Disulfide < MDL ug/g 5.0 0711712002 75-15-0 SW8260B Carbon Tetrachloride < MDL ug/g 5.0 0711712002 56-23-5 SW8260B Chloroacetonitrile < MDL ug/g 6.0 0711712002 107-14-2 SW8260B Chlorobenzene < MDL ug/g 5.0 0711712002 108-90-7 SW8260B Chloroethane < MDL ug/g 5.0 0711712002 75-00-3 SW8260B Chloroform < MDL ug/g 5.0 0711712002 67-66-3 SW8260B Chloromethane < MDL ug/g 5.0 0711712002 74-87-3 SW8260B cis-1,2-Dichloroethene <MDL ug/g 5.0 0711712002 156-59-2 SW8260B cis-1,3-Dichloropropene < MDL ug/g 5.0 0711712002 10061-01-5 SW8260B Dibromochloromethane <MDL ug/g 5.0 0711712002 124-48-1 SW8260B Dibromomethane <MDL ug/g 5.0 0711712002 74-95-3 SW8260B Dichlorodifluoromethane < MDL ug/g 5.0 0711712002 75-71-8 SW8260B Diethyl Ether < MDL ug/g 5.0 0711712002 60-29-7 SW8260B Ethyl Methacrylate <MDL ug/g 5.0 0711712002 97-63-2 SW8260B Etylbenzene < MDL ug/g 5.0 0711712002 100-41-4 SW8260B Hexachlorobutadiene < MDL ug/g 5.0 0711712002 87-68-3 SW8260B Hexachloroethane < MDL ug/g 5.0 0711712002 67-72.1 SW8260B lodomethane < MDL ug/g 5.0 0711712002 74.88-4 SW8260B Isopropylbenzene < MDL ug/g 5.0 0711712002 98-82-8 SW8260B meta.Xylene < MDL ug/g 5.0 0711712002 108-38.3 SW8260B Methacrylonitrile <MDL ug/g 5.0 0711712002 126-98-7 SW8260B Methyl t-Butyl Ether <MDL ug/g 5.0 0711712002 1634-04-4 SW8260B Methylacrylate <MDL ug/g 5.0 0711712002 96-33-3 SW8260B Methylene Chloride <MDL ug/g 5.0 0711712002 75-09.2 SW8260B Methylmethacrylate <MDL ug/g 5.0 0711712002 80-62-6 SW8260B n-Butylbenzene <MDL ug/g 6.0 0711712002 104-51-8 SW8260B n-Propylbenzene <MDL ug/g 5.0 0711712002 103-66-1 SW8260B Naphthalene <MDL ug/g 5.0 0711712002 91-20-3 SW82608 Nitrobenzene <MDL ug/g 5.0 0711712002 98-95-3 SW8260B ortho-Xylene <MDL ug/g 6.0 0711712002 95.47-6 SW8260B para-Xylene <MDL ug/g 5.0 0711712002 106-42-3 SW8260B Pentachloroethane <MDL ug/g 5.0 0711712002 76.01-7 SW8260B Propionitrile <MDL ug/g 5.0 0711712002 107-12-0 SW8260B sec-Butylbenzene <MDL ug/g 5.0 0711712002 135-98.8 SW8260B Styrene <MDL ug/g 5.0 0711712002 lOG-42.5 SW8260D tert-Butylbenzene <MDL ug/g 5.0 0711712002 - 98-06.6 SW8260B Lab Sample Number.............................. AA31123 page 2 of 3 Volatiles in Solid Analysis Performed bv....• RLH Parameter Result Units MDL Date of Analysis CAS p Method Reference Tetrachloroethylene <MDL ug/g 5.0 0711712002 127-18-4 SW8260B Tetrahydrofuran <MDL ug/g 5.0 0711712002 109-99-9 SW8260B Toluene <MDL ug/g 5.0 0711712002 108-883 SW8260B trans-1,2-Dichloroethene <MDL ug/g 5.0 0711712002 156.60.5 SW8260B trans-1,3-Dichloropropene < MDL ug/g 5.0 0711712002 10061.02.6 SW82608 trans-14-Dichloro-2-butene < MDL ug/g 5.0 0711712002 110.57.6 SW8260B Trichloroethene < MDL ug/g 5.0 0711712002 79.01-6 SW8260B Trichlorofluoromethane < MDL ug/g 5.0 0711712002 75.69-4 SW8260B Vinyl Chloride < MDL ug/g 5.0 0711712002 75.01-4 SW8260B Lab Sample Number AA31123 page 3 of 3 °o ADEM M16NTGOMERY LABOR*ORY I tlgO-A Cong.Wm. Dickinson Dr.. MonLomcry.AL?6I09 (331).260-27701Phonel O3+e]77-6718 IFaxI Analysis Report p£+T Date of This Report... 09/03/2002 Fund Code- 521 Date of the Orieinal Report... 0 9/0 312 0 0 2 Send Report.. Anne F. Cross Lab Sample ID: AA31124 Source... SD-MMB-03 Location... WEST HUNTSVILLE CLEANERS Collection Date. 07/11/2002 Sample Matrix.' SEDIMENT Collection Time: 10:58:00 AM Submittal Date: 07/12/2002 Sample Collector: AFCross-AnneCross Submittal Time: 10:45:00 AM Sample Received by: C. D.AMMONS Date Analvsis Validated... 0910=002 by CDA The results on file attached report are from the sample that was receired and is referenced above. The sample was analyzed using standard EPA testing procedures and quality analysis protocol. Instrument calibration and quality control are within acceptable limits of precision and accuracy. A close review by our Quality Assurance Program certifies that all prescribed test hold time..,were met and our strict quality assurance standards were observed. Submitted by: I. ,Rru2Ck6 Quality Assurance Manager ADEAl s Central Laboratory has met all Requirements for Certification by EPA Region Four to Analyze Samples for all of the Parameters Required Under the Safe Drinking Water Act. Trace Metals Analvsis Performed by.... ADC Parameter Result Units MDL Date of Analysis CAS# Method Reference Arsenic, Total < MDL ug/g 10.0 09/03/2002 7440-38.2 EPA200.7 Cadmium, Total <MDL ug/g 1.0 091032002 7440-43-9 EPA200.7 Chromium, Total <MDL ug/g 1.5 0910312002 7440-47-3 EPA200.7 Lead, Total <MDL ug/g 10.0 0910312002 7439-92.1 EPA200.7 Mercury, Total <MDL ug/g 0.10 071162002 7439-97.6 EPA24S.5 Volatiles in Solids Analysis Performed by.... RL9 Parameter Result Units MDL Date of Analysis CAS# Method Reference_ 1,1,1,2-Tetrachloroethane <MDL ug/g 6.0 071172002 630.20.6 SW8260B 1,1,1-Trichloroethane <MDL ug/g 5.0 071172002 71-55.6 SW8260B 1,1,2,2-Tetrachloroethane <MDL ug/g 5.0 071172002 79-34.5 SW8260B 1,1,2-7'richloroethane <MDL ug/g 5.0 071172002 79.00.5 SW8260B 1,1-Dichloroethane <MDL ug/g 5.0 071172002 75-34-3 SW8260B 1,1-Dichloroethene <MDL ug/g 6.0 071172002 75.35-4 SW82605 1,1-Dichlaropropanone <MDL ug/g 6.0 071172002 513.88-2 SW8260D 1,1-Dichloropropene <MDL ug/g 5.0 071172002 563-58-6 SW8260B 1,2,3-Trichlorobenzene <MDL ug/g 5.0 071172002 87.61.6 SW8260B 1,2,3-Tichloropropane <MDL ug/g 5.0 071172002 96-18-4 SW8260B 1,2,4-Trichlorobenzene <MDL ug/g 5.0 071172002 120.82-1 SW8260B 1,2,4-Trimethylbenzene < MDL ug/g 5.0 071172002 95.63-6 SW8260B 1,2-Dibromo-3-Chloroprcpane < MDL ug/g 5.0 071172002 96-12-8 SW8260B 1,2-Dibromoethane(EDB) < MDL ug/g 5.0 071172002 106-93-4 SW8260B 1,2-Dichlorobenzene < MDL ug/g 5.0 071172002 95-50.1 SW8260B 1,2-Dichloroethane < MDL ug/g 6.0 071172002 107-06-2 SW82608 1,2-Dichloropropane < MDL ug/g 5.0 071172002 78.87-5 SW8260B 1,3,5-Trimethylbenzene < MDL ug/g 6.0 071172002 108-67.8 SW8260D 1,3-Dichlorobenzene < MDL ug/g 5.0 - 071172002 541-73-1 SW8260D 1,3-Dichloropropane < MDL ug/g 5.0 071172002 142-28-9 SW82608 Lab Sample Number.. AA31124 page 1 of 3 VO((ltlle5 Ili SO* : ....A. i., Pertbrmed bs RLH Parameter Result Units VIDL Date ofA lv''s CAS N Method Referance 1,4-Dichlorobenzene < MDL ug/g 5.0 - 0711712002 106-46-7 5VV82608 1-Chlorobutane < MDL ug/g 5.0 0711712002 109.69-3 SIV8260B 2,2-Dichloropropane < MDL ug/g 5.0 0711712002 590-20-7 SW82608 2-Butanone < MDL ug/g 5.0 0711712002 78-93-3 SW8260B 2-Chlorotoluene < MDL ug/g 5.0 0711712002 95.49-8 SIV8260B 2-Hexanone < MDL ug/g 5.0 0711712002 591-78-6 SIV8260B 2-Nitropropane < MDL ug/g 5.0 0711712002 79-46.9 SIV8260B 4-Chlorotoluene < MDL ug/g 5.0 0711712002 106-43.4 SIV8260B 4-Isopropyltoluene < MDL ug/g 5.0 0711712002 99.87-6 SIV8260B 4-Methyl-2-pentanone(MIBK) < MDL ug/g 5.0 0711712002 108.10-1 SIV8260B Acetone < MDL ug/g 5.0 0711712002 67-64.1 SW8260B Acrylonitrile < MDL ug/g 5.0 0711712002 107.13.1 SW8260B Ally Chloride < MDL ug/g 5.0 0711712002 107.05-1 SIV8260B Benzene < MDL ug/g 5.0 0711712002 71-43-2 SIV8260B Bromobenzene < MDL ug/g 5.0 0711712002 108.86-1 SIV8260B Bromochloromethane < MDL ug/g 5.0 0711712002 74-97.5 SIV8260B Bromodichloromethane < MDL ug/g 5.0 0711712002 75-27.4 SIV8260B Sromoform < MDL ug/g 5.0 0711712002 75-25.2 SW8260B Bromomethane <MDL ug/g 5.0 0711712002 74-83.9 S$V8260B Carbon Disulfide < MDL ug/g 5.0 0711712002 75-15.0 SW8260B Carbon Tetrachloride - < MDL ug/g 5.0 071172002 56-23.5 SW8260B Chloroacetonitrile < MDL ug/g 5.0 0711712002 107-14-2 SW8260B Chlorobenzene <MDL ug/g 5.0 0711712002 108.90-7 SW8260B Chloroethane <MDL ug/g 5.0 0711712002 75-00.3 SW8260B Chloroform <MDL ug/g 6.0 0711712002 67-66.3 SIV8260B Chloromethane < MDL ug/g 5.0 0711712002 74-87.3 SW8260B cis-1,2-Dichloroethene < MDL ug/g 5.0 0711712002 156-59-2 SVV8260B cis-1,3-Dichloropropene < MDL ug/g 5.0 07/17/2002 10061-01-5 SW8260B Dibromochloromethane <MDL ug/g 5.0 0711712002 12448.1 SW8260B Dibromomethane < MDL ug/g 5.0 0711712002 74-95-3 SW8260B Dichlorodifluoromethane < MDL ug/g 5.0 0711712002 75-71-8 SW8260H - Diethyl Ether <MDL ug/g 5.0 0711712002 60.29.7 SW8260B Ethyl Methacrylate <MDL ug/g 5.0 0711712002 97-63-2 SW8260B Ethylbenzene <MDL ug/g 5.0 0711712002 100-41-4 SW8260B Hexachlorobutadiene <MDL ug/g 5.0 0711712002 87-68.3 SW8260B Hexachloroethane < MDL ug/g 5.0 07/1712002 67-72-1 SW8260B lodomethane <MDL ug/g 5.0 0711712002 74.884 SW8260B Isopropylbenzene <MDL ug/g 5.0 0711712002 98-82.8 SW8260B meta-Xylene <MDL ug/g 6.0 07/17/2002 108-38-3 SW8260B Methacrylonitrile < MDL ug/g 5.0 0711712002 126.98.7 SW8260B Methyl t-Butyl Ether <MDL ug/g 6.0 071172002 1634-04-4 SW8260B Methylacrylate <MDL ug/g 5.0 071172002 96-33-3 SW8260B Methylene Chloride <MDL ug/g 5.0 071172002 75-09-2 SW8260B Methylmethacrylate < MDL ug/g 5.0 0711712002 80.62-6 SW82608 n-Burylbenzene < MDL ug/g 5.0 071172002 104.51-8 SW8260B n-Propylbenzene < MDL ug/g 5.0 071172002 103-65-1 SW8260B Naphthalene < MDL ug/g 5.0 071172002 91-20-3 SW8260B Nitrobenzene <MDL ug/g 5.0 071172002 98-95-3 SW8260B ortho-Xylene <MDL ug/g 5.0 071172002 95-47.6 SW8260B para-Xylene <MDL ug/g 5.0 0711712002 106.42-3 SW8260B Pentachloroethane < MDL ug/g 5.0 071172002 76.01.7 SW82608 Propionitrile < MDL ug/g 5.0 071172002 107-12-0 SW8260B sec-Butylbenzene <MDL ug/g 5.0 071172002 135-98-8 SW8260B Styrene <MDL ug/g 5.0 0711712002 100-42.5 SW8260B tert-Butylbenzene <MDL ug/g 5.0 071172002 98-06.6 SW8260B Lab Sample Number........ .......... ......... AA31124 Page 2 of 3 Volcitiles in Soo Annt)ais Performed/a RLH Parameter Result Units dIDL Date ofAnalvsis CAS N Method Reference Tetrachlaroethylene < MDL ug/g 5.0 0711712002 127.18.4 SfV8260B Tetrahydrofuran < MDL ug/g 5.0 0711712002 109-99-9 Sf1182608 Toluene < MDL ug/g 5.0 0711712002 108-88-3 SVV82608 trans-1,2-Dichlorcethene <MDL ugtg 5.0 0711712002 156.60.5 S)V8260B trans-1,3-Dichloropropene <MDL ug/g 5.0 0711712002 10061-02-6 SIV8260B trans-1,4-Dichloro-2-butene <MDL ug/g 5.0 0711712002 110.57.6 STV8260B Trichloroethene <MDL ug/g 5.0 0711712002 79-01-6 SIV8260B Trichlorofluoromethane < MDL ug/g 5.0 0711712002 75.69.4 SIV8260B Vinyl Chloride < MDL ug/g 5.0 0711712002 75-01.4 SIV8260B Lab Sample Number.............................. AA31124 page 3 of 3 ADEM A&NTGOMERY LABO*TORY pa 1890-A Cnng. Wm. DicAinson Dr..Mnnt_omcry. AL 36109)0( I)Jb/'-fin-]7701Phond I334P277.h)1%IFva � Analysis Report FAT Date of This Report... 09/03/2002 Fund Code• 521 Date of the Original Report 09/03/2002 Send Report... Anne F. Cross Lab Sample ID: AA31122 Source... SD-HSB-01 LocatiCollection Date: 07/11/2002 Sampan... WEST SEDIMEHUNTSVNT CLEANERS Collection Time: 10:30:00 AM Sample Matrix: SEDIMENT Submittal Date: 07/12/2002 Sample Collector: AFCross-AnneCross Submittal Time: 10:45:00 AM Sample Received by: C. D.AMMONS Date Analvsis Validated... 09/03/2002 by CDA The results on die attached report are from the sample that was received and is referenced above. The sample was analyzed using standard EPA testing procedures and quality analysis protocol. Instrument calibration and quality control are within acceptable limits of precision and accuracy. A close review by our Quality Assurance Program cerdfres that all prescribed test hold times were met and our strict quality assurance standards were observed. Submitted by: u:lli5y,,rl Quality Assurance Manager ADEM's Central Laboratory has met all Requirements for Certification by EPA Region Four to Analyze Samples fur all of the Parameters Required Under the Safe Drinking Water Act. Trace Metals Analysis Performed by.... ADC Parameter Result Units MDL Date of Analysis CAS# Method Reference Arsenic, Total < MDL ug/g 10.0 0910312002 7440.38-2 EPA200.7 Cadmium, Total <MDL ug/g 1.0 091032002 7440.43-9 EPA200.7 chromium, Total <MDL ugly 1.5 091032002 7440.47-3 EPA200.7 Lead, Total <MDL ug/g 10.0 091032002 7439-92-1 EPA200.7 Mercury, Total < MDL ug/g 0.10 07/16/2002 7439-97.6 EPA245.5 Volatiles in Solids Awl ysisPerformedby.... RLH _Parameter Result Units MDL Date of Analysis CAS# Method Reference 1,14,2-Tetrachloroethane <MDL ug/g 5.0 0711712002 630-20-6 SW8260B 1,1,1-Tcchloroethane <MDL ug/g 5.0 071172002 71-55-6 SW8260B 1,1,2,2-Tetrachloroethane <MDL ug/g 5.0 0711712002 79-34-5 $W82606 1,1,2-Tichloroethane < MDL ug/g 5.0 0711712002 79-00.5 SW8260B ' 1,1-Dichloroethane <MDL ug/g 5.0 07/172002 75-34.3 SW8260B 1,1-Dichloroethene <MDL ug/g 5.0 0711712002 75-35.4 SW8260B 1,1-Dichloropropanone <MDL ug/g 5.0 071172002 513-88-2 SW8260B 1,1-Dichloropropene <MDL ug/g 5.0 071172002 563-58-6 SW8260B 1,2,3-Trfchlorobenzene < MDL ug/g 5.0 0711712002 87.61-6 SW8260B 1,2,3-Trichicropropane <MDL ug/g 5.0 0711712002 96-18-4 SW8260B 1,2,4-Trfchlorobenzene <MDL ug/g 5.0 0711712002 120-82-1 SW8260B 1,2,4-Trimethylbenzene <MDL ug/g 5.0 071172002 95.63-6 SW8260B 1,2-Dibromo-3-Chloropropane <MDL ug/g 5.0 0711712002 96-12-8 SW8260B 1,2-Dibromoethane(EDB) <MDL ug/g 5.0 0711712002 106-93-4 SW8260B 1,2-Dichlorobenzene < MDL ug/g 5.0 071172002 95-50-1 SW8260B 1,2-Dichloroethane < MDL ug/g 5.0 0711712002 107-06-2 SW8260B 1,2-Dichloropropane < MDL ug/g 5.0 07/17/2002 78-87-5 SW8260B 1,3,5-Trimethylbenzene <MDL ug/g 5.0 071172002 108-67.8 SW8260B 1,3-Dichlorobenzene <MDL ugig 5.0 0711712002 541-73.1 SW8260B 1,3-Dichloropropane <MDL ug/g 6.0 071172002 142.28.9 SW8260B Lab Sample Number.............................. AA31122 Page 1 of 3 v0/Qtiles in SO Anu/�tviv Perfirrnr<'</G ' RLH Parameter t R Units't s 11D1 D to p lysis CAS N V! t/ d Reference 1,4-Dichlorobenzene < MDL ug/g 5.0 0711712002 106-46-7 ,SIV8260D 1-Chlorobutane <MDL ug/g 5.0 07117/2002 109-69-3 SVV8260B 2,2-Dichloropropane < MOL ug/g 5.0 0711712002 590-20.7 SW8260B 2-Butanone < MDL ug/g 5.0 0711712002 78-93-3 SW8260B 2-Chlorotoluene < MDL ug/g 5.0 0711712002 95-49-8 SIV8260B 2-Hexanone < MDL ug/g 5.0 - 0711712002 591.78-6 SIV8260B 2-Nitropropane < MDL ug/g 5.0 0711712002 79-46.9 SIVS260B 4-Chlorotoluene < MDL ug/g 5.0 0711712002 106-43-4 SW8260B 4-Isopropyltoluene < MOL ug/g 5.0 0711712002 99-87-6 SIV8260B 4-Methyl-2-pentanone(MIBK) < MDL ug/g 5.0 0711712002 108-10.1 SIV8260B Acetone < MDL ug/g 5.0 0711712002 67-64.1 SW8260B Acrylonitrile < MDL ug/g 5.0 0711712002 107-13-1 , SIV8260B Ally Chloride <MDL ug/g 5.0 0711712002 107.05-1 SIV82608 Benzene < MDL ug/g 5.0 0711712002 71.43-2 SVV8260B Bromobenzene < MDL ug/g 5.0 0711712002 108-86-1 SW8260B Bromochloromethane < MDL ug/g 5.0 07/172002 74-97-5 SIV8260B Bromodichloromethane < MDL ug/g 5.0 0711712002 75-27-4 SW82608 Bromoform < MDL ug/g 5.0 0711712002 75-25-2 SIV8260B Bromomethane < MDL ug/g 5.0 0711712002 74-83.9 SW8260B Carbon Disulfide < MDL ug/g 5.0 0711720,02 75-15.0 SW8260B Carbon Tetrachloride < MDL ug/g 5.0 0711712002 56-23-5 SW8260B Chloroacetonitrile <MDL ug/g 5.0 0711712002 107.14-2 SW8260B Chlorobenzene < MOL ug/g 5.0 071172002 108-90.7 SIV8260B Chloroethane < MDL ug/g 5.0 0711712002 75-00.3 SW8260B Chloroform < MDL ug/g 5.0 0711712002 67.66-3 SIV8260B Chloromethane <MDL ug/g 5.0 071/72002 74.87-3 SW8260B cis-1,2-Dichloroethene <MDL ug/g 5.0 071172002 156-59.2 SW8260B cis-1,3-Dichlaropropene < MDL ug/g 5.0 0711712002 10061-01.5 SW8260B Dibromochloromethane < MDL ug/g 5.0 0711712002 124-48-1 SW8260B Dibromomethane < MDL ug/g 5.0 071172002 74.96-3 SW8260B Dichlorodifluoromethane <MDL ug/g 5.0 071172002 75-71-8 SW8260B Diethyl Ether < MDL ug/g 5.0 0711712002 60-29-7 SW8260B Ethyl Methacrylate < MDL ug/g 5.0 071172002 97-63-2 SIV8260B Etylbenzene < MDL ug/g 5.0 071172002 100-41.4 SW8260B Hexachlorobutadiene <MDL ug/g 5.0 071172002 87-68.3 SW8260B Hexachloroethane <MDL ug/g 5.0 071172002 67-72-1 SW8260B lodomethane < MDL ug/g 5.0 0711712002 74-884 SW8260B lsopropylbenzene <MDL ug/g 5.0 0711712002 98-82-8 SW8260B meta-Xylene <MDL - ug/g 5.0 0711712002 108-38.3 SW8260B Methacrylonitrile <MDL ug/g 5.0 0711712002 126.98-7 SW8260B Methyl t-Butyl Ether < MDL ug/g 5.0 071172002 1634-04.4 SW8260B Methylacrylate < MDL ug/g 5.0 071172002 96-33-3 SW8260B Methylene Chloride <MDL ug/g 5.0 071172002 75-09-2 SW8260B Methylmethacrylate <MDL ug/g 5.0 071172002 80-62-6 SW8260B n-Butylbenzene < MDL ug/g 5.0 071172002 104-51.8 SW8260B n-Propylbenzene < MDL ug/g 5.0 071172002 103-65-1 SW8260B Naphthalene <MDL ug/g 5.0 071172002 91-20-3 SW8260B Nitrobenzene <MDL ug/g 5.0 071172002 98-95-3 SW8260B ortho-Xylene <MDL ug/g 5.0 071172002 95.47-6 SW8260H para-Xylene <MDL ug/g 5.0 0711712002 106-42.3 SW8260B Pentachloroethane < MDL ug/g 5.0 071172002 76-01-7 SW8260B Proplonitrile < MDL ug/g 5.0 071172002 107-12.0 SW8260B sec-Butylbenzene <MDL ug/g 6.0 071172002 135-98-8 SW8260B Styrene <MDL ug/g 5.0 071172002 100-42-5 SW8260B tert-Butylbenzene <MDL ug/g 5.0 071172002 98.06-6 SW8260B Lab Sample Number............ .. .. AA31122 page 2 of 3 Volatiles in Sol Anah'sis Performed br RLH Parameter Result Units AIDL Date ofOlysis CAS 1t Method Reference Tetrachloroethylene <MDL ug/g 5.0 0711712002 127-18.4 SW8260B Tetrahydrofuran <MDL uglg 5.0 0711712002 109-99-9 SVV82608 Toluene <MDL ug/g 5.0 0711712002 108-88-3 SW8260B trans-1,2-Dichlorcethene <MDL ug/g 5.0 0711712002 156-60-5 SVV8260B trans-1,3-Dichloropropene <MDL ug/g 5.0 0711712002 10061.02-6 SW8260B trans-1,4-Dichloro-2-butene <MDL ug/g 5.0 0711712002 110-57-6 SIV8260B Trichloroethene < MDL ug/g 5.0 0711712002 79-01-6 SW82608 Trichlorofluoromethane <MDL ug/g 5.0 0711712002 75-69.4 SIV8260B Vinyl Chloride <MDL ug/g 5.0 0711712002 75-01-4 SIV82608 Lab Sample Number AA31122 page 3 of 3 °o ADEM WNTGOMERY LABOV#TORY 1890-A Con.. Wm. Dickinson Dr.. Montgomery.AL?6109 034b260.27701phnnel 13341-277-6713 IFax1 1 t Analysis Report 4£AT Date of This Report.. 09/04/2002 Fund Code: 521 Date of the Original Report 09/04/2002 Send Report... Anne F. Cross Lab Sample ID: AA31126 Source... SO-HSB-D Location... WEST HUNTSVILLE CLEANERS Collection Date.- 07/11/2002 Sample Alatriz: SEDIMENT Collection Time: 10:30:00 AM Submittal Date: 07/12/2002 Sample Collector: AFCross-AnneCross Submittal Time: 10:45:00 AM Sample Received by: C. D.AMMONS Date Analvsis Validated... 09/04/2002 by WBB The results on the attached repo,are from the sample that was received and is referenced above. The sample was analyzed using standard EPA testing procedures and quality analysis protocol, Instrument calibration and quality control are within acceptable limits of precision and accuracy. A close review by our Quality Assurance Program certifies that all prescribed test hold times were met and our strict quality assurance standards were observed. Submittedby: 47,j g, �4'rr Quality Assurance Manager ADEM's Central Laboratory has met all Requirements for Certification by EPA Region Four to Analyze Samples for all of the Pammeten Required Under the Safe Drinking Water Act. Trace Metals Analvsis Performed by.... ADC Parameter Result Units MDL Date of Analysis CAS# Method Re erence Arsenic, Total <MDI, ug/g 10.0 0910312002 7440-38-2 EPA200.7 Cadmium, Total <MDL ug/g 1.0 0910312002 7440.43-9 EPA200.7 Chromium, Total <MDL ug/g 1.5 0910312002 7440.47-3 EPA200.7 Lead, Total < MDL ug/g 10.0 0910312002 7439-92.1 EPA200.7 Mercury, Total <MDL ug/g 0.10 0910412002 7439-97-6 EPA24S.S Volatiles in Solids Analysis Performed by.... RLN Parameter Result Units MDL Date o Analysis CAS# Method Re erence 1,1,1,2-Tetrachloroethane <MDL ug/g 6.0 0711712002 630-20-6 SW8260B 1,1,1-Trichloroethane <MDL ug/g 5.0 071172002 71-55.6 SW8260B 1,1,2,2-Tetrachloroethane <MDL ug/g 5.0 071172002 79-34-5 SW8260B 1,1,2-Trichloroethane <MDL ug/g 5.0 071172002 79-00-5 SW8260B 1,1-Dichloroethane <MDL ug/g 5.0 071172002 75-34-3 SW8260B 1,1-Dlchloroethene <MDL ug/g 5.0 071172002 75.35-4 SW8260B 1,1-Dichloropropanone <MDL ug/g 5.0 071172002 513-88-2 SW8260B 1,1-Dichloropropene <MDL ug/g 5.0 071172002 563-58-6 SW8260B 1,2,3-Trichlorobenzene <MDL ug/g 5.0 071172002 87.61-6 SW8260B 1,Z,3-Trichloropropane < MDL ug/g 5.0 071172002 96-18-4 SW8260B 1,2,4-Trichlorobenzene '<MDL ug/g 5.0 071172002 120-82-1 SW8260B 1,2,4-Trimethylbenzene <MDL ug/g 5.0 071172002 95-63-6 SW8260B 1,2-Dibromo-3-Chloropr4ane <MDL ug/g 5.0 071172002 96-12-8 SW8260B 1,2-Dibromoethane(EDB) < MDL ug/g 5.0 071172002 106-93-4 SW8260B 1,2-Dichlorobenzene < MDL ug/g 5.0 071172002 95-50-1 SW8260B 1,2-Dichloroethane <MDL ug/g 6.0 071172002 107.06-2 SW8260B 1,2-Dichloropropane <MDL ug/g 5.0 071172002 78.87-5 SW8260B 1,3,5-Trimethylbenzene <MDL ug/g 5.0 071172002 108.67.8 SW8260B 1,3-Dichlorobenzene <MDL ug/g 5.0 071172002 641-73-1 SW8260B 1,3-Dichloropropane <MDL ug/g 5.0 071172002 142-28.9 . SW8260B Lab Sample Number....................... AA31126 Page 1 of 3 Volatiles in SoliCI.V Analy.�;s Performed bv.... RLH Parameter Result Units b1D/ DateIvsis CAS x Method od Reference 1,4-Dichlarobenzene < MDL ug/g 5.0 07117/2002 106.46-7 SIV8260B 1-Chlorobutane < MDL ug/g 5.0 0711712002 109-69-3 SIV8260B 2,2-Dichloropropane <MDL ug/g 5.0 0711712002 590-20-7 SW8260B 2-Butanone < MDL ug/g 5.0 0711712002 78.93-3 SW8260B 2-Chlorotoluene < MDL ug/g 5.0 07/17/2002 95-49-8 SYV82608 2-Hexanone < MDL ug/g 5.0 0711712002 591.78-6 SIV8260B 2-Nitropropane < MDL ug/g 5.0 0711712002 79-46.9 SIV8260B 4-Chlorotoluene < MDL ug/g 5.0 0711712002 106.43.4 SIV8260B 4-Isopropyltoluene < MDL ug/g 5.0 0711712002 99-87.6 SW8260B 4-Methyl-2-pentanone(MIBK) < MDL ug/g 5.0 0711712002 108.10-1 SIV8260B Acetone < MDL ug/g 5.0 0711712002 67.64-1 SYV8260B Acrylonitrile < MDL ug/g 5.0 0711712002 107-13-1 SIV8260B Ally Chloride < MDL ug/g 5.0 0711712002 107.05.1 SW8260B Benzene < MDL ug/g 5.0 0711712002 71-43-2 SIV8260B Bromobenzene < MDL ug/g 5.0 0711712002 108-86-1 SIV8260B Bromochloromethane < MDL ug/g 5.0 07/172002 74.97-5 STY8260B Bromodichloromethane <MDL ug/g 5.0 0711712002 75-27-4 SYV82608 Bromoform < MDL ug/g 5.0 0711712002 75-25-2 SW8260B Bromomethane < MDL ug/g 5.0 0711712002 74.83-9 SW8260B Carbon Disulfide <MDL ug/g 5.0 0711712002 75-15-0 SIV8260B Carbon Tetrachloride < MDL ug/g 5.0 071172002 56-23.5 SW82608 Chlaroacetonitrile < MDL ug/g 6.0 071172002 107-14-2 SW8260B Chlorobenzene <MDL ug/g 5.0 0711712002 108-90-7 SW8260B Chloroethane <MDL ug/g 5.0 071172002 75-00-3 SW8260B Chloroform < MDL ug/g 5.0 0711712002 67-66-3 SW8260B Chloromethane < MDL ug/g 5.0 071172002 74-87-3 SW8260B cis-1,2-Dichloroethene <MDL ug/g 5.0 0711712002 156-59-2 SIV8260B cis-1,3-Dichloropropene < MDL ug/g 6.0 071172002 10061-01-5 SW8260B Dibromochloromethane < MDL ug/g 6.0 0711712002 124.48-1 SW8260B Dibromomethane <MDL ug/g 5.0 071172002 74.95-3 SW8260B Dichlorodifluoromethane < MDL ug/g 5.0 071172002 75-71-8 SW8260B Diethyl Ether < MDL ug/g 6.0 071172002 60-29-7 SW8260B Ethyl Methacrylate <MDL ug/g 5.0 071172002 97.63-2 SW8260B Ethylbenzene <MDL ug/g 5.0 071172002 100.41-4 SW8260B Hexachlorobutadiene <MDL ug/g 6.0 071172002 87-68-3 SW8260B Hexachloroethane < MDL ug/g 5.0 071172002 67-72-1 SW8260B todomethane <MDL ug/g 5.0 071172002 74-88-4 SW8260B Isopropylbenzene <MDL ug/g 6.0 071172002 98-82-8 SW8260B meta-Xylene < MDL ug/g 5.0 071172002 108.38-3 SIV8260B Methacrylonitrile < MDL ug/g 5.0 071172002 126-98.7 SW8260B Methyl t-Butyl Ether <MDL ug/g 6.0 071172002 1634-04-4 SW8260B Methylacrylate <MDL ug/g 5.0 071172002 96-33-3 SW8260B Methylene Chloride <MDL ug/g 5.0 071172002 75-09-2 SW82608 Methylmethacrylate <MDL ug/g 5.0 0711712002 80-62.6 SW8260B n-Butylbenzene <MDL ug/g 5.0 071172002 104-51-8 SW8260B n-Propylbenzene '<MDL ug/g 5.0 071172002 103.65-1 SW8260B Naphthalene <MDL ug/g 6.0 0711712002 91.20-3 SW8260B Nitrobenzene < MDL ug/g 6.0 071172002 98.95-3 SW8260B ,ortho-Xylene < MDL ug/g 5.0 071172062 95-47-6 SW8260B para-Xylene <MDL ug/g 5.0 0711712002 106.42-3 SW8260B Pentachlaroethane <MDL ug/g 5.0 071172002 76.01-7 SW8260B Propionitrile <MDL ug/g 5.0 071172002 107-12-0 SW8260B sec-Butylbenzene < MDL ug/g 5.0 071172002 135-98-8 SW8260B Styrene < MDL ug/g 5.0 071172002 100-42.5 SIV8260B tert-Butylbenzene < MDL ug/g 6.0 071172002 98-06-6 SW8260B Lab Sample Number............................. AA31126 Page 2 of 3 VOlufiles in Solids Analevis PerJnnaed bv.... RLH Parameter Result Units tIDL Date n AMlvs's CAS# Method Reference Tetrachloroethylene c MDL ug/g 5.0 0711712O02 127-18.4 SIV82608 Tetrahydrofuran < MDL ug/g 5.0 071172002 109-99.9 SW82608 Toluene < MDL ug/g 5.0 0711712002 108.88-3 SW8260B trans-1,2-Dichloroethene < MDL ug/g 5.0 071172002 156-60.5 SW8260B trans-1,3-Dichloropropene < MDL uglg 5.0 0711712002 10061-02-6 SIV82608 trans-1,4-Dlchlara-2-butene < MDL ug/g 5.0 0711712002 110-57.6 SIV8260B Trichloroethene < MDL ug/g 5.0 071172002 79.01-6 SW8260B Trichlorofluoromethane <MDL ug/g 5.0 0711712002 75-69-4 SW8260B Vinyl Chloride < MDL ug/g 5.0 071172002 75.01-4 SIV82608 Lab Sample Number.............................. AA31126 page 3 of 3 ATTACHMENT 10 Y` /1 -4DEM ALABAMA DEPARTMENT OF ENVIRONMENTAL MANAGEMENT \ = POST OFFI BOx W1463 36130.1463 4 14M CMMs NBM. 36110.M59 MONTGOMERY, ALABAMA JMIES W.WARR V.Mw.ADEM.STATE.AL.W DON SIEGELMAN D. (334)271-7700 _ G R Facsimiles:(33Q February 13, 2001 / wm015�4m:271-]550 Gmmd OOunF Nr 4i : 27 31Y30M ;B Lana: 3743 .. WMp: x793051 MEMORANDUM GunMnter: x]USW, FiNU Op Vws: 072b131 tcca B3j, � �m TO: Stephen A. Cobb,Chief Hazardous Waste Branch Land Division ^`1N31415167�e',, \ FROM: Joseph L. Gibson,Hydrogeologist 1.1 ��Y c'oN \ Groundwater Branch fill FEB 2001 'u ' n Water Division REAeEIVVED )t GROUNDWATER $' RE: Preliminary Assessment- Groundwater \ �+ BR:1NCH yro % Former John Blue SiteDSSZtiZ�y9b `i Huntsville,Madison County, Alabama The following groundwater report was prepared through a search of literature and information available to the Groundwater Branch. The author has not conducted a site reconnaissance and the findings in this report have not been field verified. LOCATION The Former John Blue Site is located in Huntsville, Madison County, Alabama (Figure 1). The United States Geological Survey's (USGS) 7.5 Minute Quadrangle Map entitled Huntsville, Alabama shows the location of the site to be in the SW '/4 of the SE '/4 of the SW '/4 of Section 2 Township 4 South, Range 1 West (Figure 2). The latitude and longitude have been estimated to be 340 42' 48" North Latitude and 860 36' 15" West Longitude. TOPOGRAPHY AND SURFACE WATER The site is situated in central Madison County in the Tennessee Valley District of the Highland Rim Section of the Interior Low Plateaus Physiogmphic Province. The Tennessee Valley District consists of plateaus of moderate relief with chert belts in the north and limestone plains along the rivers. Elevations in this district range from 600 to 800 feet MSL (Sapp & Emplaincourt, 1975). The surface elevation at the site is approximately 620 feet MSL . amcaam eam O ur 6rmd, MW4e6 N Ie_coaalal Ito V'1—Raa4 x]t55eMln Roae.3.w_ 330t PMmalm Rmx 4171 CO01m,ders Ww 91mn5 NaMm ]SxG1F<70] 00.abr,Wpairo 3 11333 MOtiIe,NWwro M15.1131 M Ie,Na JS "'121 �] (305)0s3410 (M)35Y1713 OU 4'A3100 133<l a3]2'3T 13051a41-10031Fa�1 PM)..9 IF.1 r>HI4]8 W[FvI 1334143345M IFae] PMIW m FsgdH PaCM Surface water drainage from the site (Figure 3) appears to be to the east into an unnamed tributary of Merrimac Branch. The unnamed tributary of Merrimac Branch flows approximately 1.23 miles to the south and flows into Merrimac Branch. From this point Merrimac Branch flows approximately 0.07 miles to the southeast into Huntsville Spring Branch. Huntsville Spring Branch flows approximately 11.2 miles to the southwest into Indian Creek, and Indian Creek comprises the remainder of the 15-mile surface water pathway from the site. The last 4.25 miles of Huntsville Spring Branch and the 2.5 miles of Indian creek along the surface water pathway are considered to be within Wheeler Lake. The unnamed tributary of Merrimac Branch and Merrimac Branch are not listed in the ADEM Admin. Code R. 335-6-11-.02 with a use classification; however,it is noted in the regulations that segments not listed should be designated as fish and wildlife. Huntsville Spring Branch and Indian Creek are listed with use classifications of fish and wildlife. Low flow data was not available for the unnamed tributary of Merrimac Branch, Merrimac Branch, and Huntsville Spring Branch; however, these streams are small to minimal streams and the low flow rates are estimated to be less than 10 cfs. Indian Creek has a seven day ten year low flow rate of 2.9 cfs and a seven day two year low flow rate of 4.0 cfs (Hayes, 1978). Wetlands are present along approximately 4.5 miles of the surface water pathway, and no known surface water intakes for public drinking water supplies are located along the 15- mile surface water pathway from the site. Approximately 8.9 miles of the surface water pathway is located within the boundary of the Wheeler National Wildlife Refuge. SOILS The soils mapped at the site are classified by the Soil Conservation Service as Decatur and Cumberland silty clay Ioams, eroded undulating phases. Soils in this classification are dark-red, well drained soils that consists of residuum from high-grade limestone and alluvium derived from high-grade limestone. Soils in this unit consists of Decatur and Cumberland soils that have properties so nearly alike and are some intermixed that it is impractical to map them separately. The permeability of these soils is moderate, and they have a slope of 2 to 6 percent(Swenson,et al., 1958). GEOLOGY Geologic units exposed in Madison County range in age from Silurian to Pennsylvanian and consist mainly of Mississippian limestones overlain by outliers of Pennsylvanian sandstone, shale, and coal. The units are essentially flat-lying with a gentle dip to the south and the east(LaMoreaux,et al., 1950). The geologic unit that outcrops in the vicinity of the site is the Tuscumbia Limestone (Figure 5). This unit consists of massive and thin beds of coarsely crystalline dark to • O light-gray compact limestone. The Tuscumbia Limestone contains interbedded layers of gray chert and the thickness of this unit in the Huntsville area is approximately 200 feet (LaMoreaux, et al., 1950). The site is located in an area that is underlain by limestone and is susceptible to karst development. HYDROGEOLOGY The aquifers that have recharge areas in the vicinity of the city of Huntsville are the Fort Payne — Tuscumbia aquifer, Monteagle aquifer, and the Bangor aquifer. The site is located in the recharge area of the Fort Payne —Tuscumbia aquifer (Moore, 1992). The Fort Payne—Tuscumbia aquifer is composed of the Monteagle Limestone, the Tuscumbia Limestone, and the Fort Payne Chert. The most significant sources of water in this aquifer are the Tuscumbia Limestone and the Fort Payne Chert. The aquifer is recharged throughout its outcrop area by water that infiltrates through the regolith, and is partially confined due to the lower hydraulic conductivity of the overlying regolith. The majority of water available in this aquifer is present in joints and bedding planes that have been enlarged by dissolution(Bossong and Harris, 1987). There are 3 active public water supply wells and 1 inactive public water supply spring located within 4 miles of the site (Figure 6). The closest active public water supply well (Lowe Mill Well) is operated by Huntsville Utilities, and is located approximately 0.4 miles to the northeast of the site. WELL ID OWNER AQUIFER DEPTH USE DISTANCE (feet) {miles) Braham Spring Huntsville Utilities Mtf S rin Inactive E Lowe Mill Well Huntsville Utilities Mtf 76 Public Water Su I 0.4 Dallas Well Huntsville Utilities Mtf 104 Public Water Supply 2.6 Lincoln Well Huntsville Utilities Mtf 106 Public Water Supply 2.6 Mir -Tuscumbia Limestone and Fort Payne Chen undifferentiated(Bossong and Harris, 1987) Samples collected from Braham Spring on August 26, 1997 detected tetrachloroethylene at 0.6 ppb and trichloroethylene at 0.9 ppb, and groundwater samples collected from the Lowe Well on August 31, 2000 detected tetrachloroethylene at 1.7 ppb and trichloroethylene at 2.6 ppb. Groundwater samples collected from the Dallas Well on August 31, 2000 detected tetrachloroethylene at 10.6 ppb, and groundwater samples collected from the Lincoln Well on August 31, 2000 detected tetrachloroethylene at 4.1 ppb and trichloroethylene at 6.8 ppb (FRDS, 2000). A treatment system has been constructed to treat contaminated water pumped from the Lincoln and Dallas wells prior to delivery to the water system. The Huntsville Utilities water system is a blended system that uses 40 percent groundwater and 60 percent surface water. The system serves a population of 198,000 and obtains water from two surface water intakes on the Tennessee River and five wells (FADS, 2000). The site is located in the wellhead protection areas for Braham Spring and the Lowe well, and the general groundwater flow direction in the area of the site is to the southeast (Baker and Mann, 1996). Private water supply wells are not expected in the immediate vicinity of the site due to the urban nature of the site. CLIMATE Madison County has a mild, temperate climate with an average annual temperature of 62°F. The average temperature during the summer is 80°F, and the average temperature during the winter is 460F(Malmberg and Downing, 1957). The average annual rainfall is 52 inches, and approximately 22 of the 52 inches of rain per year runs off into the streams (Bossong and Harris, 1987). cc: Larry Norris,Northern Compliance Section Jymalyn Redmond, Chief,Site Assessment Unit SELECTED REFERENCES Alabama Department of Environmental Management, Federal Reporting Data System (FRDS-II), 2000, Public Water Supply Summary: Municipal Drinking Water Supplies serving the Huntsville,Alabama. Bossong, C. R., and Harris, W. F., 1987, Geohydrology and Susceptibility of Major Aquifers to Surface Contamination in Alabama;Area 1, United States Geological Survey, Water Resources Investigation Report 87-4068. Baker, Robert, M., and Mann, S. D., 1996, Groundwater Flow Paths and Wellhead Protection Area Boundaries for the Lincoln —Dallas, and Lowe Mills Well, and Brabant Spring,Huntsville Utilities Water Department,Madison County,Alabama,Plate 5. LaMoreaux, P. E., Swindle J. R. Jr., and Lanphere, C. R., 1950, Groundwater Resources of the Huntsville Area, Alabama, Geological Survey of Alabama,Bulletin 62. Malmberg, Glenn T., and Downing, H. T., 1957, Geology and Groundwater Resources of Madison County, Alabama,Geological Survey of Alabama,County Report 3. Moore, James D., 1992, Aquifers in Alabama, Geological Survey of Alabama, Special Map 231. Sapp, Daniel C., and Emplaincourt, J., 1975, Physiographic Regions of Alabama, Geological Survey of Alabama,Map 168. Swenson, G. A., Sherard, H., Baxter, A., Farnham, R., Wesson, H. J., and Young, B. E., 1958, Soil Survey of Madison County, Alabama, United States Department of Agriculture,Soil Conservation Service. GROUNDWATER ROUTE WORKSHEET REQUIREMENTS Route Characteristics Aquifer of concern Fort Payne-Tuscumbia aquifer Gross Precipitation 52 inches Net Precipitation 10 inches (from FIRS) DDte th to Aquifer 0 to 25 feet Slope 2 to 6 percent Permeability of Unsaturated Zone 4.2 X 10'to 1.4 X iCr cmtsec. Is the Site Susceptible to Karst Yes TARGETS Groundwater use- There are 3 active public water supply wells located within four miles of the site. Distance to nearest public supply well—0.4 miles. 0 0 Former John Blue Site ALABAMA x 7f Study Area W 'v` E a 5 d Figure 1 I� C) Site Location Map pp • E II_ Fr �1—t 1 iil� / aY • •. \l - 1\ C a III L = VEafi 5 ! G H elh$ 171 M \ .g • 1 1 tiV ftu6 I .A �A. �). 4 HV 1f, MIII , r We Ivwn' ,t. \ Er Site 3s rFEaw `\ Location ! jjJJl/ a i� •' Feet 0 1,000 2,000 3,000 4,000 N Former John Blue Site Huntsville, Madison County, Alabama Huntsville, Alabama U. S.G.S. Topographic Map 1975 Figure 2 Soil Types Mapped at the • eormer John Blue Site ----------- )3 P kladkor L T` I Avcscwnls ijlc r,'\- Site Location Dt f C, - 1W e-L V 19 h NE D Op - Ooltewah Silt Loam Feet Df - Decatur and Cumberland silty clay[Dams 0 1000 20M 30M N U.S. Department of Agriculture Soil Conservation Service W*E Madison County, Alabama S Sheet # 40 Figure 4 logic Units Mapped Neal e Former John Blue Site w- ,Mt a /' �:w: . �S,^ R` Q • � t, t a-! fir -/ •JT. tir. hzw. m 4E Y 1 M. x VIM, f�'^w44 {� �{ ill 4 .a �• 1� # M+ +Hri vine r` IM� ,�1.. L, Sne Location � ' y w Miles Mm - Monteagle Limestone Mt - Tosoumbia limestone Mfp - Fort Payne Chen 0 1 2 4 Geologic Map of Alabama Northeast Sheet 1988 N W.E. Osborne, Michael W. Szabo,Thornton L.Neathery, and Charles W. Copeland Jr. w E Geological Survey of Alabama Special Map 220 Figure 5 s Public Water Supply Wells in the Vicinity of Former John Blue Site . iLincoln ' }7y Well Dallas . ei Well NE O Exit 19AD � . { Exit 19AB . . Ile ' Huntsville Exit 19AB NW ' LU Herm' cri Governors Dr _ ,_a Lowe G Ave S n 2 Mill Well 1�5 JY Y Sth Ave Sll1! Ob W2q( Mayfair e &e ;SW1 Site Bra�m Location 5 Drake Ave SW D A -Public Water Supply Well Location Miles N 0 0.5 l 1.5 W+E Base Map— Streets 98 1988-1997 Microsoft Corporation S Well Information—ADEM GPS Data Figure 6 r ATTACHMENT 11 WORKSTATION 74-13186:AFCre 11:31:25 am Monday August 26, 2002 as+++.wwaaa+wa+xx++x»a.+xwaax»aaaa+aaa+a+aaaw».xaaa.ax++x+waw++xa a+x«axa.a+++.+++.++++w++« ** 1 2 3 - 4 5 6 7 8 * 12345678901234567890123456789012345678901234567890123456789012345678901234567890 aaaaa.aaaaxwaxa+.w+.wa+x++xw»+wwwawaaawawwxwa+wa+awax+++a++xawa++aaawaaa+wwa.waw.w+waaaa.+ ' 1* Display ORGANIC ANALYSIS INFO ,•r i-; by p'rl rC1 « 1' 2' I 2« ' 7* USERID: NL * 3* ' 4* DATESTAMP: 03/09/99 * 4* * 5* TIMESTAMP: 17:07:55.79 * 5* * 6* PWS TYPE: C ACTIVITY: A SAMPLE ID: 00239 * 6* 7* 7* * 8* PWS ID: AL 0000882 SAMPLE DATE: 08/26/97 SAMPLE TIME: 12:00 t$AMPLE• POINT: '002h* 8* 9* 9* *10* *10* ' 1* CONTAMINANT ID: 2987 NAME: TETRACHLOROETHYLENE/ * 1* 2* * 2a * 3* ANALYSIS ANALYSIS ANALYSIS 3* * 4* RESULTS: 0.000600001 mg/l DATE: 09/02/97 METHOD: 524.00 * 4* 5* 5* 6* 6* * 7* TYPE OF ORGANIC: U * SAMPLE POINT IS THE SMAE AS SE ID FROM THE SOURCE * 7' ` 8* ENTITY INFO. * 8* 9' 9a *20* 15) Output *20* ' 1* 6) Add / Send * 1* ` 2* 16) Return * 2' * 3* 4) Prev / First 8) Delete * 3' * 4* 5) Next / Last 9) Modify * 4* a aaaa+w aw as+x a.ax.aax+awwaa..awa«aaaaaa+awawww+++++.aaaa::aaaa++::aaaa+w::aaaa«+aaaa.w++.a 1 2 3 4 5 6 7 8 '* ** 12345678901234567890123456789012345678901234567890123456789012345678901234567890 ** ++waa.as ax awaawaa+wwaaa++++++.+++.+w+++++++aaaa.aaaa ww ax wwawwa as aw+x..aaa++.:aaaa+«+a a.aaw WORKSTATION 74-13186:AFCr0 • 11:31:42 am Monday August 26, 2002 a+a+a««.x.+axa.*aa.wwwwawaawwaa..*aaa«aaw.+e+.+«wa«+*.*xwa++*a+a aaawaxxaa«a«+.+ ' 1 2 3 4 5 6 7 8 • •* 12345678901234567890123456789012345678901234567890123456789012345678901234567890 •"* • 1* Display ORGANIC ANALYSIS INFO 1* 2* 2a • 3* USERID: NL * 3" " 4* DATESTAMP: 03/09/99 * 4• 5* TIMESTAMP: 17:07:55.60 " 5* * 6* PWS TYPE: C ACTIVITY: A SAMPLE ID: 00239 * 6* 7" 7* * 8" PWS ID: AL 0000882 SAMPLE DATE: 08/26/971 SAMPLE TIME: 12:00 *SAMPLE POINT: '0021 8* 9• 9* *10* *10* • 1" CONTAMINANT ID: 2984 NAME: TCE (TRICHLOROETHYLENE)+ * 1• 2• 2* * 3' ANALYSIS ANALYSIS ANALYSIS * 3* * 4* RESULTS: 0:000900001 mg/l DATE: 09/02/97 METHOD: 524.00 * 4* 5* 5* 6* 6* " 7* TYPE OF ORGANIC: R * SAMPLE POINT IS THE SMAE AS SE ID FROM THE SOURCE * 7" " 8* ENTITY INFO. • 8* * 9« 9* *20* 15) Output *20* ` 1* 6) Add / Send * 1* ' 2' 16) Return * 2* * 3* 4) Prev / First 8) Delete a 3* ' 4* 5) Next / Last 9) Modify * 4* aaaa+*+aaa++aaa*xxa.++++++a+aa+a++a+.aaa«*xa«a+a a aa«wxwaaa+aaaa++aaa««a a««+a 1 2 3 4 5 6 7 8 12345678901234567890123456789012345678901234567890123456789012345678901234567890 '* WORKSTATION 74-13186:AFCris • 2:50:18 pm Wednesday August 28, 2002 +awx.xxxawxx«wx«ax«*x.x«aa*w+*w+.xwaa+++xxax+w+axxxw+aa**x.xaaxxax xx+xxx a*wxxx.a.aara+.axw 1 2 3 4 5 6 7 8 *** **" 12345678901234567890123456789012345678901234567890123456789012345678901234567890 •• a a a+xxaxaxaaxaaxa a+wxwaaaaaaa*xx«aaa+aaa«awx+w+aaa aaae*««ea*xaaxx*«xwx xxax as aaaaaaa•aaa a*+ / I a • 1* Display ORGANIC ANALYSIS INFO 2* n_ ,JUe '111i!l �f�1.�� * 1' 2a * 3* USERID: NL * 3* • 4' DATESTAMP: 03/09/99 * 4* ' S* TIMESTAMP: 17:03:04.35 * 5• * 6* PWS TYPE: C ACTIVITY: A SAMPLE ID: 00014 * 6• 7- * 7* * 8* PWS ID: AL 0000882 SAMPLE DATE: 07/22/88 SAMPLE TIME: 12:00 *SAMPLE POINT: 006 • 8* * 9* 9* *10x *10* ' 1* CONTAMINANT ID: 2987 NAME: TETRACHLOROETHYLENE * 1* 2* 2* • 3* ANALYSIS ANALYSIS ANALYSIS ' 3* • 4* RESULTS: 0.00600000 mg/1 DATE: 08/01/88 METHOD: 502.00 * 4* « S* * 5• 6* * 6* • 7* TYPE OF ORGANIC: U * SAMPLE POINT IS THE SEAS AS SE ID FROM THE SOURCE • 7* • 8* ENTITY INFO. * 8* a 9* * 9* *20* 15) Output *20* ' 1* 6) Add • / Send • 1*2* 16) Return * 2* * 3* 4) Prev / First 8) Delete * 3* * 4* 5) Next / Last 9) Modify * 4- x.x a+xxa.a wxaaxa as aa. +xxxxx«w« x««++waaa*a*.*x««aw*xxx aaax«aa*««aa.«x+**aa:: `1' ax2 as a*3 *4 5 6 7 8 ' 12345678901234567890123456789012345678901234567890123456789012345678901234567890 a*+x«aa aa«xa.+«a*xaa+wx«««aaaxa«aaaa***+**wx**wa aaaa aaaaa aaa*.«aaawx«aa ax«aaaaaa+aaax+..«+ WORKSTATION 74-13186:AFCr* • 11:30:20 am Monday August 26, 2002 +.a«xx.xwaw+xx+.x.+xxwa++xx..«««xxxwx xxxxxxa«awx xa«awxx..xxxa+xxaxa++xaw.aaaaxx x«a.xx+awaa ' 1 2 3 4 5 6 7 8 •"` •• 12345678901234567890123456789012345678901234567890123456789012345678901234567890 •• .aa.aaaaa xwawax.a.xx.+xwwawwwwwww+asaaaa.awawwaaaawa«a.aa++axwaaww++xxwaa..aaa«aa as waa.aww 2* Display ORGANIC ANALYSIS INFO LOW N11II ( I 2* ' 3• USERID: BAL * 3* ' 4* DATESTAMP: 10/19/00 * 4* * 5• TIMESTAMP: 15:05:36.31 * 5* • 6* PWS TYPE: C ACTIVITY: A SAMPLE ID: 00831 ' 6* 7w 7a ' 8* PWS ID: AL 0000882 SAMPLE'DATE: 08/31/00.'SAMPLE TIME: 12:00 *SAMPLE POINT: 006— 8• 9* * 9* *10* *10* ' 1' CONTAMINANT ID: 2987 NAME: TETRACHLOROETHYLENE . * 1* 2+ 2+ * 3* ANALYSIS ANALYSIS ANALYSIS * 3* * 4* RESULTS: 0.00176000., mg/l DATE: 09/07/00 METHOD: 524.20 ' 4* 5* 5* 6* 6* • 7* TYPE OF ORGANIC: U • SAMPLE POINT IS THE SMAE AS SE ID FROM THE SOURCE • 7* * S• ENTITY INFO. * 8* 9* 9• *20* 15) Output *20* * 1• 6) Add / Send * 1* * 2* 16) Return * 2* ' 3* 4) Prev / First 8) Delete * 3* * 4* 5) Next / Last 9) Modify • 9' +aax.wwxaaaa«aa ax xw.+«xxw aaww«w.xww xxx««++aaaa+wxx«+aaa++aaaw++.ax«xwa:as««x x.««aa::::aaaa 1 2 3 4 5 6 7 8 *• • 12345678901234567890123456789012345678901234567890123456789012345678901234567890 • ` .xww:a as+«xxw:.x.aa+xwaaaa.aaawaxwaaaaawxxxaxaaawaaawx«+«+a«xx.xwxaa a++««xw aw awawxa as awxaa ATTACHMENT 12 ® p O F �T} i5wx, ADEM GeoFrobeO in position to install a boring and obtain a groundwater sample at the John Blue Company Site Foundation of one former foundry building at the former John Blue site in Huntsville, AL Facing east at the foundation of the former foun buildin Facing south from the former foundry foundation showing GW-JBC-02 location behind Virginia College i GeoProbe®drilling and sampling of GW-JBC- 01 by ADEM personnel , A ADEM Personnel obtaining sediment and water samples along the surface water pathway from John Blue Co. Surface water and sediment sampling along the unnamed tributary and Huntsville Spring Branch Water Intake pipe at Braham Spring Braham Spring intake building o ADEM Personnel sampling public water supply at Lowe NO Well,Huntsville,AL Decontamination station for GeoProbeg equipment and GeoProbeg trailer at location for boring GW-IBC-03 y,